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| 生物样品中硒形态分析前处理技术 | |
| 引用本文： | 张绿茵,余晓平,郭亚飞,邓天龙.生物样品中硒形态分析前处理技术[J].岩矿测试,2012,31(3):407-412. |
| 作者姓名： | 张绿茵 余晓平 郭亚飞 邓天龙 |
| 作者单位： | 1. 天津科技大学,天津市海洋资源与化学重点实验室,天津300457 2. 天津科技大学,天津市海洋资源与化学重点实验室,天津300457;中国科学院青海盐湖研究所盐湖资源与化学重点实验室,青海西宁810008 3. 天津科技大学,天津市海洋资源与化学重点实验室,天津300457;成都理工大学材料与化学化工学院,四川成都610059 4. 天津科技大学,天津市海洋资源与化学重点实验室,天津300457;中国科学院青海盐湖研究所盐湖资源与化学重点实验室,青海西宁810008;成都理工大学材料与化学化工学院,四川成都610059 |
| 基金项目： | 国家自然科学基金重点项目(2083600); 天津市科技支撑重点项目(11ZCKFGX2800); 天津市特聘教授人才引进启动基金(20100405); 教育部博士学科点科研专项(20101208110003) |
| 摘 要： | 样品前处理过程在硒形态分析中至关重要。文章对生物样品中硒形态分析的前处理方法,包括液相萃取、微波辅助萃取、固相微萃取、液相微萃取等及其应用进行归纳总结,指出了痕量、超痕量硒形态分析前处理技术的未来发展方向主要集中在满足简单、快速和环境友好的自动化处理,并着重于样品前处理的各种萃取技术在线耦合以及与硒形态分析检测器联用技术。 |
| 关 键 词： | 硒 形态分析 前处理技术 生物样品 |
| 收稿时间： | 2011/11/1 0:00:00 |
| 修稿时间： | 2012/4/20 0:00:00 |
Pretreatment Techniques for Selenium Speciation Analysis in Biosamples |
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| ZHANG Lü-yin , YU Xiao-ping , GUO Ya-fei , DENG Tian-long.Pretreatment Techniques for Selenium Speciation Analysis in Biosamples[J].Rock and Mineral Analysis,2012,31(3):407-412. | |
| Authors: | ZHANG Lü-yin YU Xiao-ping GUO Ya-fei DENG Tian-long |
| Institution: | Tianjin Key Laboratory of Marine Resources and Chemistry, Tianjin University of Science and Technology, Tianjin 300457, China;Tianjin Key Laboratory of Marine Resources and Chemistry, Tianjin University of Science and Technology, Tianjin 300457, China;Key Laboratory of Salt Lakes Resources and Chemistry, Qinghai Institute of Salt Lakes, Chinese Academy of Sciences, Xining 810008, China;Tianjin Key Laboratory of Marine Resources and Chemistry, Tianjin University of Science and Technology, Tianjin 300457, China;College of Materials and Chemistry & Chemical Engineering, Chengdu University of Technology, Chengdu 610059, China;Tianjin Key Laboratory of Marine Resources and Chemistry, Tianjin University of Science and Technology, Tianjin 300457, China;Key Laboratory of Salt Lakes Resources and Chemistry, Qinghai Institute of Salt Lakes, Chinese Academy of Sciences, Xining 810008, China;College of Materials and Chemistry & Chemical Engineering, Chengdu University of Technology, Chengdu 610059, China |
| Abstract: | Pretreatment processes play an important role in selenium speciation analysis. Selenium species extractive methods including liquid extraction, microwave aided extraction, solid-phase microextraction and liquid-phase microextraction and the pretreatment methods for biosamples are summarized in this paper. The new trends of pretreatment for trace and ultra-trace of selenium species in the future should focus on satisfying the automatic requirement with simple, rapid and eco-friendly characteristics, and be capable of integrating the different extraction techniques or new pretreatment methods of direct and on-line coupling with specific selenium species detection. |
| Keywords: | selenium speciation analysis pretreatment techniques biosamples |
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