2—（2，3，5—三氮唑偶氮）—1，8—二羟基—3，6—萘二磺酸与钴的显色反应及应用

介绍了新水溶性显色剂 2 - ( 2 ,3,5 -三氮唑偶氮 ) - 1 ,8-二羟基 - 3,6-萘二磺酸与钴的显色反应及应用 ,建立了测定钴的新方法。在 pH 9.9的Na2 B4O7 NaOH缓冲液中该试剂与钴形成 1∶1蓝色稳定络合物 ,λmax为 5 88.8nm ,Co的质量浓度在 0～ 1 .0mg/L内符合比尔定律 ,表观摩尔吸光系数为 3.46× 1 0 4 L·mol- 1 ·cm- 1 。所拟方法用于环境水样及维生素B1 2 注射液中的微量钴测定 ,结果与原子吸收法相符 ,5次测定的RSD <1 %。     

Self‐purification in Upland and Lowland Streams

Ecological investigations at four streams in Saxony‐Anhalt have shown that there are considerable differences between the self‐purification power of upland and lowland streams. This result is reflected in chemistry and in microbiology. The structure of the bottom substrate mainly influences the degree of self‐purification in connection with rate of flow and flow velocity. The results and differences are demonstrated using the example of Katzsohlbach in the landscape unit “Mittel‐ and Unterharz” and the stream Olbe in the landscape unit “Magdeburger Börde”.     

Oxidation Experiment of Natural Megacrystal Clinopyroxene: Implications for Assignment of Mössbauer Spectra

The Mössbauer spectra of natural megacrystal clinopyroxene are usually fitted by 4 sets of symmetric doublets, A‐A', B‐B', C‐C' and D‐D', respectively, in terms of increasing Qs value in literature. But the assignments of those doublets are quite different, except the D‐D' doublet assigned to Fe³⁺at the lattice site M***1 in previous papers. Particularly, the assignment and interpretation of the C‐C' doublet are diverse. The oxidation experiments of natural megacrystal clinopyroxene collected from the Hannuoba basalt, North China, were performed under controlled conditions of temperature at 1000°C and oxygen fugacity of FMQ buffer in 1, 2, ***3 and 5 days respectively. The oxidized samples were then measured by X‐ray diffraction spectrometry and Mössbauer spectrometry. The oxidation of clinopyroxene is characterized by Fe²⁺ → Fe³⁺at M1 under the subsolidus conditions, which is consistent with the increase of the area of the D‐D' doublet when the heating time increases. Accordingly, the area of the A‐A' and B‐B' doublets decreases with the increasing heating time. However, the area of C‐C' keeps almost constant. Therefore, the 4 sets of doublets can be assigned correctly as follows: A‐A' doublet to Fe⁺²at M1, B‐B' Fe²⁺at M1, C‐C' Fe²⁺at M2, and D‐D' Fe³⁺at M1. The M1 site splitting is due to the NNN (Next Nearest Neighbour) effect of the M2 site. The amount of Fe³⁺at the tetrohedral site of megacrystal clinopyroxene is negligible according to this study.     

The use of sintered diamond anvils in the MA8 type high-pressure apparatus

A new multi-anvil type high-presure apparatus has been developed using sintered diamond anvils to generate pressures over 30 GPa and temperatures up to about 2000°C. A maximum sample volume of about 1 mm³ is available in this system. The pressure was confirmed by dissociation of forsterite into Mg-perovskite and periclase. The basic techniques and problems in utilizing sintered diamond in the MA8 type high-pressure apparatus are discussed with an emphasis on the future prospect of incorporating simultancous X-ray diffraction observation.     

昆仑山口西8.1级地震后青藏高原北部地区地震活动初步研究

利用相关震例分析了昆仑山口西8．1级地震后青藏高原北部地区未来1～3年地震活动特征．结果表明,沿东昆仑构造带及邻近地区发生Ms≥7．0地震后青藏高原北部地区中强地震活动有增强的趋势,祁连山地震带和东昆仑地震带的地震活动具有交替发生的特征,未来1～3年中强地震主体活动区为大型走滑活动断裂上应力转换部位和挤压会聚构造区,如东昆仑断裂带中东段和祁连山地震带中东段和西段。     

新疆伽师强震群强震主破裂面走向初探

1997年1月21日-1998年8月27日新疆伽师发生了包含9次6级地震的强震群,震源机制解表明有NE向和NW向两个节面．有观点认为主破裂面为NNW向．本通过数字地震台阵的余震序列精确定位、震源破裂过程及滑动方向、震群空间分布图像、地震烈度等震线长轴走向和微、宏观震中动态变化方向等多种方法分析后,综合判定9次6级地震的主破裂面走向极可能为北东方向．     

1997年伽师强震群活动的近场定点形变异常特征

对１９９７年伽师强震群前后的近场宁点形变资料和卡尔曼滤波结果的前兆异常进行了分析,结果表明,震前短临异常较为明显。通过密切跟踪,在后续强震的预报中发挥了重要作用。文中还对异常与孕震构造和应力场的关系进行了讨论。     

利用IRS-P6卫星数据制作遥感影像地图

本文介绍了以IRS-P6卫星数据作为信息源完成大兴安岭林区的遥感影像地图制作的方法, 通过试验初步认识到:利用IRS-P6卫星数据制作遥感影像地图,可以满足1:50000、 1:25000比例尺的平面制图精度要求,在一些专业和专题应用中可以放大到1:15000比例尺使用。     

Characteristics of recent tectonic stress field in Jiashi, Xinjiang and adjacent regions

Introduction The Pamirs region where Jiashi is located is one of the most active regions of continental plate dynamics in China. Frequent earthquakes here, especially several strong earthquakes oc- curred in 1997 and 2003, have provided excellent conditions for studying the tectonic stress field in this region and a large number of results (GAO and WEN, 2000; GAO et al, 2004; XU, 2001; ZHOU et al, 2001) have been obtained. Although different methods and data were used, under- standings …     

Fine upper crustal structure of Jiashi strong earthquake swarm region in Xinjiang inferred from high resolution seismic refraction profile data

Introduction Jiashi-Artux area in southwest Xinjiang is one of the most active earthquake provinces at pre-sent in Chinese mainland. In the last century, about 3/4 strong earthquakes in Chinese mainland hit this area, and especially from January 21 to April 16 in 1997, 7 earthquakes with the magnituderanging from 6.0 to 6.9 occurred in a very small area of 9 km×18 km near Jiashi (ZHU et al, 1998). It has never taken place before in Chinese mainland that a series of strong earthquakes shoo…