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This study presents two matrix‐matched reference materials developed for petroleum Re‐Os measurements. We present the Re and Os mass fractions and 187Re/188Os and 187Os/188Os values (ratio of the number of atoms of the isotopes) for repeatedly measured aliquots (ca. 120–150 mg test portions) of the NIST Research Material 8505 (RM 8505) crude oil, and its asphaltene and maltene fractions, and ~ 90 g of homogeneous asphaltene powder isolated from this oil. Measurements were performed using the Carius tube‐isotope dilution negative‐thermal ionisation mass spectrometry methodology. The RM 8505 crude oil contains 1.98 ± 0.07 ng g?1 Re and 25.0 ± 1.1 pg g?1 Os, with Re‐Os isotope amount ratios of 452 ± 6 for 187Re/188Os and 1.51 ± 0.01 for 187Os/188Os (n = 20, 95% conf.). The homogeneous asphaltene sample contains 16.52 ± 0.10 ng g?1 Re and 166.0 ± 0.9 pg g?1 total Os, and possesses isotope amount ratios of 574 ± 3 for 187Re/188Os and 1.64 ± 0.01 for 187Os/188Os (n = 24, 95% conf.). The intermediate precision of these data makes the RM 8505 whole oil and the (~ 90 g) homogenised asphaltene appropriate petroleum matrix‐matched reference materials for Re‐Os measurements. The asphaltene fraction of the oil is the main carrier of Re and Os of the RM 8505 whole oil, and caution is suggested in using asphaltene and maltene fractions of a single oil for Re‐Os geochronology. 相似文献
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在Linux实时进程调度算法中,RM算法是一种针对任务周期的长短来确定优先级调度算法,EDF算法是以最后期限的顺序来指定优先级的动态调度算法,这两种算法在LiFlUX内核调度算法中都得到广泛应用.在深入分析以上两种算法优缺点的基础上,提出将两种算法优点合并,根据进程的重要程度和紧急程度来选择确定进程调度的优先级,得到一个新的高效RAD(Rate And Deadline)算法,试验证明新算法RAD的运行效率更高. 相似文献
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Sidonie Révillon Danièle Hureau-Mazaudier 《Geostandards and Geoanalytical Research》2009,33(3):397-413
Total dissolution is a critical step in geochemical analysis. Despite the number of published protocols, this issue still draws attention for sediment samples, which are particularly difficult to dissolve due to the common occurrence and high abundance of refractory phases such as zircon. We present tests of different chemical digestion procedures carried out on reference materials (RM) of stream (JSd-1, JSd-2 and JSd-3) and lake (JLk-1 and LKSD-1) sediments from the Geological Survey of Japan (GSJ) and the Canadian Certified Reference Material Programme (CCRPM). We demonstrate that the fusion technique is not appropriate for our studies as not all elements of interest were recovered and blank levels were too high to permit further Sr and Pb isotopic composition measurements. Similarly, conventional HF+HNO3 dissolution methods were not efficient enough for detrital samples. Our preferred method involved using high pressure Teflon® vessel bombs in association with HClO4 . This protocol ensured a complete dissolution of the powder, as well as a complete recovery of trace elements. Moreover, blank levels were sufficiently low that Sr or Pb isotope compositions could be measured from the same mother solution. We also tested the homogeneity of RM powders by performing tests on various amount of powder. 相似文献
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自20世纪90年代关系营销理论引入我国以来,我国服务业已取得长足发展,但在许多方面依然落后于发达国家。其原因之一是缺乏一种本土化的关系营销模式。有鉴于此,文章提出了适合我国服务业市场特色的关系营销模式———基于资源的“大诚”服务关系营销模式。该模式兼具三方面内容:系统环境内化成为服务企业的内部资源、“大诚”关系营销模式以及服务关系绩效检测指标。 相似文献
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用1995年5月至1999年4月KWBC北半球500 hPa高度场5°×5°客观分析资料,应用谐波分析把等压面高度场沿纬圈作富利叶级数展开,计算逐日25°~80°N每隔5°纬度递增的沿纬圈的扰动动能与平均动能转换率(E)、角动量涡旋输送(RM),分析了E和RM的年、季分布特征及其与新疆暴风雪过程的关系.结果表明:E和RM具有显著的季节变化和周期性;E的正高值中心与新疆暴风雪过程有较好的关系,出现E正高值中心的日期作为预报指标日,其后3~6 d新疆将出现暴风雪天气过程,出现RM负低值中心的日期作为预报指标日,其后3~8 d新疆有暴风雪过程发生;当E的正高值中心和RM的负值中心同时出现时,更确定了新疆暴风雪过程出现的可能性. 相似文献
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