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TritonX-100-5-Br-PADAP光度法测定铜和镍 总被引:2,自引:0,他引:2
研究了非离子型表面活性剂Triton X- 100 存在下,用5 - Br - PADAP 光度法测定铜、镍的方法。结果表明:在pH9 .0 的硼砂缓冲介质中,5 - Br - PADAP 与铜和镍生成紫红色络合物,λCum ax = 575 nm ,εCu = 1 .04 ×105 L·mol- 1·cm - 1 ;λNim ax = 575 nm ,εNi = 1 .14 ×105 L·mol- 1·cm - 1 。铜和镍的质量浓度分别在0 ~560 μg/ L和0 ~440 μg/ L符合比尔定律。加入六偏磷酸钠后,由于偏磷酸镍的形成,镍不再与5 - Br - PADAP 显色,可通过铜及铜镍总量的测定,计算出镍的含量。用该方法实测了钢样中铜和镍的含量,结果与推荐值相符,对铜和镍5 次测定的RSD均小于5 % 。 相似文献
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Milatz Marius Hüsener Nicole Andò Edward Viggiani Gioacchino Grabe Jürgen 《Acta Geotechnica》2021,16(11):3573-3600
Acta Geotechnica - Gauging the mechanical effect of partial saturation in granular materials is experimentally challenging due to the very low suctions resulting from large pores. To this end, a... 相似文献
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SA Mwachireya M Carreiro-Silva BE Hartwick TR McClanahan 《African Journal of Marine Science》2018,40(1):25-42
Microbioerosion rates and microbioeroder community structure were studied in four Kenyan protected coral-reef lagoons using shell fragments of Tridacna giant clams to determine their response to the influence of terrestrial run-off. Fourteen different microbioeroder traces from seven cyanobacteria, three green algae and four fungi species were identified. The river discharge-impacted reef and ‘pristine’ reef showed similar composition but higher microbioeroder abundance and total cyanobacteria- and chlorophyte-bioeroded areas when compared with the other study reefs. Cyanobacteria dominated during the north-east monsoon (NEM) relative to the south-east monsoon (SEM) season, with algae and cyanobacteria being major microbioeroders in the river-impacted and pristine reefs. The rate of microbioerosion varied between 4.3 g CaCO3 m?2 y?1 (SEM) and 134.7 g CaCO3 m?2 y?1 (NEM), and was highest in the river-impacted reef (127.6 g CaCO3 m?2 y?1), which was almost double that in the pristine reef (69.5 g CaCO3 m?2 y?1) and the mangrove-fringed reef (56.2 g CaCO3 m?2 y?1). The microbioerosion rates measured in this study may not be high enough to cause concern with regard to the health and net carbonate production of Kenya’s coral reefs. Nevertheless, predicted increases in the frequency and severity of stresses related to global climate change (e.g. increased sea surface temperature, acidification), as well as interactions with local disturbances and their influence on bioerosion, may be increasingly important in the future. 相似文献
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The identification, remedial treatment, and monitoring of contaminated sediments are among the priorities for managers of the Tampa Bay Estuary. Tampa Bay, as an urbanized estuary, is subject to the input of watershed sources of chemical contaminants, including metals, pesticides, and organic chemicals. Although the use of biological indicators and their incorporation into multi-metric indices is not new, the refinement and applications of such techniques for determining environmental condition still require further development and exploration. We present a single Tampa Bay Benthic Index (TBBI) that was developed specifically for Tampa Bay. Stepwise discriminant analysis was applied to a comprehensive list of potential benthic metrics. Results from the stepwise procedure identified the metrics that best discriminated between "healthy" and "degraded" conditions, as defined by sediment contaminant effect levels and dissolved oxygen. Discriminant analysis was then applied to the resultant three variables to determine the linear combination for the index. 相似文献
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随着新能源产业的快速发展, 全球碳酸锂贸易量逐渐增长, 但其出口集中于少数国家, 这意味着全球碳酸锂供应存在一定的风险。为了深入了解全球碳酸锂贸易格局演变、供应危机传播路径及影响, 本文构建了2000—2021年全球碳酸锂贸易网络和级联失效模型, 概述了主要出口国贸易流向和贸易格局演变过程, 并模拟了不同供应危机来源的雪崩规模、传播路径及其影响。我们得到: (1)20多年来全球碳酸锂贸易集中度逐渐增加, 出口前三位国家保持稳定, 而主要进口大国变化明显, 贸易格局已由南美供应全球转变为南美供应东亚; (2)碳酸锂贸易供应危机的影响范围逐渐扩大, 间接传播逐渐占据主导地位; (3)智利供应危机对中日韩的影响程度逐渐扩大, 但对欧洲的影响时间最长; 阿根廷和中国的雪崩规模在上升、传播次数增加, 而美国则相反。本文将贸易格局演变与危机传播结合, 明确了全球碳酸锂主要贸易国智利、阿根廷、中国、德国等作为供应危机来源的影响程度及其传播路径。以上分析结果将有利于维护全球碳酸锂贸易稳定和主要贸易国采取应对策略缓解供应危机。 相似文献
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基于对子午链台站地震地磁前兆异常以及地球空间环境变化等研究方向的需求分析,利用网络、大数据、云计算等新技术,结合地震数据专家(DatistEQ)软件,设计子午链台站地磁指数报告自动产出系统。该系统通过低代码、敏捷式开发工作流程,连接不同功能节点,可以实现用户定制化、数据标准化、功能智能化的系统报告产出。通过本地或者云端一键流程化工作,将不同类型的数据发送到科研工作者或其他需求者,简化工作流程,优化数据处理,实现高效率产品产出。 相似文献
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Crustal deformation shows different patterns at different depths due to changes in the physical properties of rock.Tectonic levels can be defined based on the geometry and deformation mechanisms of crustal deformation patterns. Nujiang Gorge, with a high riverbed drop, great erosion depth, and strong deformation, has rock exposures at different tectonic levels and thus provides an ideal lab for deformation study. This paper takes the Nujiang Gorge from Chawalong to Fugong as the object to identify structural deformation patterns at different depths through field study and deformation analysis. At depth, the primary form of deformation is flow deformation, as shown on the outcrops at Maji. Ductile shear deformation can be found in many outcrops within the study region, e.g., the Gaoligong dextral shear zone and Puladi-Songta sinistral shear zone that lie to the south and north of Maji, respectively. Further to the north of Puladi, the dominated deformation pattern is similar fold and dense sub-vertical foliation. In addition, brittle faults, as evidence of shallow deformation, can be seen overprinting on the deeper deformation features all over the region. Based on those observations, this paper identifies four tectonic levels from depth to the surface: flow deformation, ductile shear deformation, similar fold, and brittle fault deformation, all of which result from the NEE-SWW compressive stress field. Further evidence from studies on the region′s thermal evolution and regional tectonics suggests that the development of different tectonic levels is closely linked to the discrepant uplift or denudation since the Miocene(~21 Ma). 相似文献