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Determination of Total Sulfur in Thirty One Geochemical Reference Materials Using an Inductively Coupled Plasma-Atomic Emission Spectrometer Fitted with a Semiconductor Photodiode Detector
Authors:Takashi Okai  Shigeru Terashima  Noboru Imai
Institution:Geological Survey of Japan, 1-1-3 Higashi, Tsukuba, Ibaraki 305-8567, Japan. e-mail:
Abstract:The total sulfur contents of thirty one geochemical reference materials were determined using an inductively coupled plasma-atomic emission spectrometer fitted with a semiconductor photodiode detector. Most samples were decomposed using an HF-aqua regia digestion. However, a few were incompletely decomposed by simple acid digestion, and these were decomposed by a fusion method. The agreement between the analytical results from this work and published data is generally good.
Keywords:sulfur  ICP-AES  reference materials  sample digestion
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