| 氢化物发生-原子荧光光谱法测定铜矿石中的砷锑铋 |
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| 引用本文： | 马玲,查立新,冯玲玲,刘文长. 氢化物发生-原子荧光光谱法测定铜矿石中的砷锑铋[J]. 岩矿测试, 2009, 28(5): 497-498 |
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| 作者姓名： | 马玲 查立新 冯玲玲 刘文长 |
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| 作者单位： | 安徽省地质实验研究所,安徽合肥,230001 |
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| 摘 要： | 样品经王水溶矿分解,在氨水存在下,以Fe3+作共沉淀剂分离铜后,用氢化物发生-原子荧光光谱法测定铜矿石中的砷、锑、铋。方法检出限为砷0.19μg/g、锑0.052μg/g、铋0.049μg/g;精密度(RSD,n=10)为砷5.87%、锑7.58%、铋2.42%。
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| 关 键 词： | 氢化物发生-原子荧光光谱法 砷 锑 铋 铜矿石 |
| 收稿时间： | 2008-10-29 |
| 修稿时间： | 2009-02-06 |
Determination of Arsenic, Antimony and Bismuth in Copper Ores by Hydride Generation-Atomic Fluorescence Spectrometry |
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| MA Ling,ZHA Li xin,FENG Ling ling and LIU Wen zhang. Determination of Arsenic, Antimony and Bismuth in Copper Ores by Hydride Generation-Atomic Fluorescence Spectrometry[J]. Rock and Mineral Analysis, 2009, 28(5): 497-498 |
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| Authors: | MA Ling ZHA Li xin FENG Ling ling LIU Wen zhang |
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| Affiliation: | Anhui Provincial Geological Experiment Institute;Anhui Provincial Geological Experiment Institute;Anhui Provincial Geological Experiment Institute;Anhui Provincial Geological Experiment Institute |
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| Abstract: | A method for the determination of arsenic,antimony and bismuth in copper ores by hydride generation-atomic fluorescence spectrometry was developed.The sample was dissolved by aqua regia and copper was then effectively separated by using Fe3+ as coprecipitation agent in ammonium hydroxide solution.Arsenic,antimony and bismuth in the sample solution were determined by hydride generation-atomic fluorescence spectrometry.The detection limits of the method are 0.19 μg/g for arsenic,0.052 μg/g for antimony and 0.049 μg/g for bismuth.The precisions(RSD,n=10) of the method are 5.87% for arsenic,7.58% for antimony and 2.42% for bismuth. |
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| Keywords: | hydride generation-atomic fluorescence spectrometry arsenic antimony bismuth copper ore |
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