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离子色谱法测定生活饮用水中溴酸盐的不确定度评定
引用本文:李清彩,陈娟,毛秀丽,赵庆令.离子色谱法测定生活饮用水中溴酸盐的不确定度评定[J].山东国土资源,2018,34(12).
作者姓名:李清彩  陈娟  毛秀丽  赵庆令
作者单位:山东省鲁南地质工程勘察院,山东省鲁南地质工程勘察院,山东省鲁南地质工程勘察院,山东省鲁南地质工程勘察院
摘    要:采用离子色谱法对生活饮用水样品中的溴酸盐进行测定,并对测量结果进行不确定度评定。剖析了影响测量不确定度的主要因素,对储备标准溶液、稀释标准溶液、拟合标准曲线、重复性测量、仪器稳定性等影响不确定度的因素进行评定,并计算出扩展不确定度,使结果的表达更加客观,为实验室质量控制提供参考依据。

关 键 词:离子色谱  不确定度  溴酸盐  生活饮用水

Uncertainty Evaluation for Ion Chromatography Determination of Bromate in Drinking Water
LI Qingcai,CHEN Juan,MAO Xiuli and ZHAO Qingling.Uncertainty Evaluation for Ion Chromatography Determination of Bromate in Drinking Water[J].Land and Resources in SHANDONG Province,2018,34(12).
Authors:LI Qingcai  CHEN Juan  MAO Xiuli and ZHAO Qingling
Abstract:The determination of bromate in drinking water samples has been carried out by ion chromatography and the uncertainty of the measurement results has been evaluated. The main sources that affect the uncertainty of measurement have beem analyzed. The factors that affect the uncertainty of the standard reserve solution, such as the dilution of standard solution, the standard curve fitting, the sample repeatability measurement and the instrument have been analyzed. The expansion inaccuracy has been calculated. It makes the result more objective and true, and provide references for laboratory quality control.
Keywords:Ion Chromatography  uncertainty  bromate  drinking water
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