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ICP-AES法测定高浓度钙和锶
引用本文:毕玉敬,李海军,赵静,宋彭生,孙柏.ICP-AES法测定高浓度钙和锶[J].盐湖研究,2011,19(4):34-37,52.
作者姓名:毕玉敬  李海军  赵静  宋彭生  孙柏
作者单位:1. 中国科学院青海盐湖研究所,青海西宁810008;中国科学院研究生院,北京100039
2. 中国科学院青海盐湖研究所,青海西宁,810008
基金项目:国家自然科学基金项目(20773152); 青海省科技创新能力促进计划项目(2009-Z-725)资助
摘    要:应用ICP-AES法测定高浓度Ca、Sr混合溶液,选择了合适的分析谱线。在较高浓度时,混合溶液中Ca、Sr之间无显著影响,配制样品及标准时可忽略两者之间的相互影响。测定时酸效应较明显。当待测样品与标准均采用水配制,待测样品总盐浓度在0.65%以内时,测定结果与标准浓度相对误差小于1%。

关 键 词:ICP-AES    

Determination of Calcium and Strontium at High Concentration by ICP-AES
BI Yu-jing,LI Hai-jun,ZHAO Jing,SONG Peng-sheng,SUN Bai.Determination of Calcium and Strontium at High Concentration by ICP-AES[J].Journal of Salt Lake Research,2011,19(4):34-37,52.
Authors:BI Yu-jing  LI Hai-jun  ZHAO Jing  SONG Peng-sheng  SUN Bai
Institution:BI Yu-jing1,2,LI Hai-jun1,ZHAO Jing1,SONG Peng-sheng1,SUN Bai1(1.Qinghai Institute of Salt Lakes,Chinese Academy of Sciences,Xining,810008,China,2.Graduate University of the Chinese Academy of Sciences,Beijing,100039,China)
Abstract:The mixed solution that contained high concentration of calcium and strontium was determined by ICP-AES.The applicable analytical lines were chosen.The interaction between calcium and strontium is not serious in mixed solution at high concentration.The interaction can be neglected when preparing standard and samples.The acid effect is obvious.The relative error can be controlled within 1% when acidity of determined sample corresponds with standard sample and the salt concentration is less than 0.65%.
Keywords:ICP-AES  Calcium  Strontium  
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