RP-HPLC法同时测定翅碱蓬中四种黄酮化合物的含量

建立RP-HPLC(反相高效液相色谱法)同时测定翅碱蓬中四种黄酮化合物-芸香苷、槲皮素3-β-D-葡萄糖苷、水仙苷和槲皮素的含量。采用Kromasil C18色谱柱(4.6 mm×250 mm,5μm),检测波长为361nm,柱温为30℃,流动相为甲醇-0.4%冰乙酸(55︰45),流速1.0mL/min,四种黄酮类化合物得到很好的分离。芸香苷、槲皮素3-β-D-葡萄糖苷、水仙苷和槲皮素浓度均为0.001~0.01 mg/mL范围内呈现良好线性关系,相关系数R2在0.9990~0.9996,加标回收率(n=3)范围为82.39%~99.03%。该方法简单、快速、高效,可以用于翅碱蓬中四种黄酮化合物的含量分析。     

一种基于点云法向量的基准特征提取与倾斜分析方法

针对目前将三维激光扫描技术应用于变形监测领域存在基准特征难以提取、点云数据分析缺乏适用的方法等问题,本文提出了一种基于点云法向量的基准特征提取与形变分析方法。首先利用局部平面拟合方法获得点云的法向量,并沿点云法矢方向探测基准点;然后利用三次B样条曲线对探测的正确基准点进行拟合;最后根据拟合曲线计算基准高程和对径点倾斜角分析基准特征形变信息。对某化工厂的罐体点云数据进行基准特征提取结果表明,该方法可以快速、全面地获取监测对象的整体信息,且能够正确分析监测对象的基准形变。     

再探温跃层有孔虫B/Ca与温度和[CO32-]的依赖性及其在24 ka以来热带西太平洋次表层碳酸盐系统重建中的应用

The B/Ca ratio of planktonic foraminifer shells has been used as a proxy for reconstructing past ocean carbonate chemistry. However, recent studies have revealed significant uncertainties associated with this proxy, such as whether seawater temperature or [ CO_3~(2-)] is the dominant control on the partition coefficient(K_D) of planktonic foraminiferal B/Ca. To address these uncertainties and thus improve our understanding of the planktonic foraminiferal B/Ca proxy, we analysed B/Ca ratios in the tests of Neogloboquadrina dutertrei(300–355 μm) and Pulleniatina obliquiloculata(355–400 μm) in surface sediment samples from the tropical western Pacific and South China Sea. The relationship between these B/Ca ratios and bottom water calcite saturation states(Δ[ CO_3~(2-)]) is weak, thus suggesting only a small dissolution effect on the B/Ca of the two species. The correlation coefficients(R~2) between the B/Ca ratios of N. dutertrei and P. obliquiloculata and environmental parameters(e.g., temperature, salinity, phosphate, DIC and ALK) in the tropical western Pacific and South China Sea are not high enough to justify using B/Ca ratios as a palaeoenvironmental proxy in the study areas. The significant correlation between K_D values of N. dutertrei and P. obliquiloculata and carbonate system parameters(e.g.,[ CO_3~(2-)], DIC, ALK, pH and [ HCO_3~-]) in the study area reflect chemical links between the K_D denominator and these variables. Based on our surface sediment calibration, an empirical relationship between the K_D of N.dutertrei and temperature is proposed in the tropical western Pacific. We also generated a record of B/Ca ratios in N. dutertrei(300–355 μm) from Core MD06-3052 in the tropical western Pacific over the past 24 ka to evaluate the application of the revised B/Ca proxy method. Based on the reconstructed empirical relationship for B/Ca and subsurface seawater ALK, we estimated subsurface seawater carbonate system parameters in the tropical western Pacific since 24 ka. In general, the estimated subsurface seawater pH and [ CO_3~(2-)] show an increase with time, and the record of subsurface seawater pCO_2 shows a decrease with time, in the tropical western Pacific over the past 24 ka. The consistent trends in subsurface seawater pCO_2 and opal flux during deglaciation may imply that the reported increase in subsurface water pCO_2 in the study area was promoted by enhanced upwelling in the Southern Ocean.     

黄河三角洲地区GF-3雷达数据与Sentinel-2多光谱数据湿地协同分类研究

黄河三角洲湿地的动态变化监测对湿地资源合理利用、开发保护具有重要意义。采用C波段全极化高分三号（GF-3）合成孔径雷达数据与欧洲空间局哨兵二号（Sentinel-2B）多光谱数据,分析了黄河三角洲湿地7类地物的光谱、指数、极化散射以及纹理等特征信息,分别基于最大似然法（maximum likelihood,ML）、决策树（decision tree,DT）、支持向量机（support vector machine,SVM）方法实现了有监督分类,评估了两者协同与单独应用于湿地地物分类与识别的能力,结果表明,两者协同分类时,其总体精度分别可达90.4%、95.4%、95.7%,均明显高于两者单独分类的结果,证明了GF-3雷达数据与多光谱数据在湿地协同分类方面的可靠性和应用潜力。     

基于B/S的测绘仪器信息管理系统的设计与实现

我国各工程单位拥有测绘仪器种类多种多样,开发一个实用有效的测绘仪器信息管理系统变得非常有必要。在Visual Studio 2013集成环境下结合ASP.NET网页编程技术、IIS服务器和SQL Server数据库技术开发了基于B/S的测绘仪器信息管理系统,详细介绍了系统的设计思想、架构体系和软硬件平台搭建等关键技术,提出了一系列对工程单位测绘仪器数字化管理的有效措施。     

基于Sentinel-1B SAR数据的洪水提取和监测

洪涝灾害是我国最严重的气象灾害之一,及时准确的洪灾监测是防灾减灾的重要前期工作和基础。本文利用sentinel-1B雷达数据,以黑瞎子岛为研究区,联合使用OSTU阈值分割法和随机森林面向对象分类法针对像素统计单波形、双波形、多波形SAR影像提取洪水要素,实现对洪灾淹没面积的时序监测,为灾情监测提供数据和技术支撑。     

单锚腿系泊系统动力计算的新方法

在Hamilton型拟变分原理体系下,建立了一种时间子域以三次和五次B样条函数插值的时间子域法,并将这种新方法用于单锚腿系泊系统的动力响应分析中。算例表明,新方法比传统的动力计算方法Wilson-θ法,在计算精度上有明显的优势,表明本方法能够用于计算单锚腿系泊系统的动力响应。     

基于双树复小波的CBERS-02B星遥感影像融合及评价

以CBERS-02星全色、多光谱图像及IKONOS多光谱图像为数据源,利用离散小波变换和双树复小波变换进行融合试验。结果表明,双树复小波变换在空间细节表现力和光谱保持方面能够较好地达到平衡,较离散小波变换更能提高图像融合质量。通过融合方法对比分析可知,02B星全色波段不仅与其多光谱波段融合能够得到信息更加丰富的图像,而且与其它传感器数据融合同样有很好的目视效果和可读性,具有较大的应用前景。