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GDX-502树脂富集高效液相色谱法测定地表水中酚类化合物 总被引:2,自引:2,他引:2
采用自制GDX-502固相萃取小柱萃取水中苯酚、对硝基酚、间甲酚、2,4-二氯酚、2,4,6-三氯酚、五氯酚等6种酚类化合物,以乙腈作为洗脱剂,选择280nm和290nm双波长紫外高效液相色谱进行检测。结果表明,方法检出限为0.01-0.05mg/L,IL水的平均加标回收率为82.5%-95.0%,精密度(RSD,n=7)为3.6%-9.2%。方法用于实际地表水中痕量酚类化合物的检测,操作简单,有机溶剂用量少,分析效率高;萃取小柱可多次重复使用,分析成本低。 相似文献
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ZY-102C星数据在矿山遥感监测中的应用研究与分析 总被引:1,自引:0,他引:1
利用资源一号(ZY-1)02C卫星(以下简称02C星)全色高分辨率相机(HR)和多光谱相机(MUX)数据,以河北承德多金属矿区和江西寻乌稀土矿区为实验区,开展了1∶5万矿山遥感监测应用研究;分析了应用过程中存在的问题,提出了解决方案和建议,对02C星数据在矿山遥感监测中的规模化应用起到了示范效果。研究结果表明:在数据处理流程上,对空间分辨率为2.36 m的02C星全色HR1与HR2数据需先进行正射纠正再拼接,对空间分辨率为10 m的多光谱数据MUX可采用假彩色合成方法进行模拟真彩色合成;在矿山地物识别上,与SPOT5图像比较,02C星图像可更好地反映出开采面、开采点、中转场和矿山建筑等矿山地物类型,不足之处是纹理信息较平滑、矿山地物的边界相对模糊,因而增加了室内解译的难度;在经济效益上,02C星数据的性价比优势明显。因此,尽管02C星数据处理和解译工作量较大,但其能满足1∶5万矿山遥感监测要求,总体经济效益显著。 相似文献
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Results from a spectral study of the quasar Kaz 102 are presented. It is shown that its spectrum varies as a whole; that is,
the parameters of both the lines and the continuum change. Based on a comparison of results presented previously and in this
paper, it is concluded that over a time of approximately 27.5 years the equivalent widths and relative intensities of the
lines have increased, while their half widths have decreased. The spectral composition of Kaz 102 has also changed: new lines,
HeII λ4686, [OIII] λ4363, and others, appear in spectra of 2000 and 2001 which were not observed in spectra taken in 1973.
The electron density, and the mass and effective radius of the gas component are determined to be 2·107 cm-3, 2·104 M⊙, and 0.2 pc.
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Translated from Astrofizika, Vol. 50, No. 2, pp. 161–170 (May 2007). 相似文献
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川藏公路是西藏连结中国西南地区的主要通道。1991年6月发生的川藏公路102滑坡(古滑坡复活)严重影响着公路的畅通。2002年采用原路边坡锚拉桩板护坡方案进行整治,暂时解决了交通阻断问题,但经6年多的使用证明,整治效果不佳。从滑坡的成因、滑坡物质构成和影响因素分析,102滑坡仍然是一个不稳定的滑坡。经论证,隧道方案可以克服滑坡对道路的危害和威胁问题,达到畅通的目的。虽然该方案一次性投资较大,但建成使用后,由道路畅通带来的社会效益将是巨大的。因此,无论是从根治滑坡对道路的影响角度还是从社会经济效益角度,隧道方案都是一个工程价值较高的方案。 相似文献
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We report results of our optical photometric observations of ten gamma-ray loud blazers, namely: 0219+428 (3C66A), PKS 0420-014 (OA 129), S5 0716+714, 0754+100 (OI 090.4), 0827+243 (OJ248), 1652+398 (Mrk 501), 2200+420 (BL Lacertae), 2230+114 (CTA 102), 2251+158 (3C 454.3) and 2344+514. The observations were carried out in September-October, 2000 using the 70 cm optical telescope at Abstumani Observatory, Georgia. We found intra-day variations in 0420-014, S5 0716+714, BL Lacertae and CTA 102. A variation of 0.3 magnitude over a time scale of about 3 hours was observed in the R passband in BL Lacertae on JD 2451827. We did not detect any variation in 3C 66A, Mrk 501, or 3C 454.3 during our observations. Nor did we detect any clear evidence of variation in 1ES 2344+514 during our two weeks' observing run of the TeV gamma-ray source. 相似文献
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Trare amounts of benzene hydrocarbons obtained in Jiaozhou Bay (Qindao) were enriched bysorption on a GDX-102 column and eluted by carbon disulfide. The eluted was concenttaled and then de-temened by capillary column gas cbornatognphy.The contents of virious kinds of benzene hydrocarbons in Jiaozhou Bay coastal water were benzene(22.3-141.6)× 10~(-9)g/L, toluate (15.2-94.0) × 10~(-9) g/L, ethyl benzene(11.8-85.1)×10~(-9) g/L, p -xylene(15.2-78.5) ×10(-9) g/L, m-xylene (10.9-79.4) ×10(-9) g/L, o -xylene (12.4-80.1) x ×10(-9)g/L; iso-propyl(8.4- 73.1) x ×10(-9)g/L, n -propyl (6.9-76.4) ×10(-9) g/L, 1, 3, 5-trimethylbenzene (10.9- 35.9)×10(-9) g/L, 1,2, 4-trimethybenzene (10.0- 38.0)×10(-9) g/L, n - butydriare (8. 1 - 34.6) ×10(-9)g/L. The recovery of benzenehydrocarbons was (85.1 -95.6)%. 相似文献
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