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1.
Paul R. Craddock Olivier J. Rouxel Lary A. Ball Wolfgang Bach 《Chemical Geology》2008,253(3-4):102-113
We have developed a technique for the accurate and precise determination of 34S/32S isotope ratios (δ34S) in sulfur-bearing minerals using solution and laser ablation multiple-collector inductively coupled plasma mass spectrometry (MC-ICP-MS). We have examined and determined rigorous corrections for analytical difficulties such as instrumental mass bias, unresolved isobaric interferences, blanks, and laser ablation- and matrix-induced isotopic fractionation. Use of high resolution sector-field mass spectrometry removes major isobaric interferences from O2+. Standard-sample bracketing is used to correct for the instrumental mass bias of unknown samples. Background on sulfur masses arising from memory effects and residual oxygen-tailing are typically minor (< 0.2‰, within analytical error), and are mathematically removed by on-peak zero subtraction and by bracketing of samples with standards determined at the same signal intensity (within 20%). Matrix effects are significant (up to 0.7‰) for matrix compositions relevant to many natural sulfur-bearing minerals. For solution analysis, sulfur isotope compositions are best determined using purified (matrix-clean) sulfur standards and sample solutions using the chemical purification protocol we present. For in situ analysis, where the complex matrix cannot be removed prior to analysis, appropriately matrix-matching standards and samples removes matrix artifacts and yields sulfur isotope ratios consistent with conventional techniques using matrix-clean analytes. Our method enables solid samples to be calibrated against aqueous standards; a consideration that is important when certified, isotopically-homogeneous and appropriately matrix-matched solid standards do not exist. Further, bulk and in situ analyses can be performed interchangeably in a single analytical session because the instrumental setup is identical for both. We validated the robustness of our analytical method through multiple isotope analyses of a range of reference materials and have compared these with isotope ratios determined using independent techniques. Long-term reproducibility of S isotope compositions is typically 0.20‰ and 0.45‰ (2σ) for solution and laser analysis, respectively. Our method affords the opportunity to make accurate and relatively precise S isotope measurement for a wide range of sulfur-bearing materials, and is particularly appropriate for geologic samples with complex matrix and for which high-resolution in situ analysis is critical. 相似文献
2.
In the Gran Paradiso massif (western Alps), the boundary between the Erfaulet orthogneiss and the overlying metasediments (Money Complex) is interpreted as a Late Palaeozoic intrusive contact. Major arguments in favour of this hypothesis are: (i) the obliquity of the sedimentary layering with respect to the contact; (ii) the presence of aplitic dykes within the Money Complex; (iii) the lack of a mylonitic zone; and (iv) rare relics of an early generation of garnet in the Money metasediments, interpreted as evidence of the contact metamorphism of the Erfaulet granite. To cite this article: B. Le Bayon, M. Ballèvre, C. R. Geoscience 336 (2004). 相似文献
3.
This paper reviews the approach taken by several UK coastal partnerships in developing research strategies and programmes. It reports on the status of these research initiatives and describes how the co-ordination and communication of scientific research have been approached through active partnerships with universities and the wider research community. Results of semi-structured interviews are followed by in-depth case studies of research networks on the Sefton Coast (focusing on coastal morphology) and the Severn Estuary (focusing on coastal change and climate change impacts). The results reveal the constraints and opportunities that exist in bringing together a variety of knowledge holders in the coastal zone. The paper identifies key elements of these initiatives and highlights lessons that can be applied to the development of other research initiatives in order to achieve science supported, ecosystem-based management. 相似文献
4.
5.
The Bosworgey granite cusp forms an apical portion of the concealed northern extension of the Tregonning-Godolphin granite ridge. It is characterised by unusually high values of B, P, Mn, Fe, As, Cu, Nb, Ta, Bi, Sn, W, U and S which are present largely as tourmaline, apatite, pyrite, arsenopyrite, chalcopyrite, bismuth, columbite, cassiterite, wolframite and uraninite; and low levels of Zr, Hf, Ti and REE present in zircon, ilmenite and monazite. The granite is classified as Sn and W specialised (Tischendorf, 1974) and it belongs to the ilmenite series of Japanese workers. The classification of Chappell and White (1974) (S and I type granites) is shown to be inapplicable to Cornubian rocks although the Bosworgey samples show characteristics of S type granites. The accessory mineral assemblages are typical of high temperature lodes (cassiterite, wolframite, arsenopyrite, chalcopyrite) and the assamblage is concluded to be the cusp analogue of hypothermal lodes produced by extreme differentiation and concentration of volatiles. It is speculated that such granites could provide the parent material for the mesothermal crosscourse mineralisation (pitchblende, bismuth, pyrite, galena, sphalerite). 相似文献
6.
R.M. Brown H.R. Andrews G.C. Ball N. Burn Y. Imahori J.C.D. Milton E.L. Fireman 《Earth and Planetary Science Letters》1984,67(1):1-8
14C has been measured in three North American and seven Antarctic meteorites with the Chalk River MP tandem accelerator. In most cases cosmogenic14C, which is tightly bound, was separated from absorbed atmospheric radiocarbon by stepwise heating extractions. Terrestrial ages obtained by comparing cosmogenic14C in the meteorite to that in Bruderheim are (7.2 ± 0.6) × 103 years for Yamato 7304, (11.6 ± 0.4) × 103 years for Estacado, and range from (32.7 ± 0.5) × 103 to (41.0 ± 0.8) × 103 years for six meteorites recovered at Allan Hills and its vicinity. The present upper limit to age determination by the accelerator method varies from 50 × 103 to 70 × 103 years depending upon mass and carbon content of the sample. The natural limit caused by cosmic ray production of14C in silicate rocks at 2000 m elevation is estimated to be (55 ± 5) × 103 years. “Weathering ages” were estimated for the Antarctic meteorites from the specific activity of loosely-bound CO2 considered to be absorbed from the terrestrial atmosphere on weathering. The accelerator measurements are in accordance with previous low-level counting measurements but have higher precision and sensitivity. 相似文献
7.
As a result of affiliation between the Hudson's Bay Company and the Royal Society a relatively large number of instrumental temperature records are available from York Factory and Churchill Factory on the southwest of Hudson Bay beginning in 1768. The nature of these records, details of the instruments and information about the observers are presented. The major difficulty with the records is that the number of observations and the time of observation varied considerably. Adjustment factors were calculated for all of the combinations using a modern record maintained at the Churchill airport. By combining the Hudson's Bay Company record with data recorded by members of the Royal Canadian Mounted Police after 1852, and up to 1910, a long and relatively continuous record of daily and monthly average temperatures has been created for Central Canada. 相似文献
8.
Measurements of low-level dissolved-sulfide concentrations in estuarine water from San Francisco Bay have been made using
the sulfide-specific electrode after preservation, separation, and preconcentration of the sulfide species. The separation
and preconcentration were acheived by coprecipitation of ZnS with Zn(OH)2 followed by collection and dissolution of the precipitate, giving concentration factors up to 160-fold Preconcentration provided
sulfide solutions that were adequately measurable within the practical working range of the specific-ion electrode The sulfide
detection limit with the preconcentration step is 0 02 μg/l Spike recoveries in the range of 81 to 10 1% have been achieved
for laboratory-prepared samples having S2− concentrations as low as 0 6 μg/l and 84 to 100% for an estuarine sample spiked in the field with 2 μg/l (S(−II) Positive
correlations have been found between dissolved S(−II) concentrations and concentrations of dissolved Cd, Cu, and Ni, negative
correlations have been found between bisulfide (HS−) activity and activities of Cd2+, Cu2+, and Ag+ species 相似文献
9.
10.
Andrew Ball and Ian Crawford report on NASA's planning for a return to the Moon, with some thoughts on opportunities open to the UK. 相似文献