雾化进样石墨炉原子吸收光谱法的研究 Ⅰ.直接雾化进样装置及其性能

介绍一种自行设计和加工的直接雾化石墨炉进样装置的结构、工作原理和操作方法。该装置由微机控制与石墨炉加热程序同步工作,可以实现自动控制和自动测量。对雾化进样石墨炉分析的仪器参数和实验条件进行了研究和选择。结果表明,该装置与石墨炉结合具有自动化程度高、重现性好、样品利用率高和分析速度快等特点。     

Fast iterative solution of large undrained soil‐structure interaction problems

In view of rapid developments in iterative solvers, it is timely to re‐examine the merits of using mixed formulation for incompressible problems. This paper presents extensive numerical studies to compare the accuracy of undrained solutions resulting from the standard displacement formulation with a penalty term and the two‐field mixed formulation. The standard displacement and two‐field mixed formulations are solved using both direct and iterative approaches to assess if it is cost‐effective to achieve more accurate solutions. Numerical studies of a simple footing problem show that the mixed formulation is able to solve the incompressible problem ‘exactly’, does not create pressure and stress instabilities, and obviate the need for an ad hoc penalty number. In addition, for large‐scale problems where it is not possible to perform direct solutions entirely within available random access memory, it turns out that the larger system of equations from mixed formulation also can be solved much more efficiently than the smaller system of equations arising from standard formulation by using the symmetric quasi‐minimal residual (SQMR) method with the generalized Jacobi (GJ) preconditioner. Iterative solution by SQMR with GJ preconditioning also is more elegant, faster, and more accurate than the popular Uzawa method. Copyright © 2003 John Wiley & Sons, Ltd.     

Ammonium regeneration in intertidal sediments of the Yangtze estuary during air-exposure

The influences of exposure to the atmosphere on ammonium cycle in the intertidal surface sediments were in situ studied with a geochemical approach at a typical station in the Yangtze Estuary during three tidal cycles in September 2003. During an about 8-h emersion period of each diurnal tide, six high-resolution vertical profiles of adsorbed and dissolved ammonium were measured. It was observed that both adsorbed and dissolved ammonium generally had an increasing trend in sediment cores during the exposure. The rate of ammonium regeneration in sediments was estimated using the accumulation amount of ammonium including adsorbed and soluble fractions during the daytime emersion. The calculation result showed that there was relatively high ammonification rate (˜500 nmol N cm⁻³ day⁻¹), which reflected that organic nitrogen in sediments was quickly decomposed with a residence time of ˜52.7 days. Due to the dramatic temperature difference observed in sediment profiles, free convection was considered an important mechanism of regulating the efflux of produced ammonium into overlying waters. The total estimated amount of regenerated ammonium was ˜1.35×10⁵ t N year⁻¹ in the intertidal flat of the Yangtze Estuary, which occupied 7.6% of the total inorganic nitrogen annually transported to the estuarine ecosystem.     

中国和日本梅雨锋区（个例）结构的比较

通过１９８２年梅雨期的个例分析，研究和比较了中国和日本梅雨我的结构。分析表明：１．梅雨锋区系统对流层上部宽广的斜压区和对流层低层较狭窄的弱斜压区共同组成；２．在两个个例中，中国剖面上锋区均呈“椅”型结构。日本剖面上，６月呈均匀倾斜结构，７月略呈“椅型”，涡度场上中国剖面为相当正压结构，日本剖面为斜压结构；３．梅雨锋区系统可民是均匀斜压区在不均匀和加热情况下结构改变结果；４．中国大陆雨区高层大量潜热     

Properties of wave velocity for two types of granitoids at high pressure and temperature and their geological meaning

The wave velocity for two types of granitoids was measured using the analytic method of full-wave vibration at high pressure and high temperature. The laws of velocity changes for them differ with the pressure boost and temperature rise, and the velocity change of S-type is more violent than that of I-type. The “softening point” of compressional wave velocity (V μ) is also revealed during the measurement for two types of granitoids imitating the pressure and temperature at a certain depth. But the depth of “softening”, V_p after “softening” and the percentage of V_p’s drop around the “sofrening point” for two types of granitoids are obviously different. The depth of “softening” is 15 km approximately and V_p after “softening” is 5.62 km/s for S-type granitoid. But for I-type granitoid the depth of “softening” is 26 km approximately and V_p after “softening” is 6. 08 km/s. Through careful analysis of rock slices after the experiment, it was found that the “softening” of elastic-wave velocity is caused by the partial melting of granite. Combined with the results of geophysical prospecting, these results suggest that the low-velocity layers developing in the interior of Earth crust are related to thc partial melting of different types of granitoids. The formation of the low-velocity layer in the upper-middle Earth crust is closely related to the development of S-type granitoid, but that in the lower Earth crust is closely related to the development of I-type granitoid.     

Budd—Chiari综合征的CT评价

回顾性分析了５２例Ｂｕｄｄ－Ｃｈｉａｒｉ综合征的ＣＴ表现，ＣＴ显示肝尾叶增大５０例（９６％），肝脏呈低度密度或密度不均，４２例（８１％）肝静脉未明显，２２例（４２％）见有肝内侧枝血管，４９例（９４％）有肝外侧枝血管，作者认为ＣＴ检查对Ｂｕｄｄ－Ｃｈｉａｒｉ综合征有较高的诊断价值。     

中国地质统计学（空间信息统计学）发展的回顾与前景

讨论了地质统计学（空间信息统计学）发展的若干问题，其内容包括４部分：１．地质统计学的理论及方法；２．关于软件系统的现状；３．关于实际应用；４．地质统计学发展前景的若干看法。     

Soil respiration in tropical seasonal rain forest in Xishuangbanna, SW China

With the static opaque chamber and gas chromatography technique, from January 2003 to January 2004 soil respiration was investigated in a tropical seasonal rain forest in Xishuangbanna, SW China. In this study three treatments were applied, each with three replicates: A (bare soil), B (soil+litter), and C (soil+litter+seedling). The results showed that soil respiration varied seasonally, low from December 2003 to February 2004, and high from June to July 2004. The annual average values of CO2 efflux from soil respiration differed among the treatments at 1% level, with the rank of C (14642 mgCO2· m-2. h-1)＞B (12807 mgCO2· m-2. h-1)＞A (9532 mgCO2· m-2. h-1). Diurnal variation in soil respiration was not apparent due to little diurnal temperate change in Xishuangbanna. There was a parabola relationship between soil respiration and soil moisture at 1% level. Soil respiration rates were higher when soil moisture ranged from 35% to 45%. There was an exponential relationship between soil respiration and soil temperature (at a depth of 5cm in mineral soil) at 1% level. The calculated Q1o values in this study,ranging from 2.03 to 2.36, were very near to those of tropical soil reported. The CO2 efflux in 2003was 5.34 kgCO2· m-2. a-1 from soil plus litter plus seedling, of them 3.48 kgCO2· m-2. a-1 from soil (accounting for 62.5%), 1.19 kgCO2· m-2. a-1 from litter (22.3%) and 0.67 kgCO2·m-2. a-1 from seedling (12.5%).     

平和县灵通山旅游开发策略

闽南漳州市的平和县灵通山，是福建省第三批省级风景名胜区，但目前仍处于旅游地的参与阶段。要进入发展阶段，实现景区开发的经济、社会和环境效益，必须在明确旅游开发主体的前提下，挖掘旅游资源潜力、科学规划与设计景点、塑造鲜明的旅游形象并有针对性地进行旅游市场营销。此外，改善交通状况、完善景区解说系统、营造良好的旅游社会环境也是必不可少的重要策略。     

微陆块属性厘定的依据——以中亚造山带南缘中段为例

造山带中残存有许多前寒武纪地质体,其中一些被当作前寒武纪基底用于探讨所在微陆块的大地构造属性。由于微陆块属性对于造山带结构和演化具有重要意义,以及所讨论的前寒武纪地质体蕴含地球早期历史演化信息,对微陆块属性的厘定成为造山带研究的重点和难点问题之一。笔者等以中亚造山带南缘中段的微陆块为例,总结梳理了微陆块厘定的相关依据：岩石组合和变质变形特征,碎屑锆石谱峰显示的源区时代特征,地质事件序列,前寒武纪地壳演化信息,继承锆石、捕获锆石和古生代侵入体同位素显示的深源地壳信息,以及地球物理等方面的特征。由于不同学者采用的厘定依据不同,对微陆块属性认识争论不断,即使相同依据也有一定的差异,从而影响对造山带结构和演化的认识。基于以上原因,笔者等认为前寒武纪基底的亲缘性探讨不仅要注重岩石组合和形成时代,还要在精细野外解剖和高精度年代学工作基础上,注意其变质—变形特征、接触关系、源区时代特征、岩石成因和构造环境、地壳增生信息和深源地壳信息等的综合对比分析,以得到较全面依据,探讨其构造属性。当获得一组前寒武纪地质体信息时,可先进行同构造单元内对比,再与其他构造单元对比。当特征相异时则需进行构造单元拆分或考虑构造就位的可能（包括但不限于推覆体、走滑外来体、俯冲刮削的构造岩片）;当特征相似时,可能指示了相同微陆块的裂解或破坏或者不同的微陆块共同经历了相似的前寒武纪演化历程。