罗子沟盆地有机质热演化对砂岩物性的改造作用

基于岩石薄片观察、压汞分析、扫描电镜和X衍射分析等方法对罗子沟盆地大砬子组砂岩物性特征进行了定性-定量研究。结果表明：罗子沟盆地大砬子组砂岩成分成熟度和结构成熟度低,以岩屑长石砂岩和长石砂岩为主;岩石孔隙度高,孔隙度主要为16.2%~26.4%,次生孔隙占总孔隙度面孔率的88%,但总体渗透率极低,渗透率主要分布在（0.13~1.68）×10^-3 μm²,为高孔特低渗的物性特征。有机元素分析、色谱分析、岩石热解及显微组分镜检分析表明,罗子沟盆地大砬子组泥页岩中有机质在热演化过程中产生大量有机酸,有机酸对砂岩中长石等矿物的溶蚀作用是次生孔隙发育的主要原因,但有机酸溶蚀产生的次生矿物在一定程度上堵塞了孔隙喉道。因此,研究区砂岩形成高孔特低渗的物性特征。     

广州红砂岩文物保护新方法

当前环境污染日益严重,不少珍稀石质文物因缺少保护而遭受严重风化。为保护风化石质文物,文章将纳米材料和传统石质文物保护剂相结合,提出一种新的保护方法：用纳米二氧化钛银与NS-系列文物水性保护剂按一定比例调和,涂抹于红砂岩文物表面;一段时间后在其表面喷洒NS-系列文物水性保护剂。为检验新方法之功效,分别用该方法和NS-系列文物水性保护剂处理采自于广州的红砂岩文物样品,用高效液相色谱仪测定其有机酸种类和质量分数,发现前者较后者的有机酸质量分数明显减少。又经实验检测,发现该方法处理后的样品能经受水流冲刷,能耐酸碱腐蚀。这表明新方法既能防水、耐酸碱,又能降解有机酸;可以有效延缓石质文物风化,较传统石质文物保护剂具有更好的保护效果。     

泥质砂岩液相渗透率计算新方法

液相渗透率描述了岩石的渗流特性,是评价储层与预测油气产能的重要参数.液相渗透率是指盐水溶液在岩石孔隙中流动且与岩石孔隙表面黏土矿物发生物理化学作用时所测得的渗透率;液相渗透率的实验测量条件更加接近实际地层泥质砂岩的条件,使得液相渗透率更能反映地层条件下泥质砂岩的渗流特性;然而,现有的液相渗透率评价模型较少,且模型未能揭示液相渗透率与溶液矿化度之间的关系.基于此,开展了液相渗透模型推导与计算方法研究;文中首先将岩石等效为毛管束模型,推导建立了液相渗透率与比表面、喉道曲折度、总孔隙度、黏土束缚水孔隙度等参数之间的关系;其次,根据岩石物理体积模型,推导建立了黏土束缚水孔隙度与阳离子交换容量、溶液矿化度等参数的关系;最终,将黏土束缚水孔隙度引入液相渗透率计算公式,建立了基于总孔隙度、阳离子交换容量、溶液矿化度、比表面、喉道曲折度等参数的液相渗透率理论计算模型.液相渗透率计算模型与两组实验数据均表明,液相渗透率随阳离子交换容量的增大而降低,随溶液矿化度的增大而增大.然而,液相渗透率理论计算模型的实际应用中喉道曲折度、比表面等参数求取困难,直接利用理论模型计算液相渗透率受到限制.在分析液相渗透率与孔隙渗透率模型的基础上,建立了液相渗透率与空气渗透率之间的转换模型,形成了利用转化模型计算液相渗透率的新方法.为进一步验证液相渗透率与空气渗透率转化模型的准确性,基于两组实验数据,利用转换模型计算了液相渗透率;液相渗透率计算结果与岩心测量液相渗透率实验结果对比显示,液相渗透率计算结果与实际岩心测量结果吻合较好,文中建立的液相渗透率与空气渗透率转化模型合理可靠.     

含流体砂岩地震波频散实验研究

为了研究孔隙流体对不同渗透率岩石地震波速度的影响,在实验室利用跨频带岩石弹性参数测试系统得到了应变幅值10-6的2~2000Hz频段下的地震波速度和1 MHz频率下的超声波速度,利用差分共振声谱法得到了频率600Hz岩石干燥和完全饱水情况下岩石声学参数.实验表明,在低饱和度下,致密砂岩在地震和超声频段下没有明显的频散;在高饱和度下纵波速度的频散变得明显.从干燥到完全水饱和条件,不同频率测量的致密砂岩的体积模量随岩石孔隙度增高而降低,且体积模量的变化量受岩石微观孔隙结构的影响较大.高孔、高渗砂岩无论在低含水度下还是在高含水饱和度下频散微弱,并且在地震频段下围压对于岩石纵横波速度的影响要大于频率的影响.高孔、高渗砂岩和致密砂岩不同含水饱和度下的频散差异可应用于储层预测,油气检测等方面,同时该研究可以更好地帮助理解岩石的黏弹性行为,促进岩石物理频散理论的发展,提高地震解释的精度.     

REE地球化学在砂岩型铀成矿研究中的应用--以川北砂岩型铀矿床为例

本文在系统的取样分析基础上,总结了川北砂岩型铀矿床的稀土元素地球化学特征,分析研究了围岩、矿石、方解石脉和铀矿物的稀土元素组成、关系,讨论了岩、矿石沉积和成岩过程的稀土元素变化规律,与国内外典型的火山岩型和变质岩型热液成因铀矿床进行了对比,认为川北砂岩型铀矿具有热液（水）改造成矿作用的稀土元素地球化学特征,铀矿化经历了沉积成岩和热液改造富集两个阶段,为砂岩型铀矿成矿研究提供了新的思路。     

Seismic stratigraphy and hydrocarbon prospectivity of the Lower Cretaceous Knurr Sandstone lobes along the southern margin of Loppa High,Hammerfest Basin,Barents Sea

The Lower Cretaceous Knurr Sandstone deposited along the southern slope of Loppa High and overlain by the Kolje and Kolmule seals forms an attractive play in the Hammerfest Basin of the Barents Sea. Late Jurassic organic-rich Hekkingen shale directly underlies the Knurr Sandstone and acts as a source to provide effective charge. Three wells, 7120/2-2, 7122/2-1 and 7120/1-2, have proven the Knurr-Kolje play in structural traps, with an oil discovery in 7120/1-2. Prospectivity related to stratigraphic traps is, however, highly under-explored.In order to document and map the reservoir distribution and stratigraphic-trap fairway, the Lower Cretaceous sedimentary package containing the Knurr Sandstone is divided into a number of depositional sequences and systems tracts using key regional seismic profiles calibrated with logs. Mapping of the key surfaces bounding the Knurr sandstone has been carried out using all the seismic vintages available from Norwegian Petroleum Directorate (NPD).The thick massive nature of the sandstone (123 m in well 7122/2-1), sedimentary features characteristic of gravity flow deposits, high-resolution internal seismic reflections and stratal geometries (truncations and lapout patterns), and sequence stratigraphic position of the Knurr Sandstone on seismic profiles confirm that the lobes identified on the seismic section are gravity driven base of the slope lobes. These Knurr lobes and slope aprons were formed as a result of uplift of the Loppa paleo-high in the Late Jurassic to Early Cretaceous times which caused subaerial exposure and incision. The characteristic mounded, lobate geometry evident on the seismic can be mapped along the toe-of-slope and records multiple stacked lobes fed by multiple feeder canyons. Lateral partitioning and separation of the lobes along the toe-of-slope could potentially create stratigraphic traps. The existing 2D seismic coverage is, however, not sufficient to capture lateral stratigraphic heterogeneity to identify stratigraphic traps. 3D seismic coverage with optimum acquisition parameters (high spatial and vertical resolution, appropriate seismic frequency and fold, long offsets and original amplitudes preserved) can allow for the reconstruction of 3D geomorphologic elements to de-risk potential stratigraphic traps prior to exploratory drilling.     

In situ stress field evaluation of deep marine tight sandstone oil reservoir: A case study of Silurian strata in northern Tazhong area,Tarim Basin,NW China

Deep marine tight sandstone oil reservoirs are the subject of considerable research around the world. This type of reservoir is difficult to develop due to its low porosity, low permeability, strong heterogeneity and anisotropy. A marine tight sandstone oil reservoir is present in the Silurian strata in the northern Tazhong area of the Tarim Basin, NW China, at a depth of more than 5000 m. The porosity is between 6% and 8%, and the gas permeability is between 0.1 and 1 × 10⁻³ μm². The features of this type of reservoir include the poor effects of conventional fracturing modifications and horizontal wells, which can lead to stable and low levels of production after staged fracturing. Here, we conduct a comprehensive evaluation of the mechanical properties of the rock and the in situ stress of the target tight sandstones by using numerous mechanical and acoustic property tests, conducing crustal stress analysis and using data from thin section observations. The dispersion correction technique is used to transform velocity at the experimental high frequency (1 MHz) to velocity at the logging frequency (20 kHz). The logging interpretation models of the transverse wave offset time, mechanical parameters and in situ stress are calculated, and each model represents a high precision prediction. Simulating the in situ stress field of the Silurian strata using a three-dimensional finite element method demonstrates that the average error between the simulation result and the measured value is less than 6%. The planar distribution of each principal stress is mainly controlled by the burial depth and fault distribution. By conducting in situ stress orientation analysis for the target layer via the analysis of paleomagnetism, borehole enlargement, fast shear wave orientation and stress field simulation, we show that the direction of the maximum horizontal stress is N45E. In this paper, a typical and successful comprehensive evaluation of the stress field of the deep tight sandstone oil reservoir is provided.     

Utility of GOI,QGF, and QGF-E for interpreting reservoir geohistory and oil remigration in the Hudson oilfield,Tarim basin,northwest China

The physical mechanisms responsible for hydrocarbon migration in carrier beds are well understood. However, secondary migration is one of poorly understood facets in petroleum system. The Carboniferous Donghe sandstone reservoir in the Tarim Basin's Hudson oilfield is an example of a secondary (or unsteady) reservoir; that is, oil in this reservoir is in the process of remigration, making it a suitable geologic system for studying hydrocarbon remigration in carrier beds. Experimental methods including grains containing oil inclusions (GOI), quantitative grain fluorescence (QGF) and quantitative grain fluorescence on extract (QGF-E) -- together with the results from drilling, logging and testing data -- were used to characterize the nature of oil remigration in the Donghe sandstone. The results show that (1) significant differences exist between paleo- and current-oil reservoirs in the Donghe sandstone, which implies that oil has remigrated a significant distance following primary accumulation; (2) due to tectonic inversion, oil remigration is slowly driven by buoyancy force, but the oil has not entered into the trap entirely because of the weak driving force. Oil scarcely enters into the interlayers, where the resistance is relatively large; (3) the oil-remigration pathway, located in the upper part of the Donghe sandstone, is planar in nature and oil moving along this pathway is primarily distributed in those areas of the sandstone having suitable properties. Residual oil is also present in the paleo-oil reservoirs, which results in their abnormal QGF-E. A better understanding of the characteristics of oil remigration in the Donghe sandstone in the Hudson oilfield can contribute to more effective oil exploration and development in the study area.     

致密砂岩储层流体参数核磁共振实验研究

利用核磁共振技术对致密砂岩储层岩心流体参数进行研究,简述致密砂岩储层流体参数核磁共振测量原理及计算岩心流体参数方法。实验确定了岩心流体动用参数T2截止值方法,进行了可动流体致密砂岩储层分类评价研究。油田矿场核磁共振测量岩心含油饱和度、可动流体饱和度,并对可动流体饱和度、含油饱和度识别油水层方法进行研究。表明:实验测定红河区块岩心T2截止值为4.06ms,利用致密砂岩储层岩心可动流体等级划分标准,对致密砂岩储层岩心单井及不同层位、多井之间进行储层比较分类评价。油田矿场核磁共振技术测量计算的含油饱和度结果与常规方法测量的含油饱和度结果对比,表明油田矿场核磁测量含油饱和度是可行且可靠的。岩心含油饱和度与可动流体饱和度比值大小可识别油水层。      

基于匹配追踪的瞬时能量异常属性在Albertine地堑油气预测中的应用

东非裂谷Albertine地堑是当今世界油气勘探的热点地区之一,具有埋藏浅、演化快、地层新的地质特点。作为主力含油气层段的新生代地层中疏松砂岩异常发育,物性参数差异较大,受控于孔隙度以及孔隙流体的综合影响,含油气储层的地震响应无明显规律,油气预测难度较大。基于能量吸收分析思想的指导,在利用匹配追踪时频分解方法有效提高时频分辨率的前提下,进一步提出瞬时能量异常属性的计算方法。以Albertine地堑的W油田为例,针对含油气储层表现的低频能量增加、高频能量衰减的异常特征,借助瞬时能量异常属性实现了油气预测,预测结果获得了钻井的验证。