CORS系统的差分定位终端设计与实现

当前广泛使用的实时GNSS定位应用可分为两种:一种是低成本定位应用,其采用廉价的芯片和天线,广泛应用于手机、共享单车和公交车定位等方面;另一种是高精度GNSS定位应用,采用网络RTK技术并结合测量型天线和接收机,为高精度测量用户提供实时厘米级测量服务。随着物联网、5G等技术的发展,实时分米到亚米级的定位需求逐渐增多。原有的低成本GNSS定位技术无法达到这一精度要求,高精度定位的设备成本高昂,无法用于大众导航领域。因此,本文实现了一种基于CORS系统的低成本差分定位终端。该终端包括两个部分:外接设备和手机。试验表明,在接入CORS系统后,该设备水平方向的定位精度可以达到亚米级,对推进CORS系统的大范围应用具有一定的意义。     

Zircon M127 – A Homogeneous Reference Material for SIMS U–Pb Geochronology Combined with Hafnium,Oxygen and,Potentially, Lithium Isotope Analysis

In this article, we document a detailed analytical characterisation of zircon M127, a homogeneous 12.7 carat gemstone from Ratnapura, Sri Lanka. Zircon M127 has TIMS‐determined mean U–Pb radiogenic isotopic ratios of 0.084743 ± 0.000027 for ²⁰⁶Pb/²³⁸U and 0.67676 ± 0.00023 for ²⁰⁷Pb/²³⁵U (weighted means, 2s uncertainties). Its ²⁰⁶Pb/²³⁸U age of 524.36 ± 0.16 Ma (95% confidence uncertainty) is concordant within the uncertainties of decay constants. The δ¹⁸O value (determined by laser fluorination) is 8.26 ± 0.06‰ VSMOW (2s), and the mean ¹⁷⁶Hf/¹⁷⁷Hf ratio (determined by solution ICP‐MS) is 0.282396 ± 0.000004 (2s). The SIMS‐determined δ⁷Li value is ?0.6 ± 0.9‰ (2s), with a mean mass fraction of 1.0 ± 0.1 μg g^?1 Li (2s). Zircon M127 contains ~ 923 μg g^?1 U. The moderate degree of radiation damage corresponds well with the time‐integrated self‐irradiation dose of 1.82 × 10¹⁸ alpha events per gram. This observation, and the (U–Th)/He age of 426 ± 7 Ma (2s), which is typical of unheated Sri Lankan zircon, enable us to exclude any thermal treatment. Zircon M127 is proposed as a reference material for the determination of zircon U–Pb ages by means of SIMS in combination with hafnium and stable isotope (oxygen and potentially also lithium) determination.     

浙江西部建德群锆石LA-ICP-MS之U-Pb同位素年龄及其地层学意义

利用LA-ICP-MS测试技术对浙西地区中生代晚期寿昌盆地典型剖面建德群9件凝灰岩和安山岩样品的锆石进行了同位素测年分析。结果显示:建德群锆石206Pb/238U年龄加权平均值范围在134～115Ma之间,属于早白垩世中—晚期;其所属的劳村组、黄尖组、寿昌组和横山组的锆石年龄分别是134～125Ma、125～118Ma、125～121Ma和121～115Ma,各自对应于欧特里夫期—巴雷姆期、阿普特期早—中期、阿普特期早期、阿普特期中期。由此认为,黄尖组的时代与寿昌组+横山组大致相当,前者与后两者横向可能为同时异相,并非上下关系;在寿昌和丽水两个盆地的寿昌组近乎同时,其上为时代大致相当的横山组与馆头组。     

MT法中利用阻抗相位资料对畸变视电阻率曲线的校正

从理论上论证了在一定条件下大地电磁响应中的相位资料将不受随机电磁噪声的影响，介绍了由相位资料递推计算视电阻率的方法，通过与远参考资料的比较，证明利用阻抗相位资料可分段恢复校正畸变的实测视电阻率数据。     

New Reference Materials and Assessment of Matrix Effects for SIMS Measurements of Oxygen Isotopes in Garnet

Accurate ion microprobe analysis of oxygen isotope ratios in garnet requires appropriate reference materials to correct for instrumental mass fractionation that partly depends on the garnet chemistry (matrix effect). The matrix effect correlated with grossular, spessartine and andradite components was characterised for the Cameca IMS 1280HR at the SwissSIMS laboratory based on sixteen reference garnet samples. The correlations fit a second‐degree polynomial with maximum bias of ca. 4‰, 2‰ and 8‰, respectively. While the grossular composition range 0–25% is adequately covered by available reference materials, there is a paucity of them for intermediate compositions. We characterise three new garnet reference materials GRS2, GRS‐JH2 and CAP02 with a grossular content of 88.3 ± 1.2% (2s), 83.3 ± 0.8% and 32.5 ± 3.0%, respectively. Their micro scale homogeneity in oxygen isotope composition was evaluated by multiple SIMS sessions. The reference δ¹⁸O value was determined by CO₂ laser fluorination (δ¹⁸O_LF). GRS2 has δ¹⁸O_LF = 8.01 ± 0.10‰ (2s) and repeatability within each SIMS session of 0.30–0.60‰ (2s), GRS‐JH2 has δ¹⁸O_LF = 18.70 ± 0.08‰ and repeatability of 0.24–0.42‰ and CAP02 has δ¹⁸O_LF = 4.64 ± 0.16‰ and repeatability of 0.40–0.46‰.     

A Review of the IAG GeoPT™ and Certification Programmes,their Protocols,and the Differences between the Original and Potential Modifications to the Certification Protocol

The IAG conducts two programmes, the GeoPT ^? proficiency test and a certification programme that are closely interconnected. Both support the quality control/quality assurance activities of geochemical laboratories. Each derives an estimate of ‘true value’ for a number of samples, but arrives at that estimate, and its uncertainty, differently. This review discusses the history of the two programmes and compares the ‘true values’ and their uncertainties obtained through each. It then considers ‘fitness‐for‐purpose’ issues related to both GeoPT ^? and certification uncertainties. Issues related to potential modification of the IAG protocol for certification are also considered.     

激光探针质谱及单颗粒矿物^40Ar／^39Ar法年龄的测定

将掺钕的钇铝榴石（Ｎｄ：ＹＡＧ）激光器与高精密ＭＭ１２００质谱计、电子倍增器联网，应用连续激光质谱对单颗粒矿物、光片样品进行微区４０Ａｒ／３９Ａｒ测年、坪年龄和等时线年龄研究。在光片上测定南极乔治王岛北海岸玄武岩等时线年龄（５２．３８±１．０５）Ｍａ和贵州绿豆岩年龄（２３９．１６±１４．１３）Ｍａ，两者与实际地质背景吻合。对两个中生代和太古代单颗粒黑云母进行连续激光质谱阶段升温４０Ａｒ／３９Ａｒ坪年龄谱测定，获得与常规法相一致的坪年龄谱     

高台车站断裂全新世活动特征

高台车站断裂属于河西走廊内次级隆起——榆木山隆起北侧断裂系的组成部分,它位于榆木山北缘断裂北侧6km、是与榆木山隆起有成生联系、活动时间比北缘断裂更新的现代活动断裂。高台车站断裂呈向北北东略微凸出的弧形,走向总体为北西向,倾向南西,自南东向北西走向由北西向渐变为北西西、甚至近东西向,倾角自中等变化为低角度。高台车站断裂的活动性质在剖面上表现为南西盘向上逆冲为主、水平位移不明显,在近两万年以来的晚更新世晚期—全新世期间,该断裂可能发生过5期明显的新构造活动,活动时间具有自东向西逐渐变新的迁移性特点,最新一次在2.0~3.0ka左右,与高台地震时间是吻合的,它是高台地震的发震构造。     

河北某斑岩型钼矿提高选矿指标试验研究

河北省某钼矿为单一斑岩型钼矿,主要金属矿物为辉钼矿。为了进一步提高钼精矿的品位和回收率,试验采用混合捕收剂(煤油∶2号油=2∶1)和新型捕收剂PE-100相结合的方法,粗选时可使粗精矿的回收率提高2个百分点,品位也略有提高。为节约生产成本,试验采用阶段磨矿阶段选别的选矿工艺,即原矿磨矿(-0.074mm占60%)后,经一次粗选,一次扫选,粗精矿再磨(-0.038mm占85%)后再进行5次精选,最终获得钼精矿品位w(Mo)=50.007%,回收率为89.90%的较好指标。     

包头市地下水质量评价

地下水质量评价为保护和开发地下水资源,防止和控制地下水污染,保障人民身体健康提供科学依据。结合相关地下水调查资料采用单指标评价、内梅罗指数和模糊综合评价三种方法,对包头市地下水水质分别进行评价,通过对评价结果综合分析认为:模糊综合评价结果更符合区域地下水总体特征,包头市潜水Ⅳ类、Ⅴ类占到取样点总数的36%,质量整体较差;承压水Ⅰ—Ⅲ类遍及包头市全区,质量整体较好。