Speciation analysis of metals （Tl, Cd and Pb） in Tl-containing pyrite and its cinder from Yunfu Mine, China, by ICP-MS with sequential extraction

The speciation of heavy metals such as thallium, cadmium and lead existing in pyrite and pyrite cinder was analyzed by ICP-MS with a sequential extraction procedure. The distribution patterns of these metals including exchangeable, reducible, oxidizable and residual fractions were obtained. Tl, Cd and Pb in pyrite and pyrite cinder samples from each extraction step were determined by inductively coupled plasma mass spectrometry (ICP-MS). Under the optimized instrumental conditions, detection limits of Tl, Cd and Pb in different matrices were within the range of 0.006–0.07 μg/L, and the relative standard deviations ranged from 0.8% to 1.2%. The accuracy of Tl, Cd and Pb determination was checked by analyzing two certified reference materials. The results demonstrate that trace Tl, Cd and Pb in the samples can be accurately determined. The sequential extraction results revealed that the percent contents of Tl, Cd and Pb in exchangeable, reducible and oxidizable fractions in pyrite cinder are different from those in pyrite and in pyrite cinder. Tl, Cd and Pb mostly are distributed in residual fraction. Therefore, the mobility of metals in pyrite is higher than that in pyrite cinder. Although distributions of Tl, Cd and Pb in the non-residual fraction are not dominant in pyrite cinder, the total concentrations of them could not be ignored. Consequently, attention must be paid to the risk of potential pollution by pyrite cinder.     

电感耦合等离子体发射光谱法测定海水中微量钡

研究了用ICP-AES测定海水中微量钡的方法,选取了最佳工作条件,检出限为0.003mg·L-1,RSD为0.64%～0.84%,回收率在98.2%～104%之间。该法简便、快速、准确,结果令人满意。     

电感耦合等离子体质谱分析仪简介

电感耦合等离子体质谱分析仪Inductively Coupled Plasma Mass Spectrometry（ICP—MS）是西安地质调查中心实验测试中心于2006年引进的。电感耦合等离子体质谱分析仪能适用于广泛领域的各种样品的元素分析,尤其适用于各类复杂基体的环境、食品、矿物、动植物、卫生防疫等样品中各种无机元素的分析。     

火箭人工增雨效果评价系统的设计

利用GoogleEarth二次开发工具API,开发了基于Web技术的海南省火箭人工增雨作业效果评价系统,该系统能形象地描绘火箭人工增雨作业车的位置,动态地勾画和快速计算火箭作业区-对比区的区域面积,并通过互联网技术访问人工增雨数据库、气象资料数据库和自动雨量数据库,随时可以进行人工增雨作业效果评价,导出效果报告。该系统在Web页上操作,便于推广和应用,从而为各市县人工增雨作业提供了一套操作简便、可视化、交互式的人工增雨效果评价平台,实现了全省作业效果评价的统一,提高了人工增雨作业的科技水平和防灾减灾的服务能力。     

在人体内配送药物的纳米火箭

首席科学家詹·赫斯特说：“我们的纳米火箭基于简单的设计，即聚合物泡囊，这是一种球形胶囊。”纳米粒子的大小比细菌体型小10倍，     

钒钛磁铁矿中钪的准确测定

研究了钒钛磁铁矿的快速分解技术。建立了钪与主体成分分离的新方法，并探讨其机理。采用等离子发射光谱法测定钪。标准物质分析结果与推荐值一致。     

引力场中磁场重联的数值研究（Ⅲ）等离子体团的形成和运动

应用解析和数值相结合的方法求得了含有闭场区、中性片和开场区的二维局域磁静力平衡日冕基态，进而在此基态下数值研究了由电阻撕裂模不稳定性引起的磁场重联过程．结果表明，在电流片长度远大于其半宽度的情况下，仍将发生具有两个Ｘ线的磁场重联，形成磁岛和高温高密度的等离子体团．等离子体团运动的方向取决于闭合区底部等离子体压力和磁压的比值β_０．当β_０较大时，等离子体团向下运动，引起结合不稳定性和磁岛的合并，等离子体团中的等离子体不断落入闭合磁场区两侧．当β_０较小时，等离子体团向上运动，导致电流片中等离子体的喷发．结果还表明，磁张力的分布是决定等离子体团运动方向的主要因子．     

电离层的直接探測研究

本文叙述了利用地球物理火箭和人造地球卫星研究电离层和无綫电波传播的各种实驗方法,对各方法之間的关系及其所能解决的問题作了說明,并綜述了在这方面已經得到的重要研究成果。最后扼要地指出了今后研究的主要趋向。     

Space Observation and Study of the Sun.

The ejection of energetic electrons and protons,and γ-ray burst are revealed by solar space observations,which have confirmed some related theories of solar radio emission and uncovered the nuclear reaction in flares.The difference and relationship between CME and plasma cloud in flares are shown by space observations.The hot and cold regions of flares are known.The theory of nonlinear magnetohydrodynamics is developed by solar and heliospheric magnetic field observations.     

高纬电离层中非麦克斯韦分布等离子体的非相干散射谱的模拟

使用一个修正的双麦克斯韦分布函数，通过最小均方适应技术使它与高纬电离层Ｆ区中离子的非麦克斯韦速度分布函数相适配．结果表明，使用这样的分布函数可以简化非相干散射谱的计算，并有助于简化高纬地区电离层非相干散射谱的反演．