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α谱法测定低微量铀、钍含量的研究 总被引:1,自引:0,他引:1
Alpha-spectrometric technique is described as an independent method of determining micro-content of U^233 and Th^233. This method is based on the comparison of U^234 and Th^233 alpha spectral activity in geological samples with U^232 and Th^233 spectral activity contributed by the spike of known concentration. The experiment procedure consists in dissolving fine powdered sample with acid and adding a given amount of U^232-Th^223 spike. The uranium and thorium are then separated by ion exchange. After purification each fraction is mounted on a separate stainless steel disk for measurement by alpha spectrometer which consist essentially of a surface barrier deterctor and a low noise amplification system connected to a multichannel analyser. After correcting for background, tail and other factors, the desired U^232 and Th^232 concentrations can be calculated. The data obtained by the alpha-spectrometric method using U^232-Th^223 spike are compared with colorimetric determination. Excellent agreement is obtained between the two sets of results. The coefficient of correlation is about 0.98 for U^234 and 0.97 for Th^232. The accuracy of uranium and thorium analyses by this method depends primarily upon the counting statistics of U^233, U^232, Th^233 and Th^223 and, to a lesser extent, upon the calibration of U^233-Th^238 spike. Errors of uranium and thorium concentration by this method are generally 2 to 5 per cent. 相似文献
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夏季金塔绿洲及邻近沙漠地面风场、气温和湿度场特性的对比分析 总被引:3,自引:4,他引:3
利用2004年7~8月金塔“绿洲系统能量与水分循环过程观测与数值研究”观测试验期间的资料,对比分析了金塔绿洲及邻近沙漠地面风场和空气温湿特性的水平差异。结果表明:绿洲及邻近沙漠的温湿和风速差异明显,绿洲内部冷湿风弱,而外部干热风稍大;绿洲内的温湿场为非对称结构,冷湿中心偏离绿洲的几何中心,在绿洲东部,当地盛行风向的上风方位置上;而风速场结构对称,弱风中心与绿洲的几何中心一致;在不同的风向时空气比湿有较大的差异,存在明显的来自东北方沙漠戈壁的干平流和来自西南方水库及绿洲的湿平流。 相似文献
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