DETERMINATION OF RARE EARTH ELEMENTS IN SIXTEEN SILICATE REFERENCE SAMPLES BY ICP-MS AFTER TM ADDITION AND ION EXCHANGE SEPARATION |
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Authors: | JA BARRAT F KELLER J AMOSSÉ RN TAYLOR RW NESBITT T HIRATA |
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Institution: | UniversitéJoseph Fourier, UFR de Géologie, Laboratoire de Géodynamique des Chaînes Alpines (UPRES associéau CNRS n°5025), 15 rue Maurice Gignoux, 38031 Grenoble Cedex, France;Southampton Oceanography Center, European Way, Southampton, SO14 37H, U.K.;Tokyo Institute of Technology, Dept, of Earth and Planetary Sciences, O-Okayama, 2 12 1, Meguro, Tokyo 152, Japan |
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Abstract: | This study reports the results of thirteen rare earth elements (REE) in sixteen geochemical reference samples. The analytical procedure involved dissolution of a whole rock or mineral separate, spiking with Tm, and separation of the REE using a simple ion-exchange chromatography procedure. The resulting REE solutions were analysed by ICP-MS. The results are compared with literature values. The agreement between our data and recommended or ID-TIMS values is very favorable. The precision of the technique is better than 5% (2) for all the REE. |
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