| ID-ICP-MS测定高纯石英中微量铀的方法研究 |
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| 引用本文： | 谭靖, 姚海云, 侯艳先, 郭冬发, 崔建勇, 武朝晖, 张彦辉. ID-ICP-MS测定高纯石英中微量铀的方法研究[J]. 地球学报, 2003, (6): 627-630. doi: 10.3321/j.issn:1006-3021.2003.06.028 |
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| 作者姓名： | 谭靖 姚海云 侯艳先 郭冬发 崔建勇 武朝晖 张彦辉 |
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| 作者单位： | 核工业北京地质研究院分析测试中心，北京100029;东华理工学院应用化学系，江西抚州344000;核工业北京地质研究院分析测试中心，北京100029;核工业北京地质研究院分析测试中心，北京100029;核工业北京地质研究院分析测试中心，北京100029;核工业北京地质研究院分析测试中心，北京100029;核工业北京地质研究院分析测试中心，北京100029 |
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| 摘 要： | 采用一种脉冲增压微色谱柱,阴离子交换树脂,分离富集高纯石英中的微量铀,分离效果好,本底低.样品处理用低温密封闷罐酸溶.同位素稀释电感耦合等离子体质谱(ID-ICP-MS)测定高纯石英中的微量铀,方法检出限低:0.1 ng/g(3σ,n=10),分析速度快,是理想的测定微量铀的方法.
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| 关 键 词： | 同位素稀释 电感耦合等离子体质谱法 微量铀 高纯石英 |
Determination of Trace Uranium in High Purity Quartz by Means of ID-ICP-MS |
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| Determination of Trace Uranium in High Purity Quartz by Means of ID-ICP-MS[J]. Acta Geoscientica Sinica, 2003, (6): 627-630. doi: 10.3321/j.issn:1006-3021.2003.06.028 |
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| Authors: | TAN Jing YAO Hai-yun HOU Yan-xian GUO Dong-f CUI Jian-yong WU Chao-hui ZHANG Yan-hui |
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| Affiliation: | Center of Analysis, Beijing Research Institute of Uranium Geology, Beijing, 100029;Department of Applied Chemistry, East China Institute of Technology, Fuzhou, Jiangxi, 344000;Center of Analysis, Beijing Research Institute of Uranium Geology, Beijing, 100029;Center of Analysis, Beijing Research Institute of Uranium Geology, Beijing, 100029;Center of Analysis, Beijing Research Institute of Uranium Geology, Beijing, 100029;Center of Analysis, Beijing Research Institute of Uranium Geology, Beijing, 100029;Center of Analysis, Beijing Research Institute of Uranium Geology, Beijing, 100029 |
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| Abstract: | A method called pulse-pressurized capillary column is used for preconcentration and separation of uranium, followed by determination of trace uranium in high purity quartz by ID-ICP-MS. Acid is used to dissolve the sample in an airproof vessel at a low temperature. The result of GSD-10 indicates that good precision and veracity can be achieved, and that the limit of determination is low (0.1 ng/g).Therefore,ID-ICP-MS is a good technique for determining trace element. |
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| Keywords: | isotope dilution (ID) inductively coupled plasma mass spectrometry uranium high purity quartz |
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