Small hypervelocity particles captured in aerogel collectors: Location,extraction, handling and storage

Abstract— It has now been about a decade since the first demonstrations that hypervelocity particles could be captured, partially intact, in aerogel collectors. But the initial promise of a bonanza of partially‐intact extraterrestrial particles, collected in space, has yet to materialize. One of the difficulties that investigators have encountered is that the location, extraction, handling and analysis of very small (10 μm and less) grains, which constitute the vast majority of the captured particles, is challenging and burdensome. Furthermore, current extraction techniques tend to be destructive over large areas of the collectors. Here we describe our efforts to alleviate some of these difficulties. We have learned how to rapidly and efficiently locate captured particles in aerogel collectors, using an automated microscopic scanning system originally developed for experimental nuclear astrophysics. We have learned how to precisely excavate small access tunnels and trenches using an automated micromanipulator and glass microneedles as tools. These excavations are only destructive to the collector in a very small area—this feature may be particularly important for excavations in the precious Stardust collectors. Using actuatable silicon microtweezers, we have learned how to extract and store “naked” particles—essentially free of aerogel—as small as 3 μm in size. We have also developed a technique for extracting particles, along with their terminal tracks, still embedded in small cubical aerogel blocks. We have developed a novel method for storing very small particles in etched nuclear tracks. We have applied these techniques to the extraction and storage of grains captured in aerogel collectors (Particle Impact Experiment, Orbital Debris Collector Experiment, Comet‐99) in low Earth orbit.     

The X-ray and extreme-ultraviolet flux evolution of SS Cygni throughout outburst

We present the most complete multiwavelength coverage of any dwarf nova outburst: simultaneous optical, Extreme Ultraviolet Explorer and Rossi X-ray Timing Explorer observations of SS Cygni throughout a narrow asymmetric outburst. Our data show that the high-energy outburst begins in the X-ray waveband 0.9–1.4 d after the beginning of the optical rise and 0.6 d before the extreme-ultraviolet rise. The X-ray flux drops suddenly, immediately before the extreme-ultraviolet flux rise, supporting the view that both components arise in the boundary layer between the accretion disc and white dwarf surface. The early rise of the X-ray flux shows that the propagation time of the outburst heating wave may have been previously overestimated.
The transitions between X-ray and extreme-ultraviolet dominated emission are accompanied by intense variability in the X-ray flux, with time-scales of minutes. As detailed by Mauche & Robinson, dwarf nova oscillations are detected throughout the extreme-ultraviolet outburst, but we find they are absent from the X-ray light curve.
X-ray and extreme-ultraviolet luminosities imply accretion rates of  3 × 10¹⁵ g s⁻¹  in quiescence,  1 × 10¹⁶ g s⁻¹  when the boundary layer becomes optically thick, and  ∼10¹⁸ g s⁻¹  at the peak of the outburst. The quiescent accretion rate is two and a half orders of magnitude higher than predicted by the standard disc instability model, and we suggest this may be because the inner accretion disc in SS Cyg is in a permanent outburst state.     

Biostratigraphic and aminostratigraphic constraints on the age of the Middle Pleistocene glacial succession in north Norfolk,UK

Considerable debate surrounds the age of the Middle Pleistocene glacial succession in East Anglia following some recent stratigraphical reinterpretations. Resolution of the stratigraphy here is important since it not only concerns the glacial history of the region but also has a bearing on our understanding of the earliest human occupation of north‐western Europe. The orthodox consensus that all the tills were emplaced during the Anglian (Marine Isotope Stage (MIS) 12) has recently been challenged by a view assigning each major till to a different glacial stage, before, during and after MIS 12. Between Trimingham and Sidestrand on the north Norfolk coast, datable organic sediments occur immediately below and above the glacial succession. The oldest glacial deposit (Happisburgh Till) directly overlies the ‘Sidestrand Unio‐bed’, here defined as the Sidestrand Hall Member of the Cromer Forest‐bed Formation. Dating of these sediments therefore has a bearing on the maximum age of the glacial sequence. This paper reviews the palaeobotany and describes the faunal assemblages recovered from the Sidestrand Unio‐bed, which accumulated in a fluvial environment in a fully temperate climate with regional deciduous woodland. There are indications from the ostracods for weakly brackish conditions. Significant differences are apparent between the Sidestrand assemblages and those from West Runton, the type site of the Cromerian Stage. These differences do not result from contrasting facies or taphonomy but reflect warmer palaeotemperatures at Sidestrand and a much younger age. This conclusion is suggested by the higher proportion of thermophiles at Sidestrand and the occurrence of a water vole with unrooted molars (Arvicola) rather than its ancestor Mimomys savini with rooted molars. Amino acid racemisation data also indicate that Sidestrand is significantly younger than West Runton. These data further highlight the stratigraphical complexity of the ‘Cromerian Complex’ and support the conventional view that the Happisburgh Till was emplaced during the Anglian rather than the recently advanced view that it dates from MIS 16. Moreover, new evidence from the Trimingham lake bed (Sidestrand Cliff Formation) above the youngest glacial outwash sediments (Briton's Lane Formation) indicates that they also accumulated during a Middle Pleistocene interglacial – probably MIS 11. All of this evidence is consistent with a short chronology placing the glacial deposits within MIS 12, rather than invoking multiple episodes of glaciation envisaged in the ‘new glacial stratigraphy’ during MIS 16, 12, 10 and 6. Copyright © 2009 John Wiley & Sons, Ltd.     

The palaeoenvironment associated with a partial Iguanodon skeleton from the Upper Weald Clay (Barremian, Early Cretaceous) at Smokejacks Brickworks (Ockley, Surrey, UK), based on palynomorphs and ostracods

In 2001 a partial skeleton of an Iguanodon was discovered in the Upper Weald Clay (Barremian, Early Cretaceous) at Smokejacks Brickworks near Ockley, Surrey, UK. When the dinosaur was excavated, a detailed stratigraphic section was logged and 25 samples taken for palynological and micropalaeontological (ostracod and megaspore) analysis, including a detailed sample set of the dinosaur bed itself. Qualitative and quantitative analysis of the palynoflora revealed rich and well-preserved non-marine assemblages of pollen and spores, including early angiosperms, and freshwater green algae. Four types of angiosperm pollen are described and assigned to the genus Retimonocolpites Pierce, 1961, but left in open nomenclature. Some marine elements such as dinoflagellate cysts are identified as the result of reworking of Middle and Upper Jurassic sediments. The pollen/spore assemblages depict a vegetational change from principally gymnosperm-dominated assemblages at the base to principally pteridophyte-dominated assemblages at the top of the section. The dinosaur bed shows a pteridophyte-dominated assemblage, with a significantly high amount of the freshwater green alga Scenedesmus novilunaris He Cheng-quan et al., 1992. Samples close to the dinosaur bed yielded the first useful ostracod finds from Smokejacks Brickworks: well-preserved assemblages containing Cypridea clavata (Anderson, 1939), Damonella cf. pygmaea (Anderson, 1941), Stenestroemia cf. cressida Anderson, 1971 and Stenestroemia sp. A, and fragments and damaged valves of a thin-shelled ostracod, possibly belonging to Mantelliana Anderson, 1966. Those identified as Cypridea clavata show a wide range of morphological variety and in opposition to Anderson's (1967, 1985) taxonomic scheme, which would assign them to up to five different taxa, they are considered to be intraspecific variants of a single species. The possibilities and limitations of age determination of the Wealden sediments using palynomorphs and ostracods are discussed; distinct forms of early angiosperm pollen, together with the ostracod fauna, are consistent with an early Barremian age. Pollen and spores are discussed in terms of their parent plants and the reconstruction of vegetation and palaeoclimate. Palynology and ostracods give evidence for temporary freshwater conditions at the time when the Iguanodon died and the carcase was buried.     

Transport and accumulation of organochlorines in the ovaries of Atlantic croaker (Micropogonias undulatus)

The role of vitellogenin in the transport of organochlorines was investigated in Atlantic croaker (Micropogonias undulatus) by exposing them through the diet to o,p′-DDT at a concentration of 10.8 μg/100 g fish/day for 14 days or Aroclor 1254 (PCB) at a concentration of 0.5 mg/100 g fish/day for 30 days during gonadal recrudescence. Tissue samples were taken from the fish at various times after initial exposure, and o,p′-DDT and PCBs were extracted in acetonitrile and analyzed by gas chromatography. Analysis of the ovarian tissue collected 2 and 3 weeks from the start of exposure revealed that the o,p′-DDT concentration increases as the gonadosomatic index (GSI) increases (r² = 0.63), with accumulation ranging from less than 1% to as much as 8% of the total dosage. Interestingly, o,p′-DDT did not accumulate in the testes during the same exposure period. Accumulation of PCBs was found to be 40 times higher in the ovaries than in the testes. Gel filtration of plasma from exposed females showed that o,p′-DDT elutes in the low density lipoprotein and vitellogenin fractions. Control plasma incubated with o,p′-DDT at 4 °C for 16 h followed by chromatography on Sepharose 6B gave similar results with an o,p′-DDT concentration of 0.6μg/mg protein in the vitellogenin fraction. Furthermore, both o,p′-DDT and PCBs were found to bind to purified croaker vitellogenin. These results suggest that lipoproteins, including vitellogenin, are involved in the transport and accumulation of organochlorines in the ovaries of exposed fish.     

Book reviews

THE IMPACT OF VOLCANIC HAZARDS AT RABAUL, PAPUA NEW GUINEA (Discussion Paper No. 33) by R. J. Blong and C. Aislabie. 17 × 25 cm, xiv and 207 pages. Institute of National Affairs: Port Morseby 1988 (ISBN 9980 77 086 4).

A PRACTICAL APPROACH TO SEDIMENTOLOGY by R. C. Lindholm. 15 × 23 cm, xviii and 279 pages. Allen & Unwin: London 1987 (ISBN 0 04 551132 2) $A45.00 (soft).

THE ATMOSPHERE AND WEATHER OF SOUTHERN AFRICA by R. A. Preston‐Whyte and P. D. Tyson. 18 × 24 cm, xiii and 375 pages. Oxford University Press: Cape Town 1988 (ISBN 0 19 570 514 9) R56.00 (hard); (ISBN 0 19 570 496 7) R39.14 (soft).

QUATERNARY PALEOCLIMATOLOGY: Methods of Paleoclimatic Reconstruction by R. S. Bradley. 15 × 23 cm, xvii and 472 pages. Allen & Unwin: Boston 1985 (ISBN 0 04 551067 9) $A69.95 (hard); (ISBN 0 04 551068 7) $A39.95 (soft).

PROCESSES IN PHYSICAL GEOGRAPHY by R. D. Thompson, A. M. Mannion, C. W. Mitchell, M. Parry and J. R. Townsend. 24 × 19 cm, xii and 380 pages. Longman: London 1986 (ISBN 0 582 30136) $A44.95.

PERSPECTIVES ON A DYNAMIC EARTH by T. R. Paton. 16 × 24 cm, 142 pages. Allen & Unwin: London 1986 (ISBN 0 04 55 0043 6) $A23.95 (soft).

LAND DEGRADATION AND SOCIETY edited by P. Blaikie and H. Brookfield. 15 × 23 cm. xxiv and 296 pages. Methuen: London 1987 (ISBN 0 416 40150 3) $A32.95 (soft).

THE PENGUIN DICTIONARY OF HUMAN GEOGRAPHY by B. Goodall. 13 × 20 cm, 509 pages. Penguin: Harmondsworth 1987 (ISBN 0 14 051095 8) $A19.95 (soft).

MAKING SENSE OF DEVELOPMENT: An Introduction to Classical and Contemporary Theories of Development and Their Application to South‐east Asia by P. W. Preston. 14 × 22 cm, xxi and 318 pages. Routledge & Kegan Paul: London 1986 (ISBN 0 7102 0813 8) $A87.95 (hard).

THE DEMOGRAPHIC DIMENSION IN INDONESIAN DEVELOPMENT by G. J. Hugo, T. H. Hull, V. J. Hull and G. W. Jones. 16 × 25 cm, xxv and 417 pages. Oxford University Press: Singapore 1987 (ISBN 0 19 582699 X) $A49.95 (hard).

GLOBAL ISSUES AND OUTLOOK IN PULP AND PAPER edited by G. F. Schreuder, 18 × 26 cm, ix and 302 pages. University of Washington Press: Seattle 1988 (ISBN 0 295 96642 4) $US40.00 (hard).

AN HISTORICAL GEOGRAPHY OF MODERN AUSTRALIA: The Restive Fringe (Cambridge Studies in Historical Geography No. 11) by J. M. Powell. 16 × 33 cm, xx and 400 pages. Cambridge University Press: Cambridge 1988 (ISBN 0 521 25619 4) $A39.95 (hard).

HISTORICAL GEOGRAPHY: Progress and Prospect edited by M. Pacione. 14 × 22 cm, 306 pages. Croom Helm: London 1987 (ISBN 0 7099 40467) $A27.50 (hard).

THE ROLE OF THEORY IN URBAN PLANNING: A Study of Metropolitan Planning in Perth, Western Australia (Geowest No. 24) by O. Yiftachel. 21 × 29 cm, 102 pages. Department of Geography, University of Western Australia: Nedlands 1987 (ISBN 0 86422 063 4).

SYDNEY INTO ITS THIRD CENTURY: Metropolitan Strategy for the Sydney Region by NSW Department of Environment and Planning. 21 × 29 cm, 72 pages. NSW department of Environment and Planning: Sydney 1988 (ISBN 0 7305 4312 9).

BUS SERVICES IN WESTERN SYDNEY: Private Bus Operators and Government Transport Departments (Monograph Series No. 3) by P. Tranter. 21 × 29 cm, v and 98 pages. Department of Geography and Oceanography, University College, Australian Defence Force Academy: Campbell, ACT 1988 (ISBN 0 7317 0036 8).

AGEING IN VICTORIA: An Electronic Social Atlas by A. L. Howe, P. Newton and P. Sharwood. 30 × 21 cm, 105 pages. National Research Institute for Gerontology and Geriatric Medicine, Mt. Royal Hospital and University of Melbourne: Melbourne 1987 (ISBN 0 958326 6 2) $A10.00 (soft).

READINGS IN AUSTRALIAN GEOGRAPHY: Proceedings of the 21st Institute of Australian Geographers’ Conference, Perth 10–18 May 1986, edited by A. Conacher. 21 × 29 cm, vi and 493 pages. Institute of Australian Geographers (WA Branch) and Department of Geography, University of Western Australia: Perth 1987 (ISBN 0 909678 30 B) $A25.00 (soft).

GEOGRAPHY RESEARCH PROJECTS: A Senior Student's Handbook by H. Binden and H. Williams. 18 × 26 cm, 149 pages. Edward Arnold Australia: Caulfield East 1988 (ISBN 0 7131 8311 X) $A 14.95 (soft).

OUR AMERICAN LAND: 1987 Yearbook of Agriculture, ix and 323 pages. US Government Printing Office, Washington, DC: 1987 $US9.50.

THE ENCYCLOPAEDIC DICTIONARY OF PHYSICAL GEOGRAPHY edited by A. Goudie et al. 17 × 24 cm, xvi and 528 pages. Basil Black‐well: Oxford 1988 (ISBN 0 631 15581 3) $A34.95 (soft).

THE CONSERVATION OF ECOSYSTEMS AND SPECIES by Gareth E. Jones, 14 × 22 cm, 277 pages. Croom Helm: London 1987 (ISBN 0 7099 1463 6) $A87.95 (hard).

SO CAME THEY SOUTH by R. Clancy and A. Richardson. 35 × 35 cm, 176 pages. Shakespeare Head: Sydney 1988 (ISBN 0 7302 0864 8) $A34.95.     

The “El Pilote” fluorite skarn: A crucial deposit in the understanding and interpretation of the origin and mobilization of F from northern Mexico deposits

Fluorite deposits are widespread in northern Mexico and those deposits have traditionally been categorized as exclusively hydrothermal–magmatic in origin. Recently, two different fluorite-bearing type models have been proposed for the Northern Mexican deposits: (1) MVT-like deposits formed from basinal brines mobilized during the Laramide Orogeny (La Encantada deposit, Gonzalez-Partida et al., [Gonzalez-Partida, E., Carrillo-Chavez, A., Grimmer, J.O.W., Pironon, J., 2002. Petroleum-rich fluid inclusions in fluorite, Purisima mine, Coahuila, Mexico. International Geological Review 44 (8), 751–763.]; Tritlla et al., [Tritlla, J., Gonzalez-Partida, E., Levresse, G., Banks, D., Pironon, J., 2004. Fluorite deposits at Encantada-Buenavista, Mexico: products of Mississippi Valley type processes — a reply. Ore Geology Reviews 25, 329–332.]); and (2) fluorite-bearing skarns in close contact with rhyolite intrusives (Levinson, [Levinson, A.A., 1962. Beryllium–fluorine mineralization at Aguachile Mountain, Coahuila, Mexico. American Mineralogist 47, 67–75.]). The El Pilote fluorite deposit falls into the second category, and is the only known example of a magmatic-related fluorite deposit in the area. The fluorite trace-element patterns from both the El Pilote skarn and La Encantada MVT deposits display comparable and very low relative abundances as well as comparable chondrite-normalized REE patterns; this would suggest that the skarn F-source comes from the remobilization of a MVT fluorite manto.     

GGR Critical Review of Analytical Developments in 2004–2005

In 2005 Geostandards and Geoanalytical Research embarked upon a new initiative for its readers. Key researchers in various fields of geoanalytical technique development and their application were identified and invited to provide reviews pertinent to their expertise. As noted in the first of these publications "…instead of revisiting the historical context or decades of development in each analytical technique, the goal here has been to capture a snapshot of "hot topics" across a range of fields as represented in the… literature" (Hergt et al . 2005). Rather than prepare an annual review, a decision was taken earlier this year to provide a biennial summary of progress and accomplishments, in this case for the years 2004–2005. The principal techniques employed in Earth and environmental sciences are covered here, and include laser ablation and multicollector ICP-MS, ICP-AES, thermal ionisation and secondary ion mass spectrometry, as well as neutron activation analysis, X-ray fluorescence and atomic absorption spectrometry. A comprehensive review of the development of reference materials, often essential to these techniques, is also provided. The contributions assembled serve both to keep readers informed of advances they may be unfamiliar with, but also as a means of showcasing examples of the breadth and depth of work being conducted in these fields.