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RG—1型单波长冷原子吸收热释测汞仪
引用本文:卫敬生 李荣春. RG—1型单波长冷原子吸收热释测汞仪[J]. 岩矿测试, 1999, 18(3): 205-210
作者姓名:卫敬生 李荣春
作者单位:浙江宁波甬利公司,宁波,315040
摘    要:介绍了采用“化学选择表面吸附”方法在气路中使用和NaOH及Na2O2排除固样品热解产生的干扰气体的RG-1型单波长冷原子收测汞仪,仪器抗干扰能力≥3A,允许直接热解纯硫20mg及可能热解释放大量干扰气体的单矿物50mg。主要技术眼过了双波长的塞曼原理测汞仪。

关 键 词:单波长 原子吸收热释 抗干扰 测汞仪
修稿时间:1998-12-15

RG-1 Monowavelength Cold-Vapor Atomic Absorption Thermal Release Mercury Analyzer
WEI Jing-sheng,LI Rong-chun,YANG Zhu-xi. RG-1 Monowavelength Cold-Vapor Atomic Absorption Thermal Release Mercury Analyzer[J]. Rock and Mineral Analysis, 1999, 18(3): 205-210
Authors:WEI Jing-sheng  LI Rong-chun  YANG Zhu-xi
Abstract:A monowavelength coldvapor atomic absorption thermal release mercury analyzer is developed. NaOH and Na-2O-2 are used in the gas route to remove the interfering gases produced from the solid samples during thermal release step. The main technical features of this instrument are superior to the double wavelength mercury analyzer based on Zeeman principle. Combined with new computer system, the analytical functions of this instrument are extended with more convenience and flexibility. The stability of baseline is improved remarkably. Peak value, integral concentration and the statistic data for various technical specifications can be given directly. It also provides the function of phase spectrum analysis through highspeed thermal release. The detection limit of the instrument for Hg is 0.004 ng and as low as 6 ng/g of Hg in samples can be determined by this method. The precision of determination is <5% RSD(n=11) and the linear range is 3300 ng/g for Hg. The method has been applied to the determination of mercury in the national standard reference materials. The results are in agreement with the certified values.==
Keywords:monowavelength  atomic absorption  thermal release  antiinterference  mercury analyzer  
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