Application of the luciferase cell culture bioassay for the detection of refined petroleum products

A luciferase cell culture-based bioassay, developed to detect 2,3,7,8-tetrachlorodibenzo-p-dioxin (TCDD)-like activity of halo-genated and polycyclic aromatic hydrocarbons, was optimized to detect refined petroleum products and to determine their relative inducing potency. Quality control standards from 32 refined products (gasolines and diesels, jet fuels, lubricating oils, fuel oils and weathered products) and three commercial products were evaluated. Induction equivalents (I-EQs) were determined by direct comparison of the EC50 and EC20 values (based on the median and 20% TCDD maximal response, respectively) from dose-response curves for each product to those obtained with TCDD. Most petroleum products were active in the luciferase bioassay, with those products composed of fractions produced later in the distillation process (i.e. fuel oils) inducing higher levels. Additionally, weathering of products reduced their induction potency. Based on the high I-EQ estimates of many products, biological effects associated with exposure may have been previously underestimated using other diagnostic methods.     

A UT1-Like Quantity from Analysis of GPS Orbit Planes

This paper discusses a UT1-like quantity, UTGPS, determined daily from Earth-referenced GPS satellite orbits from the International GPS Service (IGS). For each satellite considered, the observed relation between the satellite's IGS orbit and a model of its orbit plane in inertial space is used to estimate UT1. This modeled orbit plane is initialized using the satellite's IGS orbit and the actual UT1 at an initial time. It is then propagated using standard models of gravitational forces and an empirical model representing the orbit-normal radiation pressure observed during several years of in-flight experience with the satellite. To estimate UT1, an a-priori transformation from terrestrial to true-of-date celestial coordinates is applied to the satellite's IGS orbit. The geocentric angular deviations of points of the resulting transformed orbit from the modeled orbit plane are analyzed, giving the angle between the ascending nodes of the satellite's transformed and modeled orbit planes. To this observed angle between nodes, converted to a UT1 difference, is added the a-priori UT1 value used in the transformation. From the result is subtracted a model of the angle, again converted to a UT1 difference, between the ascending nodes of the actual and modeled orbit planes. The final result is the estimate of UT1 from this satellite, and the median of the UT1 estimates from all satellites considered is UTGPS. The root-mean-square difference between UTGPS-UT1 at the beginning and at the end of an interval of one to four weeks is approximately 30 s times the square root of the interval's duration in weeks.This revised version was published online in October 2005 with corrections to the Cover Date.     

青藏高原比如地体与措勤地体相对古构造位置判别

本文采用蚀源区判别图解QFL和QpLsLv、微量元素图解Th -Co -Zr/10、常量元素图解K2O/Na2O -SiO2 和野外地质实测剖面等方法 ,对比如、措勤地体的构造演化进行了分析。发现并证实了在T3-J1 以前比如地体位于措勤地体的北部 :J2 -3 时随着班—恕缝合带的拉张 ,比如地体开始右旋向东滑动 :一直延续到J3-K1 时 ,班—怒缝合带闭合 ,比如地体才就位于目前位置。最后应用1/ZTR指数推测了比如地体在J2 -3 时滑移点的大致位置 (E90°49,N31°34)。     

中国与蒙古之地质

东昆仑中部缝合带清水泉一带发育石榴斜长紫苏麻粒岩、紫苏辉石黑云母石榴子石麻粒岩、石榴二辉斜长麻粒岩和石榴单斜辉石麻粒岩,它们与混合岩化黑云母石榴子石变粒岩、黑云母辉石变粒岩、石墨大理岩、含透辉石透闪石大理岩、透辉石大理岩、黑云斜长角闪岩和片麻岩等高级变质岩系以及纯橄岩、辉橄岩、橄长岩、辉长岩、辉绿岩和玄武岩等共同构成蛇绿混杂岩。麻粒岩相变质作用的温压条件为T=760~880℃,p=830~1200MPa,为高温中高压麻粒岩相变质作用,估算其形成深度为40~45km。麻粒岩相变质作用的SHRIMP锆石U-Pb年龄为(507·7±8·3)Ma。清水泉地区蛇绿岩形成于~520Ma,到~508Ma时俯冲至地下40~45km深处而发生中高压麻粒岩相变质作用,然后发生构造折返而剥露至地表。证实了清水泉高级变质岩和基性—超基性岩片是形成于早—中寒武世的蛇绿混杂岩,标志一个古生代早期的非常重要的板块汇聚边界,这对于进一步研究东昆仑造山带构造演化、乃至中国西部大地构造格局具有非常重要的意义。     

1-（4-硝基苯基）-3-（3，5-二溴吡啶）三氮烯的合成及其与镍的显色反应

合成了1-(4-硝基苯基)-3-(3,5-二溴吡啶)三氮烯(NPDBPDT),并研究了NPD-BPDT与镍的显色反应。在pH 10.0的Na2B4O7-NaOH缓冲溶液介质中,表面活性剂Triton X-100存在下,镍与试剂生成摩尔比为1∶4的络合物在470 nm处有最大正吸收峰,表观摩尔吸光系数为1.02×105L.mol-1.cm-1;在540 nm处有最大负吸收峰,表观摩尔吸光系数为1.15×105L.mol-1.cm-1;以540 nm为参比波长、470 nm为测量波长进行双波长测定,表观摩尔吸光系数为2.17×105L.mol-1.cm-1。镍含量在0~480μg/L内符合比尔定律。方法用于合金样品中镍的测定,结果与原子吸收法相符,加标回收率为98.0%~102.0%;精密度小于5%(RSD,n=6)。     

塔中地区卡塔克1区块东河砂岩地震储层预测研究

采用基于地震波形分类的地震相分析与沉积相解释、波阻抗约束稀疏脉冲反演、地震多属性储层预测及油气检测等针对岩性油气藏的储层地震预测技术，从塔中地区卡塔克1区块泥盆系东河砂岩储层的生储盖组合条件及相关的地震地质特点出发，利用卡1三维地震资料开展目的层系的目标精细解释，结合已有的钻探、测井和测试等资料，揭示了东河砂岩储层砂体的空间展布特征，圈定出砂岩发育带，并对有利储层段的潜在含油气性进行了综合预测和评价。     

灰色理论应用于轨道交通一号线一期工程承重墩沉降分析

介绍了沉降监测数据处理理论方法,讨论了灰色模型法预测沉降的过程,分析了武汉轨道交通一期工程承重墩沉降监测数据,结果表明其基础是基本稳定的。     

可数背景状态下QBD过程的平稳分布尾渐近态

考虑在可数背景状态下，时间离散的拟生灭过程（QBD过程）平稳分布的尾概率的渐近态。通过对QBD过程某些条件的限定，应用马尔可夫更新定理，得出在一定合理的条件下，当水平趋于无穷时的尾概率的几何衰变。通过初等方法，将该结论应用于时间离散的加入最短队模型。     

集均衡;;汇集干扰;;屏蔽介绍了临钢

,CATV of Lingfen Iron and Steel Company,Lingfen Shanxi 041000,China)This article introduces the design idea and experiences in innovating process of bi-directional HFC network,the design ideas of light pitch point,the optical cable skeleton line and the assignment network.Also the     

惠州市1：5000卫星正射影像图测绘工程研究

我国利用IKONOS卫星影像制作1:5000正射影像图主要是集中在研究领域。惠州市国土资源局于2004年2月利用IKONOS卫星影像制作覆盖惠州市辖区1．2万平方公里的1:5000正射影像图,项目由广东省国土资源信息中心承担。大面积的测区利用IKONOS卫星制作1: 5000正射影像图在国内还属首次。本文探讨该测绘工程的实施技术及质量控制方法。