黔北后槽下石炭统含铝岩系的粘土矿物

为揭示黔北下石炭统含铝岩系的沉积环境,本文利用贵州遵义县后槽TC718剖面系统试样的粘土矿物进行x一射线衍射测试及特征分析。含铝岩系粘土岩与下伏桐梓组粘土页岩在矿物组合和成分上均有明显的差异,水云母的结晶度指数、开形指数在剖面纵向上有三个变化拐点：一是含铝岩系与下伏桐梓组粘土页岩分界处;二是含铝岩系上、下段的接触带;三是含铝岩系顶部含炭质粘土岩出现的临界面。其变化特征表明,本区下石炭统含铝岩系粘土岩段为海相或海陆过渡相,铝质岩段为残积一坡积相,顶部为大陆湖沼相;下奥陶统桐梓组页岩段为海相。     

磁层-电离层电动耦合的中纬电离层效应

本文通过对1982年磁扰期间琼中、北京两站地磁X分量变化的分析,证实了磁层-电离层电动耦合对中纬电离层电流的影响.分析发现:磁静、磁扰条件下的平均日变化中,两站X分量变化在白天有反向的趋势.这表明它们分处于与动力效应对应的电离层发电机电流圈中心之南北两侧.在磁暴主相期间,X分量变化形态与之明显不同,两站地磁南北分量有同向变化,且变幅相近,甚至有时北京站△X更大.对环电流能量增长指数R小于-25nT/h的21次事件所作的时序叠加分析（以R最负时为零时）进一步证明,这种同向变化是普遍存在的.两站零时之△X大小相近,相关系数高达0.98.该同向变化与R指数突然变负密切相关. 以上对比表明,与发电机电流造成两站X分量反向变化不同,同向变化是磁层源高纬扰动电流向中低纬直接穿透的结果.本文对动力和电动耦合两种过程的不同进行了初步讨论.     

A Stucture—mineralogical Study of Ringwoodite

The powder XRD analysis of ringwoodite(γ-Fe2SiO4),which was synthesized in a II-stage anvil high-pressure capsule,was made,Its unit-cell parameter was calculated:a=8.219A,After the refinements,for several cycles,of the oxygen parameter x and the occupancy rate of Si in octahedron site,i.e.,the iversion degree u,the final result is R=0.077,when x=0.379A and u=27.5%,with the structural formula (Fe1.725 Si0.275)VI(Si0.725Fe0.275)IV O4 and atomic distances(Fe,Si)VI-O=2.022 A and (Si,Fe)IV-O=1.836A,Meanwhile,the Moessbauer spectroscopic analysis of the sample was conducted and the results obtained are in good agreement with those of X-ray structural analysis ,This paper focuses on the phase transformation and the properties of bonds of α－Fe2SiO4→γ-Fe2SiO4.     

Characterization of cristobalite in ash and dome rock from the Soufriere Hills volcano, Montserrat： Implications for respiratory health hazards

A link between the inhalation of respirable silicas （SiO2） and respiratory diseases such as silicosis is widely recognized. Ash from dome collapse eruptions on Montserrat has been found to contain high levels （〉20%） of silicas in the form of cristobalite, tridymite, quartz and/or amorphous silica. The toxicity of these silica polymorphs varies widely. Cristobalite and quartz （tridymite less well established） are viewed as carcinogenic to humans whereas amorphous silica generally shows a reduced biological response. In assessing the potential health effects of volcanic ash particulates it is vital to determine the types and concentration of silicas as well as their size （respirable fraction）, shape and surface properties. The aim of this study is to develop methods to assess potentially toxic respirable airborne silicas in the dome collapse ash （applicable to a range of ash types） and to develop a model to predict the levels and types of respirable silicas from future eruptions. The model is being developed by comparing dome rock with related ash from a series of previous eruption events. Mineralogical assessment using conventional scanning X-ray diffraction （XRD） was hampered by difficulties in differentiating characteristic peaks for cristobalite and tridymite in complex multi-component ash samples （containing high levels of plagioclase）. These difficulties have been largely overcome using an Enraf-Nonius PDS120 diffractometer with curved （120 degrees 20） position sensitive detector （PSD）. The determination of size, shape and elemental characteristics of ash particulate and dome rock samples has been carried out using automated analytical scanning electron microscopy. The quantification of mineral proportions using PSD-XRD was highly successful with an accuracy of 1 to 2 wt%. However, the determination of phase proportions using automated analytical SEM was problematic due to scattering effects and the multiphase nature of many of the particles.     

浙江古代青瓷(1127～1279年)的化学组成及其意义

本文用ENGLE-型微探针能量色散X荧光光谱(EDXRF)技术测定了一批青釉瓷残片中的16种元素氧化物的含量,其残片来自浙江杭州地区的南宋郊坛窑和老虎洞窑。由主量元素判别方程的Q值表明,两类青釉瓷均属官窑制品。主成分统计分析看出,郊坛官窑与老虎洞官窑的瓷釉成分有明显不同,但其胎质成分的分布,却有部分的重叠,这显示了当时两处官窑的工匠们在使用胎料中的交往。从釉层、过渡层、和胎层的Al2O3和CaO的含量数据表明,郊坛官窑和老虎洞官窑的青釉瓷制品,分别存有厚度为120～140μm和230～240μm的过渡层,表明两处使用釉料和烧制工艺上的…     

微量相X射线衍射定量分析的一种简便方法

阐述了关于微量相X射线衍射定量分析的一种简便方法———近似线性关系法,它适用于二相体系(或基体吸收系数基本恒定的多相体系)材料中微量相的定量分析。该方法不需要在待测样品中加入参考物相,分析时仅需对一条衍射线进行测定,因而分析时间很短,其测定结果与实际含量的相对误差为-10.2%～ 21.4%,与外标法和内标法的测量结果的精度相当。     

理学3080E3型X射线荧光光谱仪维修实例

介绍理学3080E3型X射线荧光光谱仪样品驱动单元及高压发生器部分的故障现象及维修实例。     

地图数据的可视化网络浏览技术

本文论述了地图数据可视化网络浏览的必要性，介绍了实现地图数据网络浏览采用的Active X技术。结合地图数据库和微软的基础类库，本文详述了用于地图数据网络浏览的MapCtrl控件的制作和使用方法，成功地解决地图数据的可视化网络浏览问题。     

日本MTSAT多功能卫星

MTSAT卫星系列是日本运输省和日本气象厅合作投资的多功能(气象观测和飞行控制)卫星。第1颗卫星MTSAT-1在1999年11月发射，但由于火箭故障，星箭具毁，之后重新生产了MTSAT-1R，由于等待火箭的故障排除及改进，发射时间一再推延，直到2005年2月26日才发射，发射成功后约2～3个月播发图像。     

飓风中的涡旋罗斯贝波

文中从柱坐标系下的正压无辐散涡度方程出发,用WKBJ方法求解方程,发现在飓风中存在类似于行星罗斯贝波的涡旋罗斯贝波,这种波的形成主要是由于飓风中基态涡度垂直分量的径向梯度所决定。利用一次飓风过程的精确数值模拟所输出高分辨的资料,计算了飓风中径向涡度梯度的分布,指出这类波动主要存在于眼墙和眼心中。波动结构分析表明,波动能量具有径向频散,这有可能是飓风暖心结构的一种形成机制。最后用波射线法讨论了定常涡旋罗斯贝波的径向频散