Rapid analysis of Florida phosphates by energy-dispersive X-ray fluorescence |
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Authors: | HS Chung WF Espenscheid |
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Institution: | Central Research Division Laboratory, Mobil Research and Development Corporation, Princeton, N.J. 08540 U.S.A. |
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Abstract: | A rapid X-ray fluorescence technique has been developed to determine the BPL (Ca3(PO4)2 or Bone Phosphate of Lime) content of various streams in Florida phosphate beneficiation and in supporting laboratory flotation experiments. The method, which requires simple sample preparation, a 100-sec counting, and has an accuracy of better than 2% BPL (0.4% P), employs an Fe55 radioactive source and a room temperature detector to analyze for calcium. The BPL values, which can not be obtained readily and directly because of the weak fluorescence of phosphorus, are instead derived from a close correlation found to exist between the phosphorus and calcium concentrations. |
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