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Study of intergranular films and interstitial phases in geomaterials using high temperature centrifuge and ultrasonic method at high pressure
Institution:1. National Research Centre, Ceramics Dept., El-Bohous Str., 12622 Cairo, Egypt;2. Zagazig Uni., Faculty of Engineering, Materials Engineering Dept., 44519 Zagazig, Egypt;1. Facultad de Ingeniería Mecánica y Eléctrica, UANL, Av. Universidad S/N., Ciudad Universitaria, San Nicolás de los Garza, N.L. C.P. 66451, Mexico;2. Centro de Innovación, Investigación y Desarrollo en Ingeniería y Tecnología, UANL, Km. 10 de la Nueva Autopista al Aeropuerto Internacional de Monterrey, Apodaca 66600, Mexico;3. Gertec Tecnología y Formulación de Vidrio, Compañía Vidriera, Magallanes # 517, Monterrey, N.L. C.P. 64550, Mexico;4. Valuatec Servicios Técnicos, Magallanes # 517, Monterrey, N.L. C.P. 64550, Mexico
Abstract:Water fluids in the Earth's crust may initiate a number of mineral reactions resulting in different microstructure changes, which may appear in the form of intergranular melt films and interstitial phases. Therefore, they have an essential influence on elastic wave velocities of rocks (for example, sandstone, amphibolite, basalt). The aim of the experiment was to determine the conditions of the silicate liquid and others interstitial phases distribution in the rock intergranular space.The results obtained using the ultrasonic method at temperature up to 950 °C and under fluid pressure of 300 MPa revealed that the formation of intergranular melt films and interstitial phases network depend on chemical composition of fluids. The experiments with use of a high-temperature centrifuge at temperature 1400 °C showed that the amount of melt films, higher than 6 %, is sufficient to form a system of interconnected intergranular channels. These studies can be contributed to the petrophysical and geochemical interpretation of geophysical measurements.
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