| 四溴双酚A的合成工艺改进 |
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| 引用本文： | 陈建福.四溴双酚A的合成工艺改进[J].盐湖研究,2011,19(4):49-52. |
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| 作者姓名： | 陈建福 |
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| 作者单位： | 漳州职业技术学院,食品与生物工程系,福建漳州363000 |
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| 基金项目： | 漳州职业技术学院科技计划项目(ZZY1111) |
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| 摘 要： | 以乙腈为溶剂,在H2O2存在下,以双酚A、溴为原料制备了四溴双酚A,讨论了加料方式、搅拌速率、n(Br2)/nBPA、反应温度、氧化剂的滴加速度等工艺条件对制取四溴双酚A产率的影响。在选定的实验条件下制取四溴双酚A的产率可达95.2%。
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| 关 键 词： | 双酚A 乙腈 四溴双酚A 溴素 |
Improvement of the Synthetic Process of Tetrabromobisphenol A |
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| CHEN Jisn-fu.Improvement of the Synthetic Process of Tetrabromobisphenol A[J].Journal of Salt Lake Research,2011,19(4):49-52. |
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| Authors: | CHEN Jisn-fu |
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| Institution: | CHEN Jian-fu(Zhangzhou Institute of Technology,Department of Food and Biology Engineering,Zhangzhou,363000,China) |
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| Abstract: | The tetrabromobisphenol A was synthesized with acetonitrile as organic solvent from bisphenol-A,bromine and hydrogen peroxide.The influence on the production of bisphenol A was discussed by the way of feeding,stirring speed,the ratio of n(Br2)/n(BPA),temperature,the rate of oxidant.The production rate of bisphenol A can be up to 95.2% under given laboratory conditions. |
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| Keywords: | Bisphenol-A Acetonitrile Tetrabromobisphenol A Bromine |
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