低凝固温度琼脂糖的制备方法研究

以石花菜分级得到的琼脂糖为原料，采用甲基化方法制备低凝固温度琼脂糖。所得到的低凝固温度琼脂糖产品的凝固温度为30．1℃(1.5％浓度)，融化温度为64．8℃(1．5％浓度)，凝胶强度为264g／cm^2(1.0％浓度)，主要质量标准与Sigma公司的低凝固温度琼脂糖产品接近，符合低凝固温度琼脂糖产品的质量要求。     

辰砂摇红

七月流火,辰砂摇红。生命的炽热、浓烈、耀眼在这一刻得到全部的绽放,凝固成这固执的红色,像88年前的7月,共产党先贤为国为民所撒的热血,一种固执的信仰。晋葛洪《抱朴子·黄白》中说:"朱砂为金,服之升仙者上士也。"朱砂即辰砂,玄学道士赋予朱砂以无比强     

酸性火山岩早成岩期岩矿特征及其地质意义 ——以新西兰北岛Taupo火山带Waiotapu地热区火山喷口堆积物为例

新西兰北岛Waiotapu地热区位于Taupo火山带中部,以发育众多的第四纪酸性火山岩而闻名。通过 X衍射、电子探针、扫描电镜、激光拉曼等方法对区内一处于活动间歇期的小型火山口堆积物岩矿特征及特殊结构进行研究。结果表明,火山口堆积物可分为3类:1)球粒流纹岩,矿物组成为:α方石英-PO鳞石英—正长石、奥长石、紫苏辉石—钛铁矿(钛磁铁矿);2)流纹质晶屑熔结凝灰岩,矿物组成为:奥长石晶屑、塑性玻屑;3)硫磺土,矿物组成为:单质硫、长英质细粒岩屑。结合前人实验矿物学结论后认为,球粒流纹岩中的球粒体为富火山玻璃的流纹岩喷出堆积后在热水作用下脱玻化形成的,是酸性火山岩早成岩期表生蚀变阶段的标志;而流纹质熔结凝灰岩则为岩浆喷溢出地表后,在塑性流动中冷凝结晶形成的,是酸性火山岩早成岩期冷凝固结阶段的标志。在此基础上,提出了Waiotapu地热区酸性火山岩的表生蚀变模式,为酸性火山岩冷凝固结—表生蚀变阶段的岩矿特征及蚀变作用研究提供现代对比实例。     

有关地核的新见解

《自然》杂志最近报道了一个新的地球内核深部观察结果。布里斯托尔大学研究小组观测到令人感兴趣的“纹理”附在凝固的铁质体上,他们认为这可能是左旋的液体铁在地核外层凝固时的反映。     

多相复合陶瓷的直接凝固注模成型

低成本、高可靠性成型工艺是多相复合陶瓷产业化的关键。直接凝固注模成型（ＤＣＣ）是一种全新概念的净尺寸陶瓷成型技术。该文报道了ＤＣＣ成型的基本原理和工艺,讨论了将ＤＣＣ成型工艺应用于多相复合陶瓷必须解决的关键问题。提出了多相复合陶瓷胶态注模原位凝固成型新工艺。     

桩底后压浆浆液扩散问题研究

采用钻探取样方法,对渗透性地层中桩底后注浆浆液扩散及固结状态进行检验。实物样品表明,在相对均匀的地层中,浆液扩散呈现出向下、向侧、向上不同的渗透能力：向下最强,向侧次之,向上最弱。在粗细交互地层中,颗粒越粗,渗透更好,扩散更远;水泥浆的含量更高。在同一地层中,距注浆出口越近,水泥浆含量越高。取样结果还表明：在桩底,压力、温度不同于地表,特别是有丰富地下水的环境下,水泥浆的凝结固化时间延迟非常显著。     

Investigation of hydrolysis and coagulation mechanism of poly-iron coagulant

Chemical coagulation is very important in water treatment, in which coagulant is an essential part. Pre-polymerized Al^3＋ and Fe^3＋ products have been used in practice, continuously spread for many years. However, iron-based coagulant has become the focus of studies due to cumulative biologic toxicity of residual Al in treated water. Polyferric sulfate （PFS） and poly-silicic-ferric sulfate （PSF） are all pre-polymerized polymers of Fe^3＋ salts. The hydrolysis process and species distribution of Fe^3＋ ions have been investigated extensively by many chemists and water-treatment specialists. Generally, the coagulation mechanism of conventional or pre-polymerized coagulants was often studied through jar-test, absorption experiment, microstructure observation or hydrolysis species indirectly. However, few researches have been done on the hydrolysis process of PSF in detail and on the study of the coagulation mechanism using its hydrolysis species distribution until now. In this work, PSF was prepared using water glass, ferrous sulfate and sodium chlorate by a copolymerization method. The hydrolysis species distribution was theoretically derived from pH variation during hydrolysis process of PSF compared to that of polyferric sulfate （PFS）, and then characteristics [morphology, species size, Zeta potential, spectra of X-ray diffraction and infrared spectra （IR）] and coagulation performances were explored between them. Coagulation mechanism was analyzed according to hydrolysis species distribution, characteristics and coagulation performances. The results showed that PSF gives different species distribution at different pH values and characteristics from those of PFS, leading to different coagulation mechanisms between the two coagulants.     

pH effect on stabilization/solidification of industrial heavy metal sludge

The leaching character and toxicity of the stabilization/solidification （S/S） products of industrial heavy metal sludge were experimentally researched at different pH （1-13）. The results showed that the leaching solutions of cement S/S and lime S/S products were all alkaline; the S/S treatments could fix Pb, Cd, Cu, Zn and Ni in solid; the Cr concentration was obviously high in the leaching solution of S/S products and exceeded the regulation value of ＂Landfill Control Standard for Hazardous Wastes＂ （GB 1858 01）.