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71.
We report on the use of X-ray diffractometry under controlled conditions of temperature and relative humidity (RH-XRD) for
the investigation of NaCl deliquescence in the pore space of glass filter frits, which were used as model substrates. The
study confirms that RH-XRD is an appropriate experimental technique for the in situ observation of phase transformation in
porous materials. It is used for an investigation of both the deliquescence kinetics and the deliquescence humidity within
pores of different median pore diameter. Several major influences affecting deliquescence rates in the pore space close to
the surface of a porous material are discussed. It appears that quite short-term variation of ambient relative humidity, e.g.,
typical daily fluctuations, might induce damaging deliquescence–crystallization cycles within the pore space of building materials.
In agreement with theoretical considerations it was found that confinement of NaCl crystals in pores with median diameters
in the range 1.4–70 μm does not affect the deliquescence humidity of the salt. 相似文献
72.
A. Foubert D. Van Rooij D. Blamart J.-P. Henriet 《International Journal of Earth Sciences》2007,96(1):141-158
Three provinces, characterized by the presence of carbonate mounds interpreted as cold-water coral banks have been reported
in Porcupine Seabight, SW of Ireland and were recently subjected to many detailed studies. This contribution discusses the
use of X-ray imagery and physical properties in deciphering palaeoceanographic, sedimentological and biological processes.
Physical property core logging and X-ray imagery are used to identify and describe sedimentation regimes and so their respective
palaeoceanographic and palaeoclimatological settings in two mound provinces, respectively the Belgica mound province and the
Magellan mound province. Both provinces show at present time clear differences in the hydrodynamic environment. This study
confirms that also during the past the oceanographic and sedimentological environment of both provinces differ clearly. Impacts
of glacial–interglacial variations and locally derived ice rafting events (IRE), comparable with the North Atlantic Heinrich
events (HE) have been recognized in both provinces. Moreover, the combination of X-ray imagery, magnetic susceptibility, gamma
density and P-wave velocity makes it possible to estimate the coral content and coral distribution in unopened cores localized
on top of carbonate mounds. A comparison between on-mound and off-mound cores in both provinces allowed revealing some mechanisms
of mound evolution and coral growth versus time. 相似文献
73.
Li Guowu Shi Nicheng Xiong Ming Ma Zhesheng Bai Wenji Fang Qingsong 《Frontiers of Earth Science》2007,1(1):21-25
The origin of native Si-Fe alloy mineral is thought to be related with mantle and aerolite. The native Si-Fe alloy minerals
from podiform chromites of the Luobusha ophiolite in the Yarlong Zangbo suture zone were examined by a new method for powder-like
diffractograms of small single crystals, using an SMART APEX-CCD area-detector X-ray diffractometer. The powder diffraction
pattern shows that the minerals are composed of FeSi, FeSi2, β-FeSi2 and native silicon. The association of these minerals suggests that the crystallization order of the mineral may be from
early to late FeSi→FeSi2→native silicon, accompanied by gradually increasing deoxidization.
Translated from Acta Petrologica et Mineralogica, 2005, 24(5): 453–456 [译自: 岩石矿物学杂志] 相似文献
74.
Three resection–intersection algorithms were applied to simulated projections and clinical data from radiostereometric patients. On simulated data, the more advanced bundle-adjustment-based algorithms outperformed the classical Selvik algorithm, even if the error reductions were small for some parameters. On clinical data, the results were inconclusive.The two different projection geometries had a much larger influence on the error size and distribution. For the biplanar configuration, the position and motion errors were small and almost isotropic. For the uniplanar configuration, the position errors were comparably high and anisotropic, but still resulted in a high accuracy for some motion parameters at the expense of others.The simplified resection–intersection algorithm by Selvik may still be considered a good and robust algorithm for radiostereometry. More studies will have to be performed to find out how the theoretical advantages of the bundle methods can be utilized in clinical radiostereometry. 相似文献
75.
目的旨在提高肺结核开放-菌阴综合征的诊断和鉴别诊断,材料和方法用回顾性分析经病原学或临床确诊的开放型肺结核,而痰菌阴性的42例病人的CT影像表现。结果得到42例均见斑片状高密度灶影,其中41例不规则空洞影,4例与支气管相通;28例卫星灶影,8例纤维索条影,1例仅见小斑片状影伴卫星灶影,10例见斑点状钙化影,2例淋巴结肿大等。结论是CT对肺结核开放-菌阴综合征的诊断和鉴别诊断有较高的价值,特别是对估价空洞的形态结构,心后区,脊柱旁,后肋隔区,与肺门阴影重叠的病及少量胸腔积液等方面更有价值,对诊断和疗效的观察较可靠。 相似文献
76.
77.
Abstract: Synchrotron X-ray fluorescence analyses on individual hypersaline fluid inclusions were tested to using synchrotron source at Tsukuba (KEK), Japan. The XRF instrumentation at KEK meets the purpose of fluid inclusion analysis, nondestructive, multi–element, ppm detection limits, with micro spatial resolution. In practice, however, the quantitative chemical analysis of fluid inclusion requires further considerable data accumulation. Semi-quantitative distribution of elements (mass number > 25) in single fluid inclusion was obtained. 相似文献
78.
Using single-crystal X-ray diffraction from a diamond anvil cell, the compressibility of a synthetic fluorapatite was determined up to about 7?GPa. The compression pattern was anisotropic, with greater change along a than c. Unit cell parameters varied linearly with β a =3.32(8)?10?3 and β c =2.40(5)?10?3 GPa?1, giving a ratio β a :β c =1.38:1. Data fitted with a third-order Birch-Murnaghan EOS yielded a bulk modulus of K 0=93(4)?GPa with K′=5.8(1.8). The evolution of the crystal structure of fluorapatite was analysed using data collected at room pressure, at 3.04 and 4.72?GPa. The bulk modulus of phosphate tetrahedron is about three times greater than the bulk modulus of calcium polyhedra. The values were 270(10), 100(4) and 86(3) GPa for P, Ca1 (nine-coordinated) and Ca2 (seven-coordinated) respectively. While the calcium polyhedra became more regular with pressure, the distortion of the phosphate tetrahedron remained unchanged. The size of the channel extending along the [001] direction represented the most compressible direction. The Ca2–Ca2 distance decreased from 3.982 to 3.897?Å on compression from 0.0001 to 4.72?GPa. The anisotropic compressional pattern may be understood in terms of the greater compressibility of the channel size over the polyhedral units. The reduction of the channel volume was measured by the evolution of the trigonal prism, having the Ca2–Ca2–Ca2 triangle as its base and the c lattice parameter as its height. This prism volume changed from 47.3?Å3 at room pressure to 44.78?Å3 at 4.72?GPa. Its relatively high bulk moduli, 86(3) GPa, indicated that the channel did not collapse with pressure and the apatite structure could remain stable at very high pressure. 相似文献
79.
J. M. Léger J. Haines C. Chateau G. Bocquillon M. W. Schmidt S. Hull F. Gorelli A. Lesauze R. Marchand 《Physics and Chemistry of Minerals》2001,28(6):388-398
The structure of the cristobalite-like polymorph of phosphorus oxynitride PON has been refined using neutron powder diffraction
data. It is tetragonal, space group I&4macr;2d, Z=4. The four P–(O,N) distances are equal but the tetrahedron is compressed along c. In AX2 or ABX4 compounds, the tetragonal I&4macr;2d or I&4macr; structure is obtained when the average ratio of the cation to anion radius is below 1.186, whereas the tetragonal P41212 or orthorhombic C2221 structure is obtained at low temperatures for larger ratios. The cell parameters of this PON polymorph have been determined
as a function of hydrostatic pressure by in situ angle dispersive X-ray powder diffraction in a diamond-anvil cell. Under
truly hydrostatic pressure, a strong anisotropic behavior is observed with the c parameter being nearly incompressible. Very slight anisotropic stress strongly modifies the high-pressure behavior. According
to the pressure-temperature conditions of treatment, three phases, cristobalite-, moganite-, and quartz-like, have been obtained
by quenching experiments, and the P–T phase diagram of PON was derived. The high-pressure behavior of the α-quartz, moganite, and cristobalite-like polymorphs
of PON and SiO2 is discussed.
Received: 7 August 2000 / Accepted: 21 January 2001 相似文献
80.