A spectrophotometric measurement of soil cation exchange capacity based on cobaltihexamine chloride absorbance

Among numerous methods for cation exchange capacity (CEC) determination for soils and sediments, the cobaltihexamine chloride method is frequently used due to its ability to measure CEC at soil pH. After exchange with Co(NH₃)₆³⁺ ions, CEC is estimated via the measurement of the Co remaining in solution. The modified method proposed allows a more rapid determination of CEC based on the measurement of the absorbance at 472 nm of the cobaltihexamine chloride solution before and after exchange. This method has been applied to various soil's horizons from four sites, selected to cover a wide range of CEC and pH values. The model obtained allows one to calculate CEC from absorbance at 472 nm with 95% confidence intervals. As CEC is of relevant meaning in agronomical and environmental purposes, and more recently in ecotoxicological studies, this modified method can be proposed as a rapid test for CEC evaluation.     

Nature minéralogique et rôle nutritionnel des argiles de sols céréaliers en région subhumide à semi-aride (Tunisie)

The cereal soils of the Northwest of Tunisia derive most of the time, from alluvial deposits or altered remains of carbonated and clayey rocks. Extraction of the clayey fraction permitted to reveal the presence of the following clayey minerals: kaolinite, illite, smectite, chlorite, as well as an illite–smectite interstratified layer, which is present in the deep horizons of the vertisol and in the isohumic soil. The presence of such types of clays shows that the evolution mechanism of soils is weathering of primary minerals inherited from the sedimentary rocks of the Northwest of Tunisia. These clays ensure to soils most of their cationic exchange capacity. Thanks to these clays, which have Ca⁺⁺, Mg⁺⁺ and K⁺ as exchangeable cations, the chemical fertility of these soils is ensured. It may be improved by increasing contents of organic matter, which is naturally few abundant in these soils. To cite this article: H. Ben Hassine, C. R. Geoscience 338 (2006).     

滞回曲线对应力振幅和频率的响应

基于疲劳载荷对应力－应变滞回曲线的影响，作者研究了滞回曲线对应力振幅和频率的影响，获得了载荷超过屈服点后应力振幅增大，滞回曲线趋于稳定，应变硬化效应增强的结果，随着正弦波频率增加岩石的滞回圈频散效应增强，饱和液体加强了这种频散作用，随孔隙液体的粘滞系数增大，滞回曲线的频散效应更强。     

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结合多混沌映射和输出反馈的图像加密算法

提出了一种结合多个Logistic混沌映射和逐段正弦混沌映射的图像加密算法。通过m个Logistic混沌映射的多次迭代,分别产生m个分段正弦混沌映射的初值和参数值,由m个分段正弦混沌映射迭代产生图像加密密钥序列,并引入密文输出反馈机制,对图像像素值逐点进行2轮异或加密。实验表明,该算法使密文对明文和密钥都充分敏感,加密图像像素值具有类随机均匀分布特性,相邻像素具有零相关特性,而且算法具有密钥空间大、加密速度快的优越性。     

二维饱和多孔介质因点汇诱发比奥固结的解析解

给出了有限二维饱和多孔介质因点汇诱发的Biot固结的一个解析解。其中假设多孔介质为均匀各向同性和线弹性,假设孔隙压力场符合第1类边界条件,数学模型采用可压缩多孔介质模型。利用傅里叶和拉普拉斯变换及相应反演获得了双重无穷项级数和形式的精确解。然后特别探讨了定流量点汇诱发的稳态解析解,并用文献现有解析解进行了验证。所提出的解析解适合于验证数值解,并可用于深入分析有限二维多孔介质的流-固耦合行为。     

调频输入正弦锁相环路方程周期解的存在性与稳定性

本文进一步考虑了具有正弦鉴相特性的锁相环路,我们提供了不同于文[2]的锁定参数,且求出周期解的界和渐近稳定域。     

Causes and solutions of overshoot and undershoot and end swing in Hilbert-Huang transform

Introduction Hilbert-Huang transform (HHT) is a great break in processing nonlinear and non-stationary data and can be successfully used in many science domains. There are mainly two parts in this method. The first part is to decompose the original data into several intrinsic mode functions (IMF) with the empirical mode decomposition (EMD). IMF components are derived from the original data directly according to the local characteristics in the data under some rules, so that IMF are poste…     

精确测定地震计传递函数

提出联合阶跃标定与带精确电流测量的正弦波标定来确定地震计传递函数的方法。首先,使用阶跃标定确定地震计等效机械摆的自振周期和阻尼,得到地震计低频特性。随后,使用正弦波标定并引入电流测试技术,测定地震计全频段频率响应,幅频响应更加准确,同时可获得相频响应。最后,构建与地震计传递函数特征一致的结构来描述传递函数,采用最优化方法拟合求取地震计传递函数。该方法具有原理清楚、操作简单、易于实现、结果精确等优点,特别适用于地震计用户测试、地震计传递特性与厂方参数及各地震计间一致性和长期稳定性的验证,结果符合反馈型地震计传递函数特点。     

基于小波包分解和模糊聚类的网格结构损伤诊断方法

本文针对网格结构的特点,利用其在快速正弦扫频激励下的动力响应,基于小波包分解频带能量分析和模糊聚类法,提出了一种适合于网格结构的损伤诊断方法。利用两个传感器损伤信息的联合诊断,有效地解决了使用一个传感器无法检测出对称损伤的难题。利用有限元模拟,应用上述方法对一单层球面网壳结构进行了损伤诊断。结果表明,对网壳杆件较小程度的损伤,子频带能量成分变化敏感,用其构造诊断向量和建立损伤样本库,并进行模糊聚类和目标识别,基本可以正确地识别出网壳杆件的损伤位置和程度。同时该方法测试时间短,使用设备少,有可靠的理论基础,具有一定的工程应用参考价值。