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Homogeneity testing of microanalytical reference materials by electron probe microanalysis (EPMA)

Homogeneity testing of candidate reference materials requires distinguishing the effects of measurement uncertainty of the analytical method from true compositional variations within the material. Many in situ microanalytical techniques do not allow classical ANOVA homogeneity testing due to the infeasibility of truly replicated analyses on the same analysis volume. This also applies to the analysis of beam-sensitive and light element-bearing materials by electron probe microanalysis (EPMA). This reality has led me to reconsider the homogeneity index approach used in the testing of microanalytical reference materials by EPMA. Based on statistical considerations, I show that the homogeneity index is suitable for statistical significance testing using F and chi-squared statistics and allows estimating the contribution of compositional heterogeneity to the total uncertainty budget of the referenced values. However, there are problems of bias and masking of small compositional variations by measurement uncertainty. This contribution shows the strong impact of the total number of measurements on the resolution of a microanalytical homogeneity study and discusses how to quantify the relative contribution of heterogeneity to the total uncertainty budget. I present an example of EPMA to illustrate this approach and show some pitfalls and limitations in its application.     

Dynamics of warm inflation with gauge fields in Bianchi type I universe model

In this paper, we study the dynamics of warm inflation in which slow-roll inflation is driven by non-Abelian gauge fields. To this end, we use the geometry of locally rotationally symmetric Bianchi type I universe model. We construct dynamical equations, i.e., first model field equation, energy conservation equations and equation of motion under slow-roll approximation. In order to discuss inflationary perturbations, we evaluate parameters like scalar and tensor power spectra as well as scalar and tensor spectral indices. We also evaluate inflaton, directional Hubble parameter, slow-roll and perturbation parameters as well as tensor-scalar ratio as a function of inflaton during intermediate and logamediate inflationary eras. It is concluded that anisotropic inflationary universe model with non-Abelian gauge fields remains compatible with WMAP7.     

乔治王岛菲尔德斯半岛的地温特征和岩石热物理性质

1985—1986年度和1986—1987年度在菲尔德斯半岛对地面温度进行了测量,共获得129个数据,并对带回的样品进行了岩石热导率测量,共获得210个数据。本文在分析和归纳这些数据的基础上对菲尔德斯半岛的地温特征和岩石热物理性质进行了初步探讨。     

BOOK REVIEWS

Books reviewed in this article: Aerial Photography and Remote Sensing. Terrain Analysis and Remote Sensing . JOHN R. G. TOWNSHEND , ed. Environmental Data Use in Computer-assisted Data Handling Systems: The Results of a Survey of Applications in the Pacific Northwest States . KENNETH E. GORDON . Applied Land Use: A Spatial Approach . JOHN F. LOUNSBURY , LAWRENCE M. SOMMERS , AND EDWARD A. FERNALD , eds. The Second Battle of New Orleans: A History of the Vieux Carre Riverfront-Expressway Controversy . RICHARD O. BAUMBACH , JR. AND WILLIAM E. BORAH . Cultural Environmental Archaeology . MYRA SHACKLEY . The Immoral landscape: Female Prostitution in Western Societies . RICHARD SYMANSKI . life Among the Poor in Cairo . UNNI WIKAN , translated by Ann Henning. Women, Work and Property in Northwest India . URSULA SHARMA . The Domestication of Women: Discrimination in Developing Societies . BARBARA ROGERS Economic Optimization in Locational and Transport Analysis . A. G. WILSON , J. D. COELHO , S. M. MACGILL , H. C. W. L. WILLIAMS . New Tools for Economic Development: The Enterprise Zone, Development Bank, and RFC . GEORGE STERNLIEB AND DAVID LISTOKIN , eds. Regional Wage Inflation . R. L. MARTIN , ed. Finding A Place For Energy-Siting Coal Conversion Facilities . FRANK J. CALZONETTI WITH MARK S. ECKERT . Environmental Management, Resources, and Systems Environmentalism. Second Edition . T. O'RIORDAN . Countryside Conservation . BRYN GREEN . Medical Spatial Diffusion: An Historical Geography of Epidemics in an Island Community . A. D. CLIFF , P. HAGGETT , J. K. ORD , AND G. R. VERSEY . Philosophy and Geographic Thought Order and Skepticism: Human Geography and the Dialectic of Science . RICHARD SZYMANSKI AND JOHN A. AGNEW . Measurement of Subjective Phenomena . D. F. JOHNSTON , ed. Conceptions of Space in Social Thought: A Geographic Perspective . ROBERT DAVID SACK . The Association of American Geographers: The First Seventy-five Years: 1904-1979 . PRESTON E. JAMES AND GEOFFREY J. MARTIN . The Life and Thought of Isaiah Bowman . GEOFFREY J. MARTIN . Physical River Basin Planning: Theory and Practice . SURANJIT K. SAHA AND CHRISTOPHER J. BARROW , eds. Soils and landforms: An Integration of Ceomorphology and Pedology . A. I. GERRARD Climatic Change and Society. Consequences of Increasing Atmospheric Carbon Dioxide . WILLIAM W. KELLOGG AND ROBERT SCHWARE . Political Political Redistrictings and Geographic Theory . RICHARD L. MORRILL . Population Studies in Spanish American Population History: Dell Plain Latin American Studies NO. 8 . DAVID J. ROBINSON , ed. Population Redistribution in the Midwest . CURTIS C. ROSEMAN , ANDREW J. SOFRANKO , AND JAMES D. WILLIAMS , eds. Geographical Perspectives on the Elderly . A. M. WARNES , ed. Regional Perspective On the American South . MERLE BLACK AND JOHN SHELTON REED , eds. The Prairies and Plains: Prospects for the 80s . JOHN R. ROGGE , ed. Rural Rural Settlement in an Urban World . MICHAEL BUNCE . Social Accident at Three Mile Island: The Human Dimensions . DAVID L. SILLS , C. P. WOLF , AND VIVIEN B. SHELANSKI , eds. The American Small Town: Twentieth-Century Place Images . JOHN JAKLE . Urban A House of My Own . SUSAN LOBO . The City: Patterns and Processes in the Urban Ecosystem . CHRISTOPHER H. EXLINE , GARY L. PETERS , AND ROBERT P. LARKIN . Movement in Cities . P. W. DANIELS AND A. M. WARNES . Urbanization and Urban Planning in Capitalist Society . MICHAEL DEAR AND ALLEN J. SCOT , eds.     

Study of a thermal drill head for the exploration of subsurface planetary ice layers

The recently discovered water vapor plumes on Saturn's moon Enceladus, the polar caps of planet Mars and the possible ice volcanism on the Jovian satellites call for suitable techniques to explore deep ice layers of the solar system bodies. This paper presents a novel approach to deliver scientific probes into deeper layers of planetary ice. Several existing locomotion concepts and techniques for such probes are presented. After studying the mathematical framework of the melting locomotion process, melting tests with different head forms were done to evaluate the influence of the head's geometry on the melting process. This work led to a novel concept of a thermal drill head, using heat and mechanical drill in combination to penetrate the ice. We compare the performance of such a hybrid concept versus the melting penetration alone by a mathematical model and tests in ice with a prototype of the melting drill head.     

非饱和黄土地基降雨入渗离心模型试验及多物理量联合监测

对非饱和土降雨入渗过程及其致灾机制的深入认识有赖于室内外试验及多物理量联合监测。基于离心机超重力环境下土体响应监测技术,开展了非饱和黄土地基降雨入渗离心模型试验,测试研究了超重力环境对新研制的微型TDR探针及张力计测量的影响规律,并利用TDR、张力计及弯曲元对降雨入渗过程中土体响应进行多物理量联合监测。研究结果表明:在不同离心加速度下微型TDR探针与给定含水率土体实测原始波形重合,说明超重力环境对TDR测试没有影响,含水率的测试误差在2%以内。在离心机加速过程中,张力计所测吸力下降约2.0~2.9 kPa,当离心加速度稳定在40g时,所测吸力在10min内上升并接近常重力下土体初始吸力。在降雨入渗过程中,埋设在同一深度的TDR探针、张力计和弯曲元对湿润锋响应的时间点基本一致,降雨入渗导致土体含水率增加,基质吸力降低,剪切波速降低。这些多物理量监测数据有助于建立非饱和土含水率-吸力-剪切模量之间的关系。     

上扬子西南缘早三叠世嘉陵江组物源分析和构造环境:沉积学、重矿物电子探针和U- Pb年龄的限定

上扬子西南缘地区广泛分布峨眉山玄武岩,受其影响在中带金阳和外带荥经地区嘉陵江组发育滨岸和潮坪环境沉积物。本文在交错层理恢复的物源方向基础上,根据重矿物组成、重矿物电子探针和碎屑锆石测年结果,综合分析不同区域嘉陵江组物源区,进而探讨嘉陵江组形成的构造环境。嘉陵江组砂岩碎屑重矿物锆石、磷灰石、铬尖晶石等指示物源主要来自于岩浆岩,且自中带至外带基性岩浆岩所占比重逐渐减少。电气石电子探针分析显示,二者物源主要来自于贫锂花岗岩和变质砂岩、板岩。铬尖晶石显示,金阳地区物源来自峨眉山玄武岩和洋岛岩浆岩类岩石,荥经物源主要来自洋岛岩浆岩类岩石,个别为峨眉山玄武岩。碎屑锆石表明,嘉陵江组物源主要来自于新元古代岩浆岩和晚二叠世峨眉山玄武岩,前者经历再搬运。综合物源分析表明,嘉陵江组物源主要来自康滇古陆,岩石类型主要为峨眉山玄武岩和砂岩等。沉积序列和物源分析表明,嘉陵江组反映了沉积物蚀顶过程。结合地震资料、大火成岩省的分析成果表明,嘉陵江组形成于火山型裂谷边缘。     

‘Box‐Profile’ Ion Implants as Geochemical Reference Materials for Electron Probe Microanalysis and Secondary Ion Mass Spectrometry

Although electron probe microanalysis and secondary ion mass spectrometry are widely used analytical techniques for geochemical and mineralogical applications, metrologically rigorous quantification remains a major challenge for these methods. Secondary ion mass spectrometry (SIMS) in particular is a matrix‐sensitive method, and the use of matrix‐matched reference materials (RMs) is essential to avoid significant analytical bias. A major problem is that the number of available RMs for SIMS is extremely small compared with the needs of analysts. One approach for the production of matrix‐specific RMs is the use of high‐energy ion implantation that introduces a known amount of a selected isotope into a material. We chose the more elaborate way of implanting a so‐called ‘box‐profile’ to generate a quasi‐homogeneous concentration of the implanted isotope in three dimensions, which allows RMs not only to be used for ion beam analysis but also makes them suitable for EPMA. For proof of concept, we used the thoroughly studied mineralogically and chemically ‘simple’ SiO₂ system. We implanted either ⁴⁷Ti or ⁴⁸Ti into synthetic, ultra‐high‐purity silica glass. Several ‘box‐profiles’ with mass fractions between 10 and 1000 μg g^?1 Ti and maximum depths of homogeneous Ti distribution between 200 nm and 3 μm were produced at the Institute of Ion Beam Physics and Materials Research of Helmholtz‐Zentrum Dresden‐Rossendorf. Multiple implantation steps using varying ion energies and ion doses were simulated with Stopping and Range of Ions in Matter (SRIM) software, optimising for the target concentrations, implantation depths and technical limits of the implanter. We characterised several implant test samples having different concentrations and maximum implantation depths by means of SIMS and other analytical techniques. The results show that the implant samples are suitable for use as reference materials for SIMS measurements. The multi‐energy ion implantation technique also appears to be a promising procedure for the production of EPMA‐suitable reference materials.