Rapid screening of Zr-containing particles from Chang’e-5 lunar soil samples for isotope geochronology: Technical roadmap for future study

New samples returned by China Chang’e-5 (CE-5) mission offer an opportunity for studying the lunar geologic longevity, space weathering, and regolith evolution. The age determination of the CE-5 samples was among the first scientific questions to be answered. However, the precious samples, most in the micrometer size range, challenge many traditional analyses on large single crystals of zircon developed for massive bulk samples. Here, we developed a non-destructive rapid screening of individual zirconium-containing particle for isotope geochronology based on a Micro X-ray fluorescence analysis (µXRF). The selected particles were verified via scanning electron microscopy (SEM), 3D X-ray microscopy (XRM), and focused ion beam scanning electron microscopy (FIB-SEM) techniques, which showed that zirconium-bearing minerals with several microns were precisely positioned and readily suitable for site-specific isotopic dating by second ion mass spectrometry (SIMS). Such protocol could be also applicable in non-destructively screening other types of particles for different scientific purposes. We therefore proposed a correlative workflow for comprehensively studying the CE-5 lunar samples from single particles on nanometer to atomic scales. Linking various microscopic and spectromicroscopic instruments together, this workflow consists of six steps: (1) single-particle selection with non-destructive µXRF technique, (2) 2D/3D morphological and structural characterization with a correlative submicron 3D XRM and nanoscale resolution FIB-SEM imaging methods, (3) SEM analysis of the surface morphology and chemistry of the selected particle, (4) a series of microscopic and microbeam analyses (e.g., SEM, electron probe microanalysis, and SIMS) on the cross-section of the selected particle to obtain structural, mineralogical, chemical, and isotopic features from the micron to nanometer scale, (5) advanced 2D/3D characterization and site-specific sample preparation of thin foil/tip specimens on a microregion of interest in the selected particle with FIB-SEM technique, and (6) comprehensive analyses on the FIB-milled specimens at nanometer to atomic scale with synchrotron-based scanning transmission X-ray microscopy, analytic transmission electron microscopy, and atom probe tomography. Following this technical roadmap, one can integrate multiple modalities into a uniform frame of multimodal and multiscale correlated datasets to acquire high-throughput information on the limited or precious terrestrial and extraterrestrial samples.     

热力学计算模拟对初始月幔结构的约束SCIEI北大核心CSCD

月球岩浆洋结晶形成的初始月球内部结构是其后续演化过程的开端,其结晶过程受月球岩浆洋的初始深度和物质组成这两个参数的制约。由于缺少直接来自月球深部的岩石样品,目前关于月球岩浆洋演化过程的探讨主要依赖实验和计算模拟手段。岩浆洋模型中形成的月壳厚度是否与探测结果一致是月球岩浆洋演化模型合理性的重要约束。最新的GRAIL(Gravity Recovery and Interior Laboratory)探测数据推算月壳厚度为34~43km,低于阿波罗时期认为的约70km,这对已有的月球岩浆洋演化模型提出了挑战。本文采用并修正FXMOTR程序包,针对月球岩浆洋在不同的初始深度和物质组成情况下的结晶过程,进行了一系列热力学计算模拟。通过量化月球岩浆洋的初始深度和物质组成对月壳厚度的影响,结合关于月球内部微量元素分配的研究结果,对比了月球岩浆洋结晶后期的残余熔体与原始克里普组分(urKREEP)的成分。本文的模拟结果显示,一个全月幔熔融且初始成分为月球初始上月幔组成(LPUM)的岩浆洋将在其深部结晶2.5%石榴子石,形成的月壳厚度符合GRAIL的约束,并且结晶出了合适的urKREEP成分。在此模型的基础上获取了月球初始的内部成分和密度结构,并对后期月幔翻转(Overturn)的程度进行了探讨。     

Research in Astronomy and Astrophysics CONTENTS

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上海天文台CHAMP掩星资料处理结果的统计分析

随着GPS全球定位系统的发展,已经有可能使用GPS掩星技术反演精确的大气温度,压强和湿度剖面．在概要地描述上海天文台(SHAO)开发的GPS掩星数据资料反演地球大气流程模块以后,分析了2002年8月1日至2002年8月17日期间2700多次CHAMP掩星数据资料的结果,并且与欧洲中尺度天气预报分析(ECMWF)资料进行比较和统计分析,讨论了CHAMP掩星数据的质量,并分析了CHAMP掩星数据的观测误差和ECMWF的分析模型误差．提出了一种优化的统计分析方法,它能更客观地反映GPS掩星技术的外部符合．统计分析结果表明GPS掩星数据将有可能成为数值天气预报和长期监测地球气候的非常有价值的数据资料．     

GPS掩星技术和电离层反演

系统地介绍了GPS无线电掩星技术的发展现状、系统组成和一些关键技术；论述了利用GPS掩星数据进行电离层反演的理论、模型及相应的计算流程．并结合GPS／MET和CHAMP卫星的实测资料，计算了电子密度剖面，与用其他方法所得结果的对比表明．GPS掩星电离层观测具有精度高、覆盖范围大等特点；最后讨论了GPS掩星技术应用于地震前兆监测的机理和前景。     

Response of GPS occultation signals to atmospheric gravity waves and retrieval of gravity wave parameters

We show that the amplitude of the Global Positioning System (GPS) signals in the radio occultation (RO) experiments is an indicator of the activity of the gravity waves (GW) in the atmosphere. The amplitude of the GPS RO signals is more sensitive to the atmospheric wave structures than is the phase. Early investigations used only the phase of the GPS occultation signals for statistical investigation of the GW activity in the height interval 10–40 km on a global scale. In this study, we use the polarization equations and Hilbert transform to find the 1-D GW radio image in the atmosphere by analyzing the amplitude of the RO signal. The radio image, also called the GW portrait, consists of the phase and amplitude of the GW as functions of height. We demonstrate the potential of this method using the amplitude data from GPS/Meteorology (GPS/MET) and satellite mission Challenge Mini-satellite Payload (CHAMP) RO events. The GW activity is nonuniformly distributed with the main contribution associated with the tropopause and the secondary maximums related to the GW breaking regions. Using our method we find the vertical profiles of the horizontal wind perturbations and its vertical gradient associated with the GW influence. The estimated values of the horizontal wind perturbations are in fairly good agreement with radiosonde data. The horizontal wind perturbations v(h) are ±1 to ±5 m s with vertical gradients dv/dh ±0.5 to ±15 m s km at height 10–40 km. The height dependence of the GW vertical wavelength was inferred through the differentiation of the GW phase. Analysis of this dependence using the dispersion relationship for the GW gives the estimation of the projection of the horizontal background wind velocity on the direction of the GW propagation. For the event considered, the magnitude of this projection changes between 1.5 and 10 m s at heights of 10–40 km. We conclude that the amplitude of the GPS occultation signals contain important information about the wave processes in the atmosphere on a global scale.     

Non-Continuation of Integrals of the Rotating Two-body Problem in Hill's Lunar Problem

We consider Hill's lunar problem as a perturbation of the integrable two-body problem. For this we avoid the usual normalization in which the angular velocity of the rotating frame of reference is put equal to unity and consider as the perturbation parameter. We first express the Hamiltonian H of Hill's lunar problem in the Delaunay variables. More precisely we deduce the expressions of H along the orbits of the two-body problem. Afterwards with the help of the conserved quantities of the planar two-body problem (energy, angular momentum and Laplace–Runge–Lenz vector) we prove that Hill's lunar problem does not possess a second integral of motion, independent of H, in the sense that there exist no analytic continuation of integrals, which are linear functions of in the rotating two-body problem. In connection with the proof of this main result we give a further restrictive statement to the nonintegrability of Hill's lunar problem.     

一种基于嫦娥一号CCD影像的影像匹配方法

月球测绘是完成月球探测任务的基础保障。这里提出了一种适合于CE-1获取的CCD影像的多尺度约束自动匹配方法。首先利用SURF算子提取影像上特征点;然后进行基于准核线和最小欧式距离约束的影像匹配;最后采用随机采样算法对误匹配点进行剔除而得到同名点信息。实验结果表明,该匹配方法提取的同名点有利于CE-1月球影像DEM的生成。     

月球Airy均衡状态与月壳厚度估计

月球水准面异常和表面地形变化是其内部密度不均匀和各个界面的起伏变化的体现,因此利用水准面和地形之比(geoid to topography ratio,GTR)可估计月球均衡和月壳厚度。本文基于月球重力场模型SGM100h和地形模型STM359_grid-02,经过去除表面玄武岩填充和深层异常质量影响,并结合理论Airy均衡模型中GTR与参考月壳厚度的关系,计算得到了新的月壳厚度模型。该模型的月壳平均厚度为36.9 km,背面比正面平均厚约13.5 km,Apollo12/14登陆点的月壳厚度分别是28.3 km和29.1 km。在各月海盆地存在着中央较薄、四周逐渐增厚的趋势。     

月球资源探测信息的管理与可视化探讨

在中国未来的月球探测计划中,可能获取的月球表层数据包括地形、地貌、岩层、土壤、资源、环境以及各种相关的结构、物质成分数据。这些数据既有空间数据,也有属性数据。为了实现月球资源探测工作信息化,可以借鉴“数字地球”的理念并采用“多S”结合与集成化技术,对所获取的海量月球表层数据进行一体化存贮管理,构建一个“数字月球”并实现其空间数据和属性数据之间的双向查询检索,以及对表层复杂结构信息分析的可视化。