一种求地球化学异常下限的新方法——含量排列法

地球化学异常下限的确定,在矿产勘查和资源预测中占有十分重要的地位。传统计算地球化学异常下限的方法,要求数据服从正态分布或对数正态分布,而且存在计算依据不充分的问题。这里在研究背景和异常关系的基础上,提出了一种求地球化学异常下限的新方法,即含量排列法。该方法不要求数据服从正态分布或对数正态分布,直接用原始数据求异常下限,方法简便。用此方法对广东始兴地区化探数据进行处理,取得了较好的效果。     

紫外-可见分光光度法测定多花黄精多糖含量

目的：测定湖南洪江国家黄精标准化基地多花黄精中的多糖含量,为多花黄精的进一步开发利用及药材质量标准研究奠定基础。方法：以葡萄糖为标准品,采用硫酸-蒽酮试剂显色,应用紫外-可见分光光度法测定多花黄精多糖含量。结果：葡萄糖在3.28～19.68μg/mL范围内线性良好（r=0.9992）,多花黄精多糖平均含量为8.05%。结论：洪江种植基地的多花黄精品质优良,洪江是道地黄精药材种植理想基地。     

ICP--XSP测定珍珠中的稀土元素

珍珠的组成包括有机成分和无机成分。无机成分是珍珠的的主要成分,其主体是碳酸钙,含有Na、K、Mg、Cr、Cu、Zn、Ba、Pb、Fe等十多种微量元素,同时还含有及其微量的稀土元素。珍珠因具有装饰、美容、药用及保健功能而备受人们的厚爱。珍珠因化学成分上的差异导致了其价值。及应用上的差别。目前已经倾向于把珍珠作为矿物材料及药材进行结构组成的研究,     

浅析如何ICP测定铁矿石中硅、磷、锰、砷、锌

称取0．1g已干燥并磨细的试样于干净、已铺有0．8g混合熔剂（按无水碳酸钠：硼酸=2：1的比例,分别粉碎后拌匀,存放于干燥器内）的铂金坩埚内,用玻璃棒拌匀,再加0．8g混合熔剂均匀地覆盖试样,盖上坩埚盖。     

三江平原沟渠系统底泥中氮、磷的分布特征

以三江平原开发强度不同的浓江流域和别拉洪河流域两个多等级渠系为研究对象,根据农、斗、支、干四个渠道级别采集沟渠底泥,分析TN、TP、NH4-N、NO3-N和PO4-P在渠系的分布特征及影响机制,结果发现,在两个多等级渠系中,底泥氮磷含量最高值主要出现在支渠、干渠中。总的来说,随着沟渠级别的增加,渠道底泥所含养分元素有增加的趋势;浓江渠系渠道所含养分元素的量略低于别拉洪河渠系,别拉洪河渠系中养分元素易于在某一渠道积累,而浓江渠系随机性较大。     

Soil evolution features of debris flow waste-shoal land

The reclamation and utilization of debris flow waste-shoal land plays an important role in the mitigation and control of debris flow hazards, which thus contributes a lot to the exploitation of insufficient land resources in mountainous areas and the reduction of losses caused by debris flow. The aim of this paper is to discuss the features and mechanism of soil evolution of debris flow waste-shoal land so as to search for the available modes of its reclamation and utilization. The Jiangjiagou Ravine, a typical debris flow ravine, was selected to study soil evolution features of debris flow waste-shoal land based on the analysis of soil physieochemical properties and soil microstructure. It was found that the soil evolution rates of debris flow waste-shoal land varied with different modes of reclamation. For the land which had been reclaimed for less than lO years, soil evolved most rapidly in paddy fields, and more rapidly in dry farmland than in naturally restored waste-shoal land. For the land which had been used for more than lo years, the soil evolution rates of dry farmland, naturally restored waste-shoal land and paddy farmland decreased in the file. For the same utilization period of time, significant differences were recognized in soil evolution features under different modes of reclamation. Analysis data showed that soil clay content, soil thickness, the psephicity of skeleton particles and contents of microaggregates （〈0.02 mm） in paddy farmland were all highest. Soil nutrients and porosity of dry farmland were better than those of paddy farmland and naturally restored waste-shoal land, and those of paddy farmland were superior to those of naturally restored waste-shoal land. Paddy farmland characterized by rapid pedogenesis, stable evolution and high utilizability was the priority candidate for the reclamation and utilization of debris flow waste -shoal land.     

Effects of diet and body size on phosphorus utilization of Liza haematocheila T. ＆ S.

A 21-d laboratory experiment was conducted to study, the phosphorus （P） utilization of two different diets by redlip mullet Liza haematocheila T. ＆ S. Sand-filtered water in salinity 30 and temperatare 25℃ was used. Twenty-nine fish individuals were divided into three groups： 11 to group 1 （G1） fed on diet 1, 11 to group 2 （G2） fed on diet 2, and 7 to contrast group. Diet 1 was a commercial feed, more valuable in nutrition than diet 2 that similar to natural detritus. The results show the intake phosphorus （IP） of G1 was significantly higher than that of G2, and both increased linearly with body size at a certain amount of diet. The retention phosphorus （RP） in fish of G1 was lower than G2. The relationship between retention phosphorus and body size was positive and stronger in G2. Significant difference in faecal phosphorus （FP） was found between G1 and G2. Body size significantly impacted the excretion phosphorus （EP） in G1 but G2. The loss of intake phosphorus in G1 was 10.83-20.27 mg per g fish weight gain, higher than that in G2 for 6.63-9.56. Of the phosphorus, about 10% was allocated into growth, 50% in faeces, and the rest lost in excretion. The main part of phosphorus was lost in faeces but excretion. The phosphorus budget of the fish could be described as 100IP = 7.40RP ＋ 47.39FP ＋ 36.63EP （Diet 1） or 100IP = 11.93RP ＋ 56.64FP ＋ 21.76EP （Diet 2）.     

珠江河口经济动物体铜铅锌镉的含量

分别于2000年4月、2001年4月和2002年8月对珠江河口水域海洋经济动物体内Cu、Pb、Zn、Cd四种重金属元素的含量进行了调查分析,结果表明,14种经济动物体肌肉Cd、Cu、Pb、Zn各元素的平均含量分别是0.08、2.67、0.05、5.69mg·kg~(-1),其变化范围为nd～0.46mg·kg~(-1)、0.24～11.85mg·kg~(-1)、nd～0.26mg·kg~(-1)、1.55～18.36mg·kg~(-1)。甲壳类与头足类生物体内铜铅锌镉含量比较接近,远远高于鱼类的含量。所检测的14种经济类海洋动物中,虾姑、乌贼Cu的含量高于其余三种元素的含量,其余12种生物Zn的含量比另三种元素含量高。三次调查该水域经济类海洋动物体铜铅锌镉的含量基本一致。与水产品中有毒有害物质限量标准比较,14种被测样品铜、铅和镉的含量全部符合该标准的要求。