Contribution of SHRIMP U–Pb zircon geochronology to unravelling the evolution of Brazilian Neoproterozoic fold belts

The South-American continent is constituted of three major geologic–geotectonic entities: the homonym platform (consolidated at the end of the Cambrian), the Andean chain (essentially Meso-Cenozoic) and the Patagonian terrains, affected by tectonism and magmatism through almost all of the Phanerozoic. The platform is constituted by a series of cratonic nuclei (pre-Tonian, fragments of the Rodinia fission) surrounded by a complex fabric of Neoproterozoic structural provinces.     

Monitoring and modelling of hydrological processes in the semiarid region of Brazil: The Cariri experimental basins

Catchments have highly variable yields of runoff and soil erosion. The size, land use and the surface cover play a significant role and influence the catchment response and parameter values of simulation models. Two experimental basins—the Cariri basins—were equipped in a semi-arid region of Brazil, for obtaining runoff and sediment yield at different catchment scales, as well as, to evaluate the influence of the land use and surface cover. In the first basin, located in the municipality of Sumé, the field studies were carried out at two different scales: four micro-catchments with an area of around 0.5 ha and nine standard Wischmeier-type erosion plots of 100 m². The experimental units had varied vegetation and management. They were subjected only to natural rainfall events, and were monitored from 1982 to 1991. The total runoff and total sediment yield were determined for each of the events. The installations in the second basin, in the municipality of São João do Cariri, from 1999, include two erosion plots, three micro-catchments, and two sub-catchments of a small basin. These basins are still being monitored for runoff and sediment production. Among the micro-catchments two are nested to detect any scale effect at the micro-catchment level. Nearly 600 events of precipitation, that produced runoff in at least one of the experimental units, have been registered. These data have been used to evaluate the influence of various factors, including cultivation practices and to calibrate hydrological models for plots and micro-catchments. Parameters have been tested by means of cross validations among micro-catchments and sub-catchments. The data sets are made available to all the catchment hydrology researchers and others at https://doi.org/10.5281/zenodo.4690886 .     

Tectonic inversion assessed by integration of geological and geophysical data: The intracontinental Rio do Peixe Basin,NE Brazil

Common basin models assume that the post‐rift tectonic evolution of most basins is usually associated with tectonic quiescence. However, tectonic inversion during the post‐rift phase has been proposed for several sedimentary basins worldwide, but how and why it happens is still a matter of debate, especially in intracontinental settings where the lithosphere is old and thick. Here, we use geological and geophysical data from the Rio do Peixe Basin in NE Brazil to show evidence that intracontinental sedimentary basins can be tectonically inverted by far‐field compressive stresses acting on pre‐existing weakness zones of lithospheric‐scale where stresses can concentrate and inversion can occur. Geomorphological and field data combined with seismic reflection, gravimetric and borehole data show that: (a) inversion occurred along two main Precambrian lithospheric‐scale shear zones, the Patos (E‐W trending) and Portalegre (NE‐SW trending), which had already been reactivated as basin‐bounding faults during the earlier rift stage; (b) post‐rift reactivation affected (mostly) the original master normal faults with the largest rift displacements, and locally produced new reverse faults; (c) during contraction, deformation was partitioned between fault reactivation and buckling of the incompetent sediment pushed against the hard basement; (d) all these signs of inversion have been observed in the field and can be demonstrated on seismic reflection profiles; and (e) combined gravimetric and seismic data show that the main structures of the basin were followed by an inversion. These data are consistent with the operation of WSW‐ENE horizontal maximum compressive stress as a result of combined pushes of the Mid‐Atlantic Ridge (towards the W) and the Andes (towards the E), responsible for the post‐rift oblique inversion of normal faults inherited from the rift phase and formed with vertical maximum compressive stress.     

Fracturing and fluid‐flow during post‐rift subsidence in carbonates of the Jandaíra Formation,Potiguar Basin,NE Brazil

Pervasive fracture networks are common in many reservoir‐scale carbonate bodies even in the absence of large deformation and exert a major impact on their mechanical and flow behaviour. The Upper Cretaceous Jandaíra Formation is a few hundred meters thick succession of shallow water carbonates deposited during the early post‐rift stage of the Potiguar rift (NE Brazil). The Jandaíra Formation in the present onshore domain experienced <1.5 km thermal subsidence and, following Tertiary exhumation, forms outcrops over an area of >1000 km². The carbonates have a gentle, <5?, dip to the NE and are affected by few regional, low displacement faults or folds. Despite their simple tectonic history, carbonates display ubiquitous open fractures, sub‐vertical veins, and sub‐vertical as well as sub‐horizontal stylolites. Combining structural analysis, drone imaging, isotope studies and mathematical modelling, we reconstruct the fracturing history of the Jandaíra Formation during and following subsidence and analyse the impact fractures had on coeval fluid flow. We find that Jandaíra carbonates, fully cemented after early diagenesis, experienced negligible deformation during the first few hundreds of meters of subsidence but were pervasively fractured when they reached depths >400–500 m. Deformation was accommodated by a dense network of sub‐vertical mode I and hybrid fractures associated with sub‐vertical stylolites developed in a stress field characterised by a sub‐horizontal σ₁ and sub‐vertical σ₂. The development of a network of hybrid fractures, rarely reported in the literature, activated the circulation of waters charged in the mountainous region, flowing along the porous Açu sandstone underlying the Jandaíra carbonates and rising to the surface through the fractured carbonates. With persisting subsidence, carbonates reached depths of 800–900 m entering a depth interval characterised by a sub‐vertical σ₁. At this stage, sub‐horizontal stylolites developed liberating calcite which sealed the sub‐vertical open fractures transforming them in veins and preventing further flow. During Tertiary exhumation, several of the pre‐existing veins and stylolites opened and became longer, and new fractures were created typically with the same directions of the older features. The simplicity of our model suggests that most rocks in passive margin settings might have followed a similar evolution and thus display similar structures.     

Late Pleistocene tectonic-geomorphological development within a passive margin — The Cariatá trough, northeastern Brazil

Studies on the geomorphological evolution of the South American passive margin have been based on the pediplanation model, which predicts that its morphology is a response to regional uniform uplift and concomitant development of erosion surfaces. We combined remote sensing, geological mapping, lithostratigraphic and facies analyses, and luminescence dating in the Cariatá trough, northeastern Brazil, in order to determine how brittle tectonics and climate influenced colluviation and the shaping of local landforms in the Quaternary. Our work indicates that Cariatá is an asymmetrical trough  40 km long,  25 km wide, 250–550 m deep, and delimited by ENE–WSW-trending faults to the north and south. We recognized an ENE–WSW-oriented compression related to a strike-slip faulting regime, which corresponds to the present-day stress field in the region. This faulting event led to the deposition of colluvial fans, shed from adjacent uplifted crustal blocks, in a tectonically controlled depression. The colluvial succession is  45 m thick and presents two facies assemblages that filled the southern and, in particular, the northern borders of the trough: non-cohesive debrisflow and mudflow deposits. Optically stimulated luminescence dates of the sedimentary infill yielded ages at 224–128 ka and 45–28 ka, dominated by debrisflow and mudflow deposits, respectively. These ages may be over-estimated due to poor bleaching of colluvium, but they and our field data suggest that the margins of the trough were tectonically uplifted and eroded twice in the Late Pleistocene. The spasmodic colluvial accretion reflects the occurrence of high-magnitude, low-recurrence episodes probably associated with climate shifts in a semi-arid hillslope system. It follows that the present-day low-lying piedmont in which the Cariatá trough occurs is a juxtaposition of surfaces of various ages. This trough may have counterparts across the region. These conclusions do not corroborate the application of the cyclical pediplanation hypothesis in the area.     

Induced seismicity in the Castanhão reservoir, NE Brazil — Preliminary results

The Castanhão reservoir was built in the state of Ceará, a dry region in Northeastern Brazil, to regulate the flow of the Jaguaribe River, for irrigation, and for power generation. It is an earth-filled dam, 60 m high, with a water capacity of 4.5 × 10⁹ m³. The seismicity in the area has been monitored since 1998, with a few interruptions, using one analog or one digital station and, during a few periods, a three-station network. The first earthquakes likely to be induced events were detected in 2003, when the water level was about 20 m high. In early 2004 a very heavy rainfall season quickly filled the reservoir. Shortly after, an increase in the seismic activity occurred and many micro-earthquakes were recorded. We suggest that this activity resulted from an increase in pore pressure due to undrained response. Therefore, we may classify this cluster of micro-earthquakes as “initial seismicity.” We deployed a network with four analog stations in the area, following this activity, to determine the epicentral zone. At least three epicentral areas under the reservoir were detected. The spatio-temporal analysis of the available data revealed that the seismicity occurs in clusters and that these were activated at different periods. We identified four sets of faults (N–S-, E–W-, NW–SE-, and NE–SW-oriented), some of which moved in shallow crustal levels and as recently as the Quaternary (1.8 Ma). Under the present-day stress regime, the last two sets moved as strike-slip structures. We suggest a possible correlation between dormant faults and the observed induced seismicity.     

Strategies to Make Methods Based on Flow Injection Analysis Greener

The implementation of flow injection analysis (FIA) systems and correlated techniques in the laboratory routine provides an increase of analytical throughput and the reduction of risks of analyte losses and contamination. Naturally, it contributes to the reduction of reagent consumption and minimization of waste generation. This paper presents and discusses an overview of the main strategies adopted to make methods based on FIA systems more environmentally friendly, and offers a review of these methods that covers the period from January 2002 to December 2019. Strategies based on reagent management (adoption of procedures without reagents, replacement of toxic reagents, recycling and reuse of reagents and, use of immobilized reagents), the online waste treatment, and the improvements of FIA systems (flow system configurations that avoid reagent wastage, use of green detectors, automation, and miniaturization) are approached in this perspective.     

Unusual Carbonatite Lavas from Active Volcano, Oldoinyo Lengai

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Unusual Carbonatite Lavas from Active Volcano, Oldoinyo Lengai