湘南两个内生金属成矿系列的铅锌矿床

湖南省南部地区,岩浆活动频繁,铅锌、钨锡等矿产丰富。前人将该区与花岗岩类有关的铅锌矿床,如水口山、黄沙坪、东坡等统称为岩浆气成热液矿床。近年来,根据野外地质调查和室内研究,初步认为湘南存在两类不同成因的花岗岩类,形成与之有关的两个各具特征的铅锌矿床成矿系列。一、两类不同成因的花岗岩类湘南(北纬26°40′以南)花岗岩类岩石广布,已知有九十九个岩体(群),形成时代自古生代延续至中生代,具有多旋回、多期次的特征。其中,侏罗—白垩纪形成的两类不     

南海海绵Haliclona sp.的化学成分研究

采用硅胶、凝胶等色谱分离方法进行分离纯化,采用理化常数及波谱学方法鉴定结构,研究了南海海绵Haliclona sp.的化学成分.结果从南海海绵Haliclona sp.中分离得到9个化合物,经鉴定分别为:正十六烷基甘油醚(Cetyl ethers of glycerol,1)、正十二烷酸(Dodecanoic acid,2)、2'-脱氧腺苷(2'-deoxyadenosin,3)、尿苷(Uridine,4)、2'-脱氧尿苷(2'-deoxyuridine,5)、2'-脱氧胸苷(2'-deoxythymidine,6)、a-乙基葡萄糖苷(a-ethyl glucoside,7)、对羟基苯乙胺(Tyramine,8)、异戊胺(Isopentylamine,9).化合物4、5、7和9为首次从该属中分离得到.     

Preparation and study on performance of submicron nickel powder for multilayer chip positive temperature coefficient resistance

Base metal nickel is often used as the inner electrode in multilayer chip positive temperature coefficient resistance (PTCR). The fine grain of ceramic powders and base metal nickel are necessary. This paper uses reducing hydrazine to gain submicron nickel powder whose diameter was 200--300 nm through adjusting the consumption of nucleating agent PVP properly. The submicron nickel powder could disperse well and was fit for co---fired of multilayer chip PTCR. It analyes the submicron nickel powder through x-ray Diffraction (XRD) and calculates the diameter of nickel by PDF cards. Using XRD analyses it obtains several conclusions: If the molar ratio of hydrazine hydrate and nickel sulfate is kept to be a constant, when enlarging the molar ratio of NaOH/Ni²⁺, the diameter of nickel powder would become smaller. When the temperature in the experiment raises to 70--80℃, nickel powder becomes smaller too. And if the molar ratio of NaOH/Ni²⁺ is 4, when molar ratio of (C₂H₅O)₂/Ni²⁺ increases, the diameter of nickel would reduce. Results from viewing the powders by optical microscope should be the fact that the electrode made by submicron nickel powder has a better formation and compactness. Furthermore, the sheet resistance testing shows that the electrode made by submicron nickel is smaller than that made by micron nickel.