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Methyl-galactosides were oxidized at room temperature by galactose oxidase in a one-step reaction and afforded methyl-galactoaldehyde
in excellent yield and high purity. The resulting galactoaldehyde as a useful intermediate can be directly used in glycopeptide
synthesis. 相似文献
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4.
Sdsealbedoisdefinedasaratioofreflectivesolarradiationtototalacradiation,whichcanindicatetheaborptionandreflectivecapabilityofthe~hforsolarradiation.Itisan~tfactortoinfluencethes~radiationbalance,espeiallyfortheformationandvariationoflocalndcroclirnate.Generally,theactualdatafromo~tionalstationSforrebationareedintheanalysisofsolacealal.HOwever,therepresentativenessOfthedateisIratedduetothescarcityofobservationalstationandunevendistributionofs~condition.Afterthe1960s,theanalysisfors~ealbedoise… 相似文献
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A discrete element modelling of bonded granulates and investigation on the bond effect on their behaviour are very important to geomechanics. This paper presents a two‐dimensional (2‐D) discrete element theory for bonded granulates with bond rolling resistance and provides a numerical investigation into the effect of bond rolling resistance on the yielding of bonded granulates. The model consists of mechanical contact models and equations governing the motion of bonded particles. The key point of the theory is that the assumption in the original bond contact model previously proposed by the authors (55th CSCE‐ASCE Conference, Hamilton, Ont., Canada, 2002; 313–320; J. Eng. Mech. (ASCE) 2005; 131 (11):1209–1213) that bonded particles are in contact at discrete points, is here replaced by a more reliable assumption that bonded particles are in contact over a width. By making the idealization that the bond contact width is continuously distributed with the normal/tangential basic elements (BE) (each BE is composed of spring, dashpot, bond, slider or divider), we establish a bond rolling contact model together with bond normal/tangential contact models, and also relate the governing equations to local equilibrium. Only one physical parameter β needs to be introduced in the theory in comparison to the original bond discrete element model. The model has been implemented into a 2‐D distinct element method code, NS2D. Using the NS2D, a total of 86 1‐D, constant stress ratio, and biaxial compressions tests have been carried out on the bonded granular samples of different densities, bonding strengths and rolling resistances. The numerical results show that: (i) the new theory predicts a larger internal friction angle, a larger yielding stress, more brittle behaviour and larger final broken contact ratio than the original bond model; (ii) the yielding stress increases nonlinearly with the increasing value of β, and (iii) the first‐yield curve (initiation of bond breakage), which define a zone of none bond breakage and which shape and size are affected by the material density, is amplified by the bond rolling resistance in analogous to that predicted by the original bond model. Copyright © 2006 John Wiley & Sons, Ltd. 相似文献
7.
A. V. Bogomolov A. P. Ignat’ev K. Kudela S. N. Kuznetsov Yu. I. Logachev O. V. Morozov I. N. Myagkova S. N. Oparin A. A. Pertsov S. I. Svertilov B. Yu. Yushkov 《Astronomy Letters》2003,29(3):199-204
We consider temporal, spectral, and polarization parameters of the hard X-ray and gamma-ray radiation observed during the solar flare of May 20, 2002, in the course of experiments with the SONG and SPR-N instruments onboard the Coronas-F spacecraft. This flare is one of the most intense gamma-ray events among all of the bursts of solar hard electromagnetic radiation detected since the beginning of the Coronas-F operation (since July 31, 2001) and one of the few gamma-ray events observed during solar cycle 23. A simultaneous analysis of the Coronas-F and GOES data on solar thermal X-ray radiation suggests that, apart from heating due to currents of matter in the the flare region, impulsive heating due to the injection of energetic electrons took place during the near-limb flare S21E65 of May 20, 2002. These electrons produced intense hard X-ray and gamma-ray radiation. The spectrum of this radiation extends up to energies ≥7 MeV. Intense gamma-ray lines are virtually unobservable against the background of the nonthermal continuum. The polarization of the hard X-ray (20–100 keV) radiation was estimated to be ≤15–20%. No significant increase in the flux of energetic protons from the flare under consideration was found. At the same time, according to ACE data, the fluxes of energetic electrons in interplanetary space increased shortly (~25 min) after the flare. 相似文献
8.
四川石棉大水沟独立碲矿床堪称世界首例,其矿体两侧的围岩蚀变较窄,且蚀变带与矿脉及未蚀变岩呈清楚而截然的接触关系。主要围岩蚀变为白云石化、白(绢)云母化、云英岩化及电气石化等。这些蚀变作用分别发生于177.7~165.1Ma和91.71~80.19Ma。蚀变作用过程中SiO2大量析出,Al2O3、TiO2、CaO、MgO、K2O、H2O、CO2、Fe2O3、MnO则有不同程度地带入。与此同时,REE在此过程中包集体迁出,Te、Bi、AS等元素的含量则决定于蚀变作用及其强度,而与原岩无关。 相似文献
9.
Based on the CN and C2 comae isophotes for two comets (1961 IX and 1970 16) given by Rahe et al. and the relevant theory of physical chemistry, we have deduced the distributions of the CN and C2 modecules in the coma, their scale heights and mean lifetimes. The results favour the viewpoint that HCN is the parent of CN, and that C2H2 is the parent of C2. 相似文献
10.
CATASTROPHIC ECO-ENVIRONMENTAL CHANGE IN THE SONGNEN PLAIN, NORTHEASTERN CHINA SINCE 1900S 总被引:1,自引:1,他引:0
WANGHai-xia WANZhong-juan YUShao-peng LUOXin-zheng SUNGuang-you 《中国地理科学(英文版)》2004,14(2):179-185
Although the Songnen Plain in the northeastern China was developed relatively late in the temperate zone of the world, its eco-environment has changed greatly. This paper analyzes the changes of land cover and the rates and trends ofdesertification during the past 100 years in the Songnen Plain. According to the macroscopic analysis, we find that the eco-environment in the plain has reached to the threshold of catastrophic change since the 1950s. The Thorn Needle Catastrophic Model was used to determine and validate this conclusion. Human activities, including large-scale construction projects, such as huge dams and dikes, and excessive grazing were the primary factors contributing to regional eco-environmental catastrophe. And irrational reclamation of the wilderness also affected the eco-environmental change. The results reveal the complex human-land interactions. 相似文献