火焰原子吸收法间接测定磷矿中氯

火焰原子吸收法间接测定磷矿中氯达刘生１云南个旧市化肥厂中心化验室个旧６６１４１１目前磷矿中Ｃｌ－含量的测定多采用浊度法、氯离子选择电极法及离子色谱法。本文采用火焰原子吸收法来间接测定磷矿中Ｃｌ－，即在试样溶液中加入定量的Ａｇ＋，试样中Ｃｌ－与Ａｇ＋生...     

铋的原子吸收光谱分析进展

文章对１９８５年以来用原子吸收光谱法测定Ｂｉ的情况进行了综述，着重介绍了用氢化物发生法、石墨炉法和火焰法测Ｂｉ时，为了提高灵敏度所采用的各种氢化物发生装置及根据不同试样所使用的各种分离富集手段。主要参考文献１０１篇。     

电吸附找矿方法寻找隐伏金矿床的研究

电吸附找矿方法是指对采集的样品在室内特别装置中通电，并用吸附体吸附试样中电运移元素，通过这些元素所形成的异常来发现矿体的一种方法，该方法是依据野外地电提取方法的理论发展起来的，具有设备简单，成本低，工效效率高，工作条件及质量容易控制等优点。     

The transition from passive to active margin tectonics: a case study from the zone of Samedan (eastern Switzerland)

The Zone of Samedan is part of a fossil, early Mesozoic rift system originally situated in the distal, Lower Austro-Alpine domain of the Adriatic passive continental margin. An early Mesozoic configuration of asymmetrical rift basins bounded by relative structural highs compartmentalized Late Cretaceous active margin tectonics; Jurassic half-grabens were folded into arcuate synclines, whereas relative structural highs engendered thin, imbricated thrust sheets. West-directed thrusting and folding initiated at the surface and continued to depths favoring mylonitization under lower greenschist-facies conditions. At this time Liguria-Piemontese ophiolites were accreted to Lower Austro-Alpine units directly underlying the Zone of Samedan. Late Cretaceous orogenic collapse of the Adriatic active margin involved the reactivation of west-directed thrusts as low-angle, top-to-the-east, normal faults. These faults accommodated extensional uplift of Liguria-Piemontese ophiolites and Lower Austro-Alpine units beneath and within the Zone of Samedan. During Paleogene collision, some Late Cretaceous faults in the Zone of Samedan were reactivated under lower anchizonal conditions as north-directed thrusts. The latter stages of this early Tertiary thickening were transitional to brittle, high-angle normal faulting associated with top-to-the-east extension and spreading above the warm, uplifting Lepontine dome.     

碳酸盐岩的反射光谱特征的研究及应用

在室内对新疆塔里木盆地西北缘柯坪地区碳酸盐岩的反射光谱进行了测量。分析结果表明：碳酸盐岩的特征吸收谱带位于２３００～２３５０ｎｍ，随着碳酸盐岩中Ｍｇ２＋含量的增加，其特征吸收谱带的中心波长位置具有向短波长方向移动的特点；同时，随着碳酸盐岩中碳酸盐矿物含量的增加，其特征吸收谱带的深度（Ｄ）也有增大的趋势，并且岩石的平均反射率（Ｒ）也随着增高。根据这些特征可以判定碳酸盐岩的岩石类型及碳酸盐矿物的相对含量     

1995年永登5.8级地震多种前兆异常特征

研究了１９９５年７月２２日甘肃永登５．８级地震地电、水化学、水动态、地应力、地形变等５种前兆的异常特征，得到如下结论：①该次地震中短期（１年尺度）和短临异常空间分布符合“异常震源地点发震机制主要活断层”之间的特定关系，近２～３年的中期异常集中分布在西秦岭北缘北西向断裂带和海原通渭武都南北向断裂带上；②震前约１年时间尺度震源区发育起来了北北西南南东向挤压变化突出的附加应力场，并引起断层错动；③源兆集中分布在本次地震震源周围，场兆集中分布在上述两条活动断裂带上．源兆占异常的大多数，场兆占少数．在时间上场兆出现在先，源兆在后．     

An experimental study on seismic responses of multifunctional vibration‐absorption reinforced concrete megaframe structures

Two models are tested on a shake‐table. One of the models is a normal reinforced concrete megaframe structure and the other is a multifunctional vibration‐absorption reinforced concrete megaframe structure in which the laminated rubber bearings are placed between the major frame and the minor frames. Two earthquake motions (the El Centro wave and the Taft wave) are used during the test. This paper presents the dynamic characteristic, the seismic responses and the failure mechanism of these two models under varying peak acceleration levels for each of the earthquake motions. The test results demonstrate that the aseismic behavior of a multifunctional vibration‐absorption reinforced concrete megaframe structure is much better than that of a normal reinforced concrete megaframe structure. Copyright © 2003 John Wiley & Sons, Ltd.     

A comparative study on the illite crystallinity and the clay mineral reflectance spectral index for subdividing the very low-grade metamorphic belt along the Lizhou-Hekou geological section in the Youjiang sedimentary basin, Guangxi, China

To examine the application potential of hyperspectral remote sensing techniques in classifying very low-grade metamorphic belts, the composition of clay minerals and the cyrstallinity of illite from mudstones were measured using XRD and VIS-SWIR (400-2500 nm) reflectance spectroscopy. Based on the illite cyrstallinity, Kubler Index (KI), the Early Triassic LuoLou Group and the Middle Triassic lower Baifeng Formation were classified as the lower Epizone with KI△2θ° ranging from 0.22 to 0.25, the upper Baifeng Formation as upper anchizone with KI△2θ°ranging from 0.26 to 0.33, and the Hekou Formation as lower anchizone with KI△2θ° ranging from 0.38 to 0.40. According to a KI△2θ° value of 0.43, it is possible that there may exist a local diagenetic zone in the upper strata. The illite cyrstallinity Kubler index and the metamorphic grade increase from the bottom to the top of the stratigraphic sequence. The metamorphic grade boundaries nearly match the stratigraphic boundaries, indicating a burial metamorphism nature for the stratigraphic sequence. From the bottom to the top of the sequence, the spectral absorption band center of clay minerals from fresh rocks is around 2200 nm. The absorption band centers change towards shorter wavelengths: the Luolou Group being at 2220 nm, the Baifeng Formation at 2217-2213 nm, the lower member of the Hekou Formation at 2214-2206 nm, and the upper member of the Hekou Formation at 2205-2197 nm. The spectral absorption band center of illite shows the same change pattern. These results indicate that very low-grade metamorphic belts can be subdivided using spectral indices of clay minerals, which are measured by using field portable spectroradiometers. However, it may not work well with satellite and airborne sensors.     

The Present Space-Time Motion and Deformation Features of the Northeastern Margin of the Qinghai-Xizang（Tibet） Block and Its Adjacent Area

On the basis of Discontinuous Deformation Analysis (DDA), and considering the moderate intrusion of specific block boundaries to different extents, the first-order block motion model is established for the northeastern margin of Qinghai-Xizang(Tibet) block and the kinematical model for depicting deformation of small regions as well by using GPS observations of three periods (1991, 1999 and 2001). By simulating, we obtained the motion features of the firstorder blocks between the large WWN faults on the sides of the studied region, the distribution features of the principal strain rate field and the inhomogeneous motion features with spacetime of the faults in the northern boundary of the Qinghai-Xizang (Tibet) block.     

石墨炉原子吸收分光光度法测定土壤样品中痕量镉

研究了土壤样品中痕量镉的石墨炉原子吸收分光光度法测定最佳条件以及磷酸二氢铵与硝酸镁作基体改进剂对测定镉的基体改进效应，并比较了两种试样分解体系。方法检出限为0.01pg／L，精密度(RSD，n=8)为3．29％-7．69％，经国家一级标准物质分析验证，结果与标准值符合。