无火焰原子吸收法测定化探样中痕量银和镉 |
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引用本文: | 李蓉华,高建国. 无火焰原子吸收法测定化探样中痕量银和镉[J]. 岩石矿物学杂志, 1982, 1(4): 60-63 |
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作者姓名: | 李蓉华 高建国 |
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作者单位: | 地质部岩矿测试技术研究所(李蓉华),地质部岩矿测试技术研究所(高建国) |
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摘 要: | 化探样中的痕量银和镉(0.0xppm)不经分离直接用无火焰原子吸收法测定银和镉是困难的。宫本益夫曾用dowex 1×8阴离子树脂分离和富集电解铜中的银;辽宁地质局中心实验室曾用717阴离子树脂分离和富集化探样中的镉,F.Bea.Barredo和c.Polo polo曾用dowex1×8阴离子树
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The Simultaneous Determination of Silver and Cadmium in Geochemical reference Samples by Flameless Atomic Absorption Spectrometry |
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Abstract: | A method for the determination of Ag and Cd at ppb levels in gecchmic:el refernce samples by flameless atomic absorption spectrometry after separati..n with an anion-exchange resin was described The samples are digested with aqua regia. The resultant solutions of O.6N hydrochloric acid were passed through a column of 717 anion exchange resin, and eluted quantitatively with 30 ml 1.5N nitric acid. The amounts of Ag and Cd in the eluate were determined by flameless absorption spectrometry. |
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