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1.
A method was developed for the determination of organic halogens in water samples with the aim of minimizing matrix effects and simplifying the sample preparation technique commonly used. The method is based on the adsorption of organic halogens in modified hydrophilic divinylbenzene polymer columns and their elution with methanol. The adsorbent used enables rapid adsorption and desorption due to comparatively high operating flow rates and minimized solvent amounts. Furthermore, no additional reconcentration steps are needed. The methanol extract obtained is combusted with a standard EOX (extractable organic halogen) analyzer and the concentration of organically bound halogens is determined by microcoulometric analysis. The matrix effects are considerably reduced compared to the standard procedure (EN 1485) commonly used. A detection limit of 13 μg/L was established. 相似文献
2.
This paper deals with the derivation of the convective mixing height and the characteristic convective velocity w
* from profiles of
w
measured by sodar. The parameters were obtained by fitting an analytical profile to the observed data. Results were compared with values obtained by the meteorological preprocessor of a dispersion model and from noon radiosoundings. In addition, a Monte Carlo method was applied to study the influence of measurement errors. It turned out that it is inherently difficult to determine the depth of deep mixed layers from sodar measurements with a limited range, although the determination of w
* should be possible. However, a significant underestimation of
w
, and thus w
*, was found, which is probably due to disproportional sampling of updrafts and downdrafts. 相似文献
3.
Pollen, sedimentological and charcoal particle analyses are presented from Devensian Late-glacial and early- to mid-Flandrian deposits from a former lake in the Vale of Pickering, Yorkshire. The combined analytical methods provide evidence for a short-lived climatic deterioration towards the end of the Late-glacial Interstadial, followed by a brief recovery prior to the Loch Lomond Stadial. This deterioration may be correlated with one of the ‘pre-Younger Dryas’ cooling periods identified not only in other pollen sequences from Britain and Europe, but from such diverse sources as Foraminifera from the Norwegian Sea and electrical conductivity measurements from the Greenland ice sheet. Loss-on-ignition and magnetic susceptibility data suggest that the Loch Lomond Stadial was characterised by an initial prolonged temperature decline, followed by a sudden more severe downturn resulting in particularly intense solifluction. Radiocarbon accelerator dating of the early Flandrian marl deposits illustrates the problem of age determination in calcareous lakes, and an estimate of the magnitude of ‘hard water error’ is obtained. The local population expansion of Alnus glutinosa is dated to 7640 ± 85 yr BP, but there is possible evidence for a Late-glacial presence of the tree, the significance of which is discussed in relation to other sites in east Yorkshire. © 1996 John Wiley & Sons, Ltd. 相似文献
4.
Yastami Oka Petra Steinke Niranjan D. Chatterjee 《Contributions to Mineralogy and Petrology》1984,87(2):196-204
Three Al-Cr exchange isotherms at 1,250°, 1,050°, and 796° between Mg(Al, Cr)2O4 spinel and (Al, Cr)2O3 corundum crystalline solutions have been studied experimentally at 25 kbar pressure. Starting from gels of suitable bulk
compositions, close approach to equilibrium has been demonstrated in each case by time studies.
Using the equation of state for (Al, Cr)2O3 crystalline solution (Chatterjee et al. 1982a) and assuming that the Mg(Al, Cr)2O4 can be treated in terms of the asymmetric Margules relation, the exchange isotherms were solved for Δ G
*,
and
. The best constrained data set from the 1,250° C isotherm clearly shows that the latter two quantities do not overlap within
three standard deviations, justifying the choice of asymmetric Margules relation for describing the excess mixing properties
of Mg(Al, Cr)2O4 spinels. Based on these experiments, the following polybaric-polythermal equation of state can be formulated:
, P expressed in bars, T in K, G
m
ex
and W
G,i
Sp
in joules/mol.
Temperature-dependence of G
m
ex
is best constrained in the range 796–1,250° C; extrapolation beyond that range would have to be done with caution. Such extrapolation
to lower temperature shows tentatively that at 1 bar pressure the critical temperature, T
c, of the spinel solvus is 427° C, with dTc/dP≈1.3 K/kbar. The critical composition, X
c, is 0.42
, and changes barely with pressure.
Substantial error in calculated phase diagrams will result if the significant positive deviation from ideality is ignored
for Al-Cr mixing in such spinels. 相似文献
5.
6.
Reservoirs have to be released when repairing of the dams is necessary. In 1995, two reservoirs in Baden-Württemberg (Germany) of similar age and volume (Lake Herrenbach near Göppingen, 1.0 Mio. m3 and Lake Breitenau near Heilbronn, 2.3 Mio. m3) were emptied. This allowed the singular possibility to investigate the effects of drainage and refilling on the limnochemistry and the phytoplankton biocoenosis of such artificial lakes.Before the drainage of the reservoirs, both lakes showed phosphorus release from the sediment during summer stagnation. Phosphorus values of Lake Herrenbach were regularly higher than those of Lake Breitenau (Lake Herrenbach 88 μg/l, Lake Breitenau 33 μg/l). During release, both lakes indicated higher phosphorus and chlorophyll concentrations as well as rising biomasses. Remarkable differences were observed during refilling of the reservoirs: while Lake Herrenbach showed higher transparency and lower phosphorus concentrations, Lake Breitenau progressed towards eutrophication (total phosphorus during summer 1996: Lake Herrenbach 30 μg/l, Lake Breitenau 55 μg/l). One reason for the reaction of Lake Breitenau was the reduced ground drainage during the refilling, which caused an accumulation of nutrients in the hypolimnion. Another reason was the mineralisation of vegetation which covered great parts of the dry lake sediment. The limnological change of Lake Herrenbach was not as clear but could be caused by the restauration of the pre-reservoir which was drainaged and dredged before the emptying of the main reservoir started as well as many other facts which differed Lake Herrenbach from Lake Breitenau. 相似文献
7.
The Little Ice Age climate of New Zealand reconstructed from Southern Alps cirque glaciers: a synoptic type approach 总被引:2,自引:1,他引:1
Andrew Lorrey Nicolas Fauchereau Craig Stanton Petra Chappell Steven Phipps Andrew Mackintosh James Renwick Ian Goodwin Anthony Fowler 《Climate Dynamics》2014,42(11-12):3039-3060
Little Ice Age (LIA) austral summer temperature anomalies were derived from palaeoequilibrium line altitudes at 22 cirque glacier sites across the Southern Alps of New Zealand. Modern analog seasons with temperature anomalies akin to the LIA reconstructions were selected, and then applied in a sampling of high-resolution gridded New Zealand climate data and global reanalysis data to generate LIA climate composites at local, regional and hemispheric scales. The composite anomaly patterns assist in improving our understanding of atmospheric circulation contributions to the LIA climate state, allow an interrogation of synoptic type frequency changes for the LIA relative to present, and provide a hemispheric context of the past conditions in New Zealand. An LIA summer temperature anomaly of ?0.56 °C (±0.29 °C) for the Southern Alps based on palaeo-equilibrium lines compares well with local tree-ring reconstructions of austral summer temperature. Reconstructed geopotential height at 1,000 hPa (z1000) suggests enhanced southwesterly flow across New Zealand occurred during the LIA to generate the terrestrial temperature anomalies. The mean atmospheric circulation pattern for summer resulted from a crucial reduction of the ‘HSE’-blocking synoptic type (highs over and to the west of NZ; largely settled conditions) and increases in both the ‘T’- and ‘SW’-trough synoptic types (lows passing over NZ; enhanced southerly and southwesterly flow) relative to normal. Associated land-based temperature and precipitation anomalies suggest both colder- and wetter-than-normal conditions were a pervasive component of the base climate state across New Zealand during the LIA, as were colder-than-normal Tasman Sea surface temperatures. Proxy temperature and circulation evidence were used to corroborate the spatially heterogeneous Southern Hemisphere composite z1000 and sea surface temperature patterns generated in this study. A comparison of the composites to climate mode archetypes suggests LIA summer climate and atmospheric circulation over New Zealand was driven by increased frequency of weak El Niño-Modoki in the tropical Pacific and negative Southern Annular Mode activity. 相似文献
8.
9.
Brendon Blue Claire Gregory Kiely McFarlane Marc Tadaki Petra van Limburg‐Meijer Nick Lewis 《New Zealand geographer》2012,68(1):62-66
The fair and effective governance of freshwater is an increasingly prominent issue in New Zealand. Emerging from a complex of cultural, economic and biophysical narratives, freshwater geographies are multiple, varied and increasingly acknowledged as worthy of interdisciplinary scrutiny. In this commentary, we reflect on a series of generative spaces that we – as group of postgraduate geographers (plus supporting staff) – created to engage with the multiplicity of freshwater meanings both within and beyond the academy. Through this evolving epistemic‐political project, we significantly reframed our own understandings about what freshwater ‘is’ and how it ought to be governed. By pursuing a deeper understanding of how the world gets made, we expand our ability to know and make it differently. 相似文献
10.
The long-term ice record (from 1964 to 2008) of an Arctic lake in northern Europe (Lake Kilpisj?rvi) reveals the response of lake ice to climate change at local and regional scales. Average freeze-up and ice breakup occurred on 9 November and 19 June, respectively. The freeze-up has been significantly delayed at a rate of 2.3 d per decade from 1964 onward (P?<?0.05). No significant change has taken place in ice breakup. Annual average ice thickness has become smaller since the mid-1980s (P?<?0.05). Air temperature during the early ice season significantly affected the ice thickness. The freeze-up date exhibits the highest correlation with the 2-month average daily minimum air temperature centered at the end of October, while the ice breakup date exhibits the highest correlation with the 2-month average daily maximal air temperature centered in mid May. A 1°C increase in the surface air temperature corresponds to a freeze-up later by 3.4?days and an ice breakup earlier by 3.6?days. Snow cover is a critical factor in lake-ice climatology. For cumulative November to March precipitation of less than 0.13?m, the insulating effect of the snow dominated, while higher rates of precipitation favored thicker ice due to the formation of snow ice. Variations in ice records of Lake Kilpisj?rvi can serve as an indicator of climate variations across the northern Europe. The North Atlantic Oscillation (NAO) does not significantly affect the ice season there, although both the local air temperatures and winter precipitation contain a strong NAO signal. 相似文献