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101.
硅酸盐样品微波加热碱熔分解方法   总被引:1,自引:0,他引:1  
本文研究了硅酸盐样品在常压下,用微波炉进行碱熔分解的熔样时间,试剂用量和滴加水量等情况对分解的影响,确定了最佳实验条件,将此法用于地球化学标准参考样品SiO2的测定,取得了满意的结果。  相似文献   
102.
多尺度分解在地震信号处理中的应用   总被引:1,自引:0,他引:1  
陈飞  赵永  刘阳  周云好 《中国地震》2004,20(4):405-409
利用小波分析中的多尺度分解及信号消噪技术,对记录不清、信噪比小、震相无法辨认的地震信号进行处理。结果表明:多尺度分解在弱震信号提取和弱震相的识别等方面有很好的效果。  相似文献   
103.
金矿样品的几种溶样方法   总被引:4,自引:0,他引:4  
通过王水、封闭和烧杯敞口及聚乙烯溶样瓶封闭溶样等方法,对含Au矿样的试样分解、溶样体系及各种溶样方法的对比表明,利用聚乙烯溶样瓶,采用HNO3 NaCl KMnO4 NH4HF2溶样体系,在水浴锅中封闭溶样40min,矿样中的Au即可完全分解。经国家标准物质分析验证,结果与标准值相符。封闭溶样可以避免样品外溢、进溅,使分析结果更准确可靠,降低成本,减少环境污染,适用于大批量样品分析。  相似文献   
104.
贵州百花湖分层晚期有机质降解过程与溶解N2O循环   总被引:7,自引:0,他引:7       下载免费PDF全文
百花湖是一个具有季节性分层的富营养小型湖泊,在秋季湖水倒转期经常发生水质恶化事件,碳氮循环出现异常。文章研究特选择在秋初,湖泊分层开始消失时,测定了湖水中不同深度的N2O,CH4,CO2,有机和无机碳同位素以及其他化学参数变化。结果发现:采样时百花湖在约6m和16m深度附近出现了两个温度不连续层(SDL和PDL),并影响到有机颗粒的沉降和分解。相对而言,有较多的有机质在这两个层内发生降解,但降解的途径有所不同,上部主要是有氧降解,下部则主要是无氧降解过程。N2O的产生和消耗与有机质的降解过程完全对应:PDL层以上,ΔN2O与AOU的线性关系反映了N2O主要形成于硝化作用;PDL层以下反硝化作用导致N2O严重不饱和;PDL内位于硝化作用和反硝化作用过渡带的N2O峰,显然是硝化与反硝化联合作用的结果。PDL层内较大的CH4浓度变化梯度,说明嗜甲烷细菌可能通过氧化NH+4贡献了部分N2O。百花湖秋、冬季表层湖水N2O都是过饱和的,都是大气N2O的源,依据分子扩散模型计算湖泊N2O的释放通量在12~14μmol/m·day之间,秋、冬季没有明显的差别。秋季底层湖水的反硝化作用是湖泊N2O的汇,其消耗通量与表层的释放通量基本相当。  相似文献   
105.
In order to clarify the relationship between microscopic and macroscopic magnetic features of a rock, we applied magnetic force microscopy (MFM) as a local probe on a sample with an intense natural remanent magnetisation, a norite from Heskestad, Norway. We studied in detail seven magnetite (Fe3O4) exsolution lamellae, five of them were about 30 μm long and a few micrometers wide, two were significantly shorter; all were located in their natural host, a grain of clinopyroxene. By combining MFM images of surface magnetisation with information about shape observed with optical microscopy (OM), the internal domain structure was determined for individual grains. In general, the lamellae were pseudo-single-domain grains with open-flux domain magnetisations parallel to their long axes. The domain sizes were, in cross-section, on the order of a micrometer for the longer lamellae and about 300 nm for the short lamellae. By increasing the separation between the MFM probe and the exposed end of the lamellae, information could be obtained about the decrease in stray fields for the individual grains. Close to the lamellae, stray fields were significant even for grains with multiple domains. The largest fields were found above the largest domains. A separation of approximately one domain width was found to be a characteristic distance, where stray fields from adjacent domains begin to cancel one another.  相似文献   
106.
After the 1995 Kobe earthquake, the expressway structures in Japan were retrofitted and they will not now be seriously damaged under a certain level of strong earthquake motion. However, the stability of a moving vehicle has not been investigated yet. It has been reported that drivers feel seismically induced vibrations, especially in the transverse direction of vehicles. Owing to this phenomenon, drivers have some difficulty in controlling the vehicles during strong shaking. For further safety promotion of the expressway networks, it is important to understand the drivers' reactions to seismic motion. The present authors have performed a series of seismic response analyses of a moving vehicle to investigate its response characteristics based on numerical simulation. However, the responses of the driver were not considered in the simulation process. In order to investigate the drivers' reactions during an earthquake, a series of virtual tests were conducted using a driving simulator. This driving simulator has six servomotor‐powered electric actuators that control its motions. Several types of tests were carried out for different examinees to investigate drivers' responses while controlling the simulator under seismic motion. The results of this study showed that a larger response time lag to strong shaking and over turning of the steering wheel may shift the vehicle into the next lane. According to this finding, trafficaccidents could possibly occur under strong ground shaking in the case of heavy traffic. Copyright © 2004 John Wiley & Sons, Ltd.  相似文献   
107.
Two approximate methods for decomposing complicated inelastic dynamic responses of wall buildings into simple modal responses are presented. Both methods are based on the equivalent linear concept, where a non‐linear structure is represented by a set of equivalent linear models. One linear model is used for representing only one vibration mode of the non‐linear structure, and its equivalent linear parameters are identified from the inelastic response time histories by using a numerical optimizer. Several theoretical relations essential for the modal decomposition are derived under the framework of complex modal analysis. Various numerical examinations have been carried out to check the validity of the proposed modal decomposition methods, and the results are quite satisfactory in all cases. Fluctuating bending moment and shear at any location along the wall height contributed by each individual vibration mode can be obtained. Modal contributions to shear and flexural strength demands, as well as the corresponding modal properties, under various seismic loading conditions can also be identified and examined in detail. Furthermore, the effects of higher vibration modes on seismic demands of wall buildings are investigated by using the modal decomposition methods. Several new insights into the complicated inelastic dynamics of multi‐story wall buildings are presented. Copyright © 2004 John Wiley & Sons, Ltd.  相似文献   
108.
Seepage driving effect on deformations of San Fernando dams   总被引:2,自引:0,他引:2  
In the process of flow deformation of an earth dam, the seepage force inside the dam plays a role as a driving force. The seepage force acts just like the gravitational force in terms of pushing soils away from their original locations after liquefaction is triggered. This paper draws attention to this seepage driving effect by presenting a set of fully coupled finite element analyses on the well-known San Fernando dams, with the objective of evaluating the impact of this seepage effect. The results indicate that while this effect is always there, its practical significance depends on a number of factors. In the case of the upper San Fernando dam, which experienced a significant, but restricted, downstream movement during the 1971 earthquake, the seepage driving effect was indeed significant. On the contrary, for the lower dam, which failed and slid into the upstream reservoir during the same earthquake, this seepage effect was relatively less pronounced. The detailed results of the analyses reveal the likely mechanisms of failure and deformation of the two dams and the likely cause behind the difference between their responses during the earthquake.  相似文献   
109.
基于小波分解的西太平洋副热带高压模糊推理预测   总被引:3,自引:2,他引:3  
基于NCEP/NCAR再分析资料,讨论了西太平洋副高脊线与其前期位置的相互关系,并在此基础上用小波分解和自适应模糊推理方法,对副高脊线进行集成建模和预测.基于小波分解重构的副高脊线短期活动集成预测结果表明,该方法可有效降低预报难度,明显改进和提高了副高脊线短期活动的预报准确率.  相似文献   
110.
考虑渗流力时对太沙基一维固结理论的修正   总被引:3,自引:2,他引:3  
吴雄志 《岩土力学》2004,25(8):1279-1282
考虑渗流力的作用,对太沙基一维固结理论进行了修正,给出了向上及向下渗流时固结度的表达式,并分析了固结过程中渗流应力的变化规律。结果表明:渗流力对固结度的影响较大,特别是在时间因素Tv=0.1附近,是否考虑渗流力的影响将导致固结度的差值达30 %,因而渗流力对固结度的影响是不可忽略的。  相似文献   
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