RP-HPLC法同时测定翅碱蓬中四种黄酮化合物的含量

建立RP-HPLC(反相高效液相色谱法)同时测定翅碱蓬中四种黄酮化合物-芸香苷、槲皮素3-β-D-葡萄糖苷、水仙苷和槲皮素的含量。采用Kromasil C18色谱柱(4.6 mm×250 mm,5μm),检测波长为361nm,柱温为30℃,流动相为甲醇-0.4%冰乙酸(55︰45),流速1.0mL/min,四种黄酮类化合物得到很好的分离。芸香苷、槲皮素3-β-D-葡萄糖苷、水仙苷和槲皮素浓度均为0.001~0.01 mg/mL范围内呈现良好线性关系,相关系数R2在0.9990~0.9996,加标回收率(n=3)范围为82.39%~99.03%。该方法简单、快速、高效,可以用于翅碱蓬中四种黄酮化合物的含量分析。     

《湘绮楼日记》记录的湖南长沙1877-1878年寒冬

在对清代王运所著的《湘绮楼日记》中长达40余年(1869—1916)的冬季(12月—2月)天气记录进行整理之后,从王运在湖南长沙、衡阳一带记录的30多个完整冬季之中,提取了一个特殊的寒冬——1877—1878年冬天(记录于长沙境内)。将这年的天气记录与日记中其他年份进行比较,其寒冷程度可以明显地体现在以下几个方面(1)降雪——降雪日数14天,为最多的年份之一,且降雪次数最多;(2)积雪——积雪日数在27天以上,为历年之最;(3)冰冻——根据该年日记记录,冰冻的严重程度和持续时间均超过其他年份;(4)《日记》作者感受——王运留下了大量对“寒”、“暖”的感应记录,这一年有历年最多的“寒”记录(15条)和最少的“暖”记录(0)。由此可以得出结论1877—1878年冬天是《湘绮楼日记》中所仅见的、异常寒冷的严冬。文中对这年当地冬季严寒的天气过程和气候特点进行了初步分析。     

Population,urbanization and economic scenarios over the Belt and Road region under the Shared Socioeconomic Pathways

The countries throughout the Belt and Road region account for more than 60% of the world's population and half of the global economy. Future changes in this area will have significant influences on the global economic growth, industrial structure and resource allocation. In this study, the proportion of the urban population to the total population and the gross domestic product were used to represent the levels of urbanization and economic development, respectively. The population, urbanization and economic levels of the Belt and Road countries for 2020–2050 were projected under the framework of the IPCC's shared socioeconomic pathways(SSPs), and the following conclusions are drawn.(1) The population, urbanization and economic levels in the Belt and Road region will likely increase under all five pathways. The population will increase by 2%–8%/10 a during 2020–2050 and reach 5.0–6.0 billion in 2050. Meanwhile, the urbanization rate will increase by 1.4%–7.5%/10 a and reach 49%–75%. The GDP will increase by 17%–34%/10 a and reach 134–243 trillion USD.(2) Large differences will appear under different scenarios. The SSP1 and SSP5 pathways demonstrate relatively high urbanization and economic levels, but the population size is comparatively smaller; SSP3 shows the opposite trend. Meanwhile, the economy develops slowly under SSP4, but it has a relatively high urbanization level, while SSP2 exhibits an intermediate trend.(3) In 2050, the population will increase relative to 2016 in most countries, and population size in the fastest growing country in Central Asia and the Middle East countries will be more than double. Urbanization will develop rapidly in South Asia, West Asia and Central Asia, and will increase by more than 150% in the fastest growing countries. The economy will grow fastest in South Asia, Southeast Asia and West Asia, and increase by more than 10 times in some counties with rapid economic development.     

锦州9-3油田海域环境现状及其评价

1 引言 石油,作为现代社会的主要能源,在全球经济迅速发展和人口激增的情况下,世界范围内的供求在不断增长,海洋石油勘探开发规模也在不断扩大.海洋油气开发已成为我国油气战略资源的主要来源之一.     

激发态质子转移分子2-(2'-羟基苯基)苯并噻唑溶液的全光开关效应

研究了激发态质子转移(ESPT)分子2-(2'-羟基苯基)苯并噻唑(HBT)在不同极性溶剂中的光开关行为,探讨了溶剂极性对HBT分子光开光效应的影响.揭示了光开关脉冲信号的形成原因,建立了基于光诱导HBT分子激发态非线性折射效应的皮秒全光开关的理论模型.根据对时间响应函数的理论计算和实验结果分析,确定了光开关脉冲信号下降前沿和上升后沿的形成机理以及影响因素,并提出了增强光开关信号下降前沿的关断深度,提升上升后沿的恢复速度的有效途径和方法.本文工作为制成皮秒量级关断,微秒甚至纳秒量级重新打开的快速全光开关器     

Improvement in the calculation of anti-Stokes energy transfer and experimental justification based on Er0.01YbxY1 - 0.01 - xVO4 crystal

The improvement on the calculation of anti-Stokes energy transfer rate is studied in the present work. The additional proportion coefficient between Stokes and anti-Stokes light intensities of quantum Raman scattering theory as compared with the classical Raman theory is introduced to successfully describe the anti-Stokes energy transfer. The theoretical formula for the improvement on the calculation of anti-Stokes energy transfer rate is derived for the first time in this study. The correctness of introducing coefficient exp{ΔE / kT} from well-known Raman scatter theory is demonstrated also. Moreover, the experimental lifetime measurement in Er_0.01Yb_xY_{1 - 0.01 - x}VO₄ crystal is performed to justify the validity of our important improvement in the original phonon-assisted energy transfer theory for the first time.     

锦州25—1区块探井钻井实践与认识

锦州25—1油田是渤海湾近年钻探发现的大型油田。锦州25—1区块先后钻了十多口探井,在钻井作业中遇到上部井眼扩大严重、井径不规则、井垮、起下钻遏阻卡、电测作业遏阻、电测井底沉砂较多、井漏等复杂情况。通过对锦州25—1区块前面几口探井钻井中出现的问题进行认真分析,研究了锦州25—1区块的地层压力剖面分布。经过不断的总结与措施改进后,在后面的探井钻井作业中做到了起下钻顺利,上部井径扩大率较小,未出现井垮情况,电测一次到底,钻井作业生产时间大幅度提高,为锦州25—1油田的生产井钻井积累了宝贵的经验。     

在SCOUNIX环境下开发实时通信系统

在SCOUNIX环境下开发实时系统 ,不仅可以利用UNIX的多任务特性 ,建立起高效可靠的系统 ,而且软硬件成本较低 ,还能享有商业软件的技术服务。介绍了基于SCOUNIX环境开发实时通信系统时多路串行通信技术及UDP网络通信技术的应用 ,同时介绍了在系统中如何建立数据日志及监视进程活动     

高重频激光测距数据处理方法

该文探讨了高重频激光测距工作中的数据处理问题。该数据处理采用了屏幕显示以及数学分析方法,以剔除卫星激光测距数据中的观测异常值,提取有效的数据点,并最终生成标准点数据。通过对奥地利GRAZ激光测距站高重频数据资料的处理表明,该数据处理方法是有效的。     

A preliminary research on the climatic records of lacustrine deposits of Qingtu Lake in the last 6000 years

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