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941.
942.
943.
以镍铝水滑石为前体(主体),以蒸馏水为分散介质,用离子交换法组装丁二酸根(客体)插层水滑石,同时用一步合成法合成丁二酸根插层水滑石,并用XRD,IR,TG-DTA和元素分析等手段对样品进行了表征。结果表明,离子交换法制得的产品中丁二酸根阴离子取代了镍铝水滑石前体层间的碳酸根离子,组装得到晶体结构良好的丁二酸根插层水滑石,层间距为1.23nm。 相似文献
944.
钻孔倾斜仪监测在塘角村1^#滑坡预警监测中的作用 总被引:2,自引:0,他引:2
塘角村1^#滑坡是三峡库区地质灾害防治监测预警工程Ⅲ期专业监测点。监测方法为滑体深部位移监测、地表位移监测,同时开展地表宏观变形调查。2007年4月滑坡开始出现变形;其中滑体深部位移由钻孔倾斜仪监测,最早发现滑体变形,随后地表位移GPS监测滑体出现变形,同时滑体地表出现裂缝,滑体局部产生溜滑现象;文章通过滑体深部位移实测监测数据纵向分析,结合与其它监测方法(GPS)监测数据进行横向对比分析印证,判断钻孔倾斜仪监测数据的有效性、准确性;阐述钻孔倾斜仪监测在塘角村1号滑坡预警监测中的重要作用。 相似文献
945.
Tiexin Gu Wei Bu Weidong Yan Changyi Shi Mingcai Yan 《Geostandards and Geoanalytical Research》2003,27(2):193-196
Sulfide mineral certified reference materials GSO 1-7, recently prepared by the Institute of Geophysical and Geochemical Exploration (IGGE), were analysed by twelve laboratories. Various reliable analytical methods based on different principles were adopted and classical chemical methods were taken as the primary analytical methods, by which 5729 determinations were carried out, 1425 average data were obtained, and twenty one to twenty seven elements and components were certified. 相似文献
946.
碳酸盐岩礁滩体系是南海海域重要的油气储层之一.南海西沙岛屿全取心的科学钻井——西科1井, 为南海碳酸盐岩礁滩体系的详细研究提供极好的条件.通过西科1井岩心的宏观描述及微观分析, 结合高分辨岩心扫描及大量分析测试结果, 对碳酸盐岩礁滩体系展开了精细研究.根据识别出的6个暴露面、2个淹没面, 将西科1井中中新世以来划分为9个三级层序.其中晚中新世黄流组和第四系乐东组为主要成礁期, 以海泛面和暴露面为标志, 将礁体归纳为淹没型生长单元和暴露型生长单元两大类, 暴露型又进一步细分为硬基底和软基底两类, 淹没型可细分为快速淹没和缓慢淹没两类.垂向上形成了极具特色的礁体组合, 即慢步礁(或淹没礁)、同步礁(加积礁)、快步礁(暴露礁).研究成果对于南海生物礁生长过程及碳酸盐岩礁滩储层勘探具有重要参考价值. 相似文献
947.
Christopher Watson Richard Coleman Neil White John Church Ramesh Govind 《Marine Geodesy》2003,26(3):285-304
An absolute calibration of the TOPEX/Poseidon (T/P) and Jason-1 altimeters has been undertaken during the dedicated calibration phase of the Jason-1 mission, in Bass Strait, Australia. The present study incorporates several improvements to the earlier calibration methodology used for Bass Strait, namely the use of GPS buoys and the determination of absolute bias in a purely geometrical sense, without the necessity of estimating a marine geoid. This article focuses on technical issues surrounding the GPS buoy methodology for use in altimeter calibration studies. We present absolute bias estimates computed solely from the GPS buoy deployments and derive formal uncertainty estimates for bias calculation from a single overflight at the 40-45 mm level. Estimates of the absolute bias derived from the GPS buoys is -10 ± 19 mm for T/P and +147 ± 21 mm for Jason-1 (MOE orbit) and +131 ± 21 mm for Jason-1 (GPS orbit). Considering the estimated error budget, our bias values are equivalent to other determinations from the dedicated NASA and CNES calibration sites. 相似文献
948.
949.
Sign-constrained robust least squares, subjective breakdown point and the effect of weights of observations on robustness 总被引:3,自引:1,他引:3
Peiliang Xu 《Journal of Geodesy》2005,79(1-3):146-159
The findings of this paper are summarized as follows: (1) We propose a sign-constrained robust estimation method, which can
tolerate 50% of data contamination and meanwhile achieve high, least-squares-comparable efficiency. Since the objective function
is identical with least squares, the method may also be called sign-constrained robust least squares. An iterative version
of the method has been implemented and shown to be capable of resisting against more than 50% of contamination. As a by-product,
a robust estimate of scale parameter can also be obtained. Unlike the least median of squares method and repeated medians,
which use a least possible number of data to derive the solution, the sign-constrained robust least squares method attempts
to employ a maximum possible number of good data to derive the robust solution, and thus will not be affected by partial near
multi-collinearity among part of the data or if some of the data are clustered together; (2) although M-estimates have been
reported to have a breakdown point of 1/(t+1), we have shown that the weights of observations can readily deteriorate such results and bring the breakdown point of
M-estimates of Huber’s type to zero. The same zero breakdown point of the L
1-norm method is also derived, again due to the weights of observations; (3) by assuming a prior distribution for the signs
of outliers, we have developed the concept of subjective breakdown point, which may be thought of as an extension of stochastic
breakdown by Donoho and Huber but can be important in explaining real-life problems in Earth Sciences and image reconstruction;
and finally, (4) We have shown that the least median of squares method can still break down with a single outlier, even if
no highly concentrated good data nor highly concentrated outliers exist.
An erratum to this article is available at . 相似文献
950.
碳酸盐岩既可作为烃源岩,也可作为储集岩存在。因此,除直接发现液态石油和气苗外,在野外和室内碳酸盐岩含油的识别都较困难。确定碳酸盐岩中含有的烃类是原生的,还是它处运移充填而来的,这在勘探实践中具有不同的指导意义,本文阐述了用岩石热解分析技术判别碳酸盐岩中烃源的方法。提出了碳酸盐岩含油判别指数P、岩石热解烃最高温度Tmax和岩石中游离烃S1含量等判别碳酸盐岩是否含运移烃的指标。用此方法研究了西藏措勤盆地碳酸盐岩含油显示,发现强龙松纳背斜在1805剖面下白垩统郎山组1段(K1l^1)碳酸盐岩曾有油气运移过程存在。同时用其它方法证明了岩石热解技术对碳酸盐岩含运移烃的识别是可靠的。 相似文献