过硫酸铵氧化容量法测定矿石中锰方法的改进

采用过硫酸铵氧化容量法测定锰时,可在低酸度(0.18mol/LH2SO4、0.29mol/LH3PO4)和大体积(300mL)溶液中氧化Mn2 至Mn7 。所测得的结果十分稳定,回收率为100%。采用管理样分析验证方法,其结果与铋酸钠容量法结果一致。对于w(Mn)=11.36%的试样进行10次分析测定,RSD=0.33%。方法可测定w(Mn)≥0.01%的常见矿种样品。     

低频泥石流特征及防治 --以四川汶川县茶园沟为例

低频泥石流指30a以上发生1次的泥石流。尽管发生频率很低，但由于自身的特征及人们认识上的原因，其造l戒的人员伤亡和财产损失却居各类泥石流之首。对低频泥石流的研究在预防和减轻泥石流灾害方面有着重要意义。文章以2003年8月9日发生在四川汶川县茶园沟的泥石流为蒯，采用形态调查法和称重法等方法确定了流量、流速及重度。分析了其物质来源及形成的自然和人为原因，探讨了低频泥石流的特征。针对低频泥石流的低频性、破坏性和隐蔽性特点，同时考虑到低频泥石流沟的防治受保护对象的重要程度及资金投入等因素的限制，提出了进行泥石流危险性分区、搞好小流域水土深持、普及泥石流防灾减灾知识及加强监测和预警预报等措施，这对减轻低频泥石流区的灾害有一定的借鉴意义。     

Ekman动量近似下中间边界层模式中的风场结构

发展了一个准三维的、中等复杂的边界层动力学模式，该模式包含了EKman动量近似下的惯性加速度和Blackadar的非线性湍流粘性系数，它进一步改进了Tan和Wu(1993）提出的边界层理论模型。该模型在数值计算复杂性上与经典Ekman模式相类似，但由于包含了Ekman动量近似下的惯性项，使得该模式比传统Ekman模式更近于实际过程。中详细地比较了该模式与其他简化边界层模式在动力学上的差异，结果表明：在经典的Ekman模式中，由于忽略了流动的惯性项作用，导致在气旋性切变气流（反气旋性切变气流）中风速和边界层顶部的垂直速度的高估（低估），而在半地转边界层模式中，由于高估了流动惯性项的作用，结果与经典Ekman模式相反。同样，该模式可以应用于斜压边界层，对于Ekman动量下的斜压边界层风场同时具有经典斜压边界层和Ekman动量近似边界层的特征。     

赣北中元古界双桥山群低变质强变形行为与格林威尔期造山作用

广泛分布于赣北地区的中元古界双桥山群，以低级区域变质作用、强烈构造变形、具陆内造山带构造变形特征；其成果系在华夏古陆与扬子古陆的碰撞拼接过程中，其应力向陆内传递的结果；时间大致在1100－800Ma，与全球格林威尔期造山作用相当。     

济阳坳陷孤南洼陷低熟油成藏特征

孤南洼陷具有丰富的低熟油资源，低熟油中的生物标志物以高伽玛蜡烷含量，植烷优势，低成熟度为特征。下第三系沙一段是低熟油的源岩，其岩性为富含藻类有机质的油页岩，油泥岩，低熟油在平面上环生烃洼陷分布，剖面上层位集中在沙二－沙一段，断层控制了低熟油的运移距离和聚集层位，低熟油的成藏模式有3种，即自源侧向运移聚集成藏，自源断层垂向运聚成茂混合运取成藏模式。孤南洼陷低熟油盆地内部以侧向运移，侧向充注入岩性－断块圈闭为主，形成单源油藏。在断藏带原油是以垂向运移及垂向充注断块圈闭为主，形成混源油藏。     

Tests on low‐ductility RC frames under high‐ and low‐frequency excitations

The response of low‐ductility reinforced concrete (RC) frames, designed typically for a non‐seismic region, subjected to two frequencies of base excitations is studied. Five half‐scaled, two‐bay, two‐storey, RC frames, each approximately 5 m wide by 3.3 m high, were subjected to both horizontal and/or vertical base excitations with a frequency of 40 Hz as well as a lower frequency of about 4 Hz (close to the fundamental frequency) using a shake table. The imposed acceleration amplitude ranged from 0.2 to 1.2g. The test results showed that the response characteristics of the structures differed under high‐ and low‐frequency excitations. The frames were able to sustain high‐frequency excitations without damage but were inadequate for low‐frequency excitations, even though the frames exhibited some ductility. Linear‐elastic time‐history analysis can predict reasonably well the structural response under high‐frequency excitations. As the frames were not designed for seismic loads, the reinforcement detailing may not have been adequate, based on the crack pattern observed. The effect of vertical excitation can cause significant additional forces in the columns and moment reversals in the beams. The ‘strong‐column, weak‐beam’ approach for lateral load RC frame design is supported by experimental observations. Copyright © 2001 John Wiley & Sons, Ltd.     

低温电镀孕镶金刚石石油取心钻头研制与应用

该钻头用于坚硬地层取心。河南油田以往常用园柱聚晶、三角聚晶钻头以及烧结孕镶金刚石钻头，取心效率低、钻速慢、成本高。近两年采用低温电镀孕镶金刚石钻头取心后，平均单筒进尺由原来的4．20m／筒提高到7．62m/筒，平均取心机械钻速由原来的0．21m/h提高到的0.84m/h。该钻头生产工艺完全改变原来高温（1000℃以上）烧结为低温（室温）电镀工艺，极大地避免了金刚石热损伤，采用高强度大颗粒的金刚石，提高了取心机械钻速。     

吉林集安铅锌矿地球化学与分散元素

吉林集安铅锌矿床是我国最早报导的少数几个典型低温铅锌矿床之一。矿化具有多期次特点 ,富矿体都是多期次矿化叠加的产物。根据矿化先后和矿物生成顺序将矿化分为五个阶段 :①石英 黄铁矿矿化阶段 ;②重晶石 闪锌矿矿化阶段 ;③石英 方铅矿矿化阶段 ;④石英 黄铁矿矿化阶段 ;⑤碳酸盐 氧化矿物矿化阶段。用均一法和爆裂法测得石英、重晶石、闪锌矿包裹体成矿温度变化在 1 1 0℃～ 1 97℃之间。矿床中除含铅锌矿外 ,还有微量的Pt和Pd,并普遍含分散元素Cd、Ga、Tl、In、Se、Ge、Te,其中以Cd含量最高 ,闪锌矿中Cd含量最高可达 71 5 5× 1 0 6。分散元素主要呈类质同象形式赋存在各种矿物之中 ,未发现独立矿物。通过矿床地质和硫铅同位素研究表明该铅锌矿床属低温沉积 改造型层控矿床。     

富碱斑岩中超镁铁深源包体岩石的矿物学特征

在云南省鹤庆县六合乡富碱斑岩体中找到超镁铁深源岩石包体，这对于研究富碱斑岩的起源和演化及其成岩成矿作用具有重要意义。本文较系统地研究了深源包体岩石的矿物学特征，揭示该深源包体具有原始上地幔岩在地幔条件下受到一定程度富集地幔流体交代作用改造的特征，具有富集地幔低程度部分熔融属性，为富碱斑岩的成岩成矿演化提供了重要的矿物学依据。     

Probing mid-mantle heterogeneity using PKP coda waves

We investigate the utility of PKP coda waves for studying weak scattering from small-scale heterogeneity in the mid-mantle. Coda waves are potentially a useful probe of heterogeneity in the mid-mantle because they are not preferentially scattered near the CMB, as PKP precursors are, but are sensitive to scattering at all depths. PKP coda waves have not been used for this purpose historically because of interference with other late-arriving energy due to near-surface resonance and scattering. Any study of deep mantle scattering using coda waves requires the removal of near-surface effects from the data. We have analyzed 3624 recordings of PKP precursors and coda made by stations in the Incorporated Research Institutions for Seismology (IRIS) Global Seismographic Network (GSN). To study the range and time dependence of the scattered waves, we binned and stacked envelopes of the recordings. We have considered precursors that arrive within a 20 s window before PKP and coda waves in a 60 s window after PKP. The PKP scattered waves increase in amplitude rapidly with range as predicted by scattering theory. At ranges below 125°, we predict and observe essentially no scattered energy preceding PKP. Coda amplitudes at these ranges are independent of range and provide an estimate of energy due to near-surface effects that we can expect at all ranges. We use the average coda amplitude at ranges from 120 to 125° to correct coda amplitudes at other ranges. PKP coda waves show a strong dependence on time and range and are clearly influenced by scattering in the lower mantle. PKP coda waves, however, do not provide a tighter constraint on the vertical distribution of mantle heterogeneity than is provided by precursors. This is due, in part, to relatively large scatter in coda amplitudes as revealed by a resampling analysis. Modeling using Rayleigh–Born scattering theory and an exponential autocorrelation function shows that PKP coda amplitudes are not highly sensitive to the vertical distribution of heterogeneity in the mantle. To illustrate this we consider single-scattering in two extreme models of mantle heterogeneity. One allows heterogeneity just at the CMB; the other includes heterogeneity throughout the mantle. The amplitudes of precursors are tightly constrained by our stack and support our earlier conclusion that small-scale heterogeneity is uniformly distributed throughout the lower mantle. The best-fit model includes 8 km scale length heterogeneity with an rms velocity contrast throughout the mantle of 1%.