U-Pb zircon and Rb-Sr whole-rock dating of low-grade metasediments example: Montagne Noire (Southern France)

Three detrital, Proterozoic zircon suites extracted from siltstones progressively metamorphosed between chlorite- and staurolite-grade independently date the major Caledonian metamorphism within the gneiss dome of the Montagne Noire (Southern France). From this, the following conclusions concerning U-Pb systematics of zircons in low-, medium- and highgrade metamorphic rocks can be drawn:

1. Temperatures of at most 350–400 °C are sufficient to open U-Pb systems of metamict zircons or domains within zircons.
2. The observed open U-Pb system behaviour during metamorphism of the host rocks was found to be due to a low-temperature recrystallisation of highly radiation damaged zircon lattices, probably enhanced by high concentrations of fluid phases in the dehydrating rock volumes.
3. Recrystallisation of metamict zircons under low temperatures causes maximum U-Pb ages for the thermal climax of metamorphism of medium-and high-grade metamorphic rocks, as annealing and accompaning closing of U-Pb systems took place before the maximum temperatures of metamorphism were reached.
4. Low-temperature recrystallisation of old — generally Proterozoic—zircons can readily help to explain the fact that the numerous zircon suites from ancient shield areas yield “lower intercept ages” which are not correlated to any known geological event. Thus, either a weak thermal pulse, not necessarily registered by the mineral assemblage of the host rock, and/or elevated temperatures during burial in the crust might supply enough energy for a structural reordering and simultaneous lead loss of at least the most disordered lattice domains.

In contrast to the U-Pb zircon method, no unambiguous dating of the Caledonian main metamorphism was possible using the Rb-Sr whole-rock technique for phyllites and mica schists sampled in the same metamorphic profile from which the zircon samples were taken. The scatter of data points can best be explained by their rotation around a probable Caledonian isochron. This rotation very probably took place during the later Hercynian orogeny, not significantly affecting the slope of the least square regression line through the scattered data points.