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铝钛柱撑改性膨润土处理两种模拟废水的实验研究 总被引:10,自引:1,他引:10
以钠基膨润土为原料制备了铝钛无机柱撑、铝钛有机柱撑改性膨润土,确定了改性膨润土的最佳铝钛比和铝土比,并将其应用于模拟废水、化学实验室废水的处理。与原土进行比较,探讨了用量、pH值、搅拌时间等对COD去除率、色度去除率、浊度去除率的影响,通过正交实验对实验条件进行了优化。结果表明:有机柱撑改性膨润土、无机柱撑改性膨润土对废水的处理效果均明显好于原土,对废水色度、浊度的去除率均大于93%;对废水COD的去除效果,有机柱撑改性膨润土比无机柱撑改性膨润土有较大提高,去除率最高达66.31%,结果令人满意。 相似文献
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锆铝基柱撑蒙脱土的制备研究 总被引:1,自引:0,他引:1
以钠基蒙脱土为原料,采用共聚法合成锆铝基柱撑蒙脱土,并研究不同锆铝摩尔比例和不同NaOH的量对柱撑蒙脱土制备的影响。XRD研究表明,当锆铝摩尔比例为1:6、加入70ml0.4mol/LNaOH时,可得到(001)面网层间距达1.9343nm的锆铝基柱撑蒙脱土。通过FT—IR发现,锆铝聚合羟基阳离子进入蒙脱土层间,形成Si-O-Al和Si-O-Zr。对柱撑前后蒙脱土的比表面积和孔径结构进行分析,发现锆铝基柱撑蒙脱土具有较大的比表面积,较为均匀的孔径分布,是一种合适的催化和吸附材料。 相似文献
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It is important to clarify the migration behavior of hydrogen gas dissolved in water-saturated, compacted bentonite, which is a promising material for geologic disposal of high-level waste and TRU waste disposal. The diffusion coefficients of helium, which can be detected under extremely low background conditions, in water-saturated, compacted Na-montmorillonite were determined as a function of temperature by a transient diffusion method. The activation energies for diffusion of helium were then obtained. The activation energies were from 6.9 ± 4.8 to 19 ± 2.8 kJ mol− 1 and were regarded to be independent of dry density. The activation energies of helium in water-saturated Na-montmorillonite were roughly equal to those in bulk water, 14.9 kJ mol− 1, and in ice, from 11 to 13 kJ mol− 1. It is possible that helium diffuses not only in pore water but also in interlayer water. 相似文献
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