阿尔金江尕勒萨依榴辉岩和围岩锆石LA-ICP-MS微区原位定年及其地质意义

阿尔金江尕勒萨依榴辉岩及其直接围岩——石榴子石黑云母片麻岩锆石的阴极发光图像、微区原位LA-ICP-MS微量元素分析研究表明,榴辉岩锆石内部结构比较均匀,少数颗粒保留斑杂状残核;位于锆石斑杂状残核测点的重稀土相对富集,Th/U比值多大于0.4,为岩浆锆石的特征;位于锆石边部与内部结构均匀颗粒上的测点显示HREE近平坦型或弱亏损型的稀土配分模式,显示了与石榴石平衡共生的变质锆石特征;而石榴子石黑云母片麻岩的锆石具有核-幔-边结构,核部为碎屑锆石,幔部则为与石榴石平衡共生的变质锆石。LA-ICP-MS微区定年获得榴辉岩的变质年龄为(493±4.3)Ma,其原岩形成年龄为(754±9)Ma;石榴子石黑云母片麻岩的变质年龄为(499±27)Ma。榴辉岩的变质年龄滞后于其原岩的形成年龄约250Ma,并且榴辉岩与其直接围岩副片麻岩的变质年龄几乎完全一致,充分表明该超高压榴辉岩的形成是陆壳深俯冲作用的产物。     

A new understanding of Demala Group complex in Chayu Area,southeastern Qinghai-Tibet Plateau: Evidence from zircon U-Pb and mica 40Ar/39Ar dating

The Chayu area is located at the southeastern margin of the Qinghai-Tibet Plateau. This region was considered to be in the southeastward extension of the Lhasa Block, bounded by Nujiang suture zone in the north and Yarlung Zangbo suture zone in the south. The Demala Group complex, a set of high-grade metamorphic gneisses widely distributed in the Chayu area, is known as the Precambrian metamorphic basement of the Lhasa Block in the area. According to field-based investigations and microstructure analysis, the Demala Group complex is considered to mainly consist of banded biotite plagiogneisses, biotite quartzofeldspathic gneiss, granitic gneiss, amphibolite, mica schist, and quartz schist, with many leucogranite veins. The zircon U-Pb ages of two granitic gneiss samples are 205 ± 1 Ma and 218 ± 1 Ma, respectively, representing the ages of their protoliths. The zircons from two biotite plagiogneisses samples show core-rim structures. The U-Pb ages of the cores are mainly 644 –446 Ma, 1213 –865 Ma, and 1780 –1400 Ma, reflecting the age characteristics of clastic zircons during sedimentation of the original rocks. The U-Pb ages of the rims are from 203 ± 2 Ma to 190 ± 1 Ma, which represent the age of metamorphism. The zircon U-Pb ages of one sample taken from the leucogranite veins that cut through granitic gneiss foliation range from 24 Ma to 22 Ma, interpreted as the age of the anatexis in the Demala Group complex. Biotite and muscovite separates were selected from the granitic gneiss, banded gneiss, and leucogranite veins for ⁴⁰Ar/³⁹Ar dating. The plateau ages of three muscovite samples are 16.56 ± 0.21 Ma, 16.90 ± 0.21 Ma, and 23.40 ± 0.31 Ma, and the plateau ages of four biotite samples are 16.70 ± 0.24 Ma, 16.14 ± 0.19 Ma, 15.88 ± 0.20 Ma, and 14.39 ± 0.20 Ma. The mica Ar-Ar ages can reveal the exhumation and cooling history of the Demala Group complex. Combined with the previous research results of the Demala Group complex, the authors refer that the Demala Group complex should be a set of metamorphic complex. The complex includes not only Precambrian basement metamorphic rock series, but also Paleozoic sedimentary rock and Mesozoic granitic rock. Based on the deformation characteristics, the authors concluded that two stages of the metamorphism and deformation can be revealed in the Demala Group complex since the Mesozoic, namely Late Triassic-Early Jurassic (203 –190 Ma) and Oligocene –Miocene (24 –14 Ma). The early stage of metamorphism (ranging from 203 –190 Ma) was related to the Late Triassic tectono-magmatism in the area. The anatexis and uplifting-exhumation of the later stage (24 –14 Ma) were related to the shearing of the Jiali strike-slip fault zone. The Miocene structures are response to the large-scale southeastward escape of crustal materials and block rotation in Southeast Tibet after India-Eurasia collision.©2021 China Geology Editorial Office.     

激光探针等离子体质谱法（LAM—ICPMS）用于年龄锆石U—Pb定年

利用激光探针等离子体普（ＬＡＭ－ＩＣＰＭＳ）技术对中生代锆石进行了详细的２０６Ｐｂ／＾２３８定年研究。采用线扫描（Ｌｉｎｅ ｓｃａｎ）进样法减小了传统的剥深（Ｄｅｐｔｈ ｐｒｏｆｉｌｅ）进样法所引起的激光熔蚀分异效应;优化仪器参数可三ＩＣＰ－ＭＳ对Ｐｂ和Ｕ的质量歧视效应。测得了精确的＾２０６Ｐｂ／＾２３８Ｕ比值及年龄。研究结果表明,均匀颗粒锆石的＾２０６Ｐｂ／＾２３８Ｕ比值测量精度为２％～１０％,     

现代沉积的210Pb计年

²¹⁰Pb具有百年时间尺度沉积计年的重要价值。²¹⁰Pb_ex计年假设：沉积物是封闭系统；进入水体的²¹⁰Pb能有效地转移到沉积物中并不发生沉积后迁移；非过剩²¹⁰Pb与其母体²²⁶Ra保持平衡。²¹⁰Pb_ex计年可用稳定输入通量-稳定沉积物堆积速率模式、常量初始浓度模式或恒定补给速率模式。沉积物柱芯必须保持原态并以0．5～1cm间隔分截；用相应层节²²⁶Ra校正。沉积物表层混合作用及²²²Rn的丢失可能导致顶部²¹⁰Pb_ex异常。季节性缺氧湖泊沉积物顶部可能存在²¹⁰Pb及²¹⁰Po的再迁移。²¹⁰Pb与¹³⁷Cs两种计年方法原理上具有根本差别。²¹⁰Pb，¹³⁷Cs与沉积纹理方法对比是准确计年的重要保证。     

Late quaternary glacial stades in the Cordillera Central,Colombia, based on glacial geomorphology,tephra–soil stratigraphy,palynology, and radiocarbon dating

Using data from glacial geomorphology, tephra–soil stratigraphy and mineralogy, palynology, and radiocarbon dating, a sequence of glacial and bioclimatic stades and interstades has been identified for the last ca. 50000 yr in the Ruiz-Tolima massif, Cordillera Central, Colombia. Six Pleistocene cold stades separated by warmer interstades occurred: before 48000, between 48000 and 33000, between 28000 and 21000, from ≥16000 to ca. 14000, ca. 13000–12400, and ca. 11000–10000 yr BP. Although these radiocarbon ages are minimum-limiting ages obtained from tephra layers on top of tills, the tills are not significantly older because most are bracketed by dated tephra sets in measured stratigraphic sections. Two minor moraine stages likely reflect glacier standstill during cold intervals ca. 7400 yr BP and slightly earlier. Finally, glaciers readvanced between the seventeenth and nineteenth centuries. In contrast to the ice-clad volcanoes of the massif, ca. 34 km² in area above an altitude of ca. 4800 m, the ice cover expanded to 1200 km² during the Last Glacial Maximum (LGM) and was still 800 km² during Late-glacial time (LGT). Glacier reconstructions based on the moraines suggest depression of the equilibrium line altitude (ELA) by ca. 1100 m during the LGM and 500–600 m during LGT relative to the modern ELA, which lies at ca. 5100 m in the Cordillera Central. Glaciers in this region apparently reached their greatest extent when the climate was cold and wet, e.g. during stades corresponding to Oxygen Isotope Stage 3; glaciers were still expanding during the LGM ca. 28000–21000 yr BP, but they shrank considerably after 21000 yr BP because of greatly reduced precipitation. © 1997 John Wiley & Sons, Ltd.     

激光探针质谱及单颗粒矿物^40Ar／^39Ar法年龄的测定

将掺钕的钇铝榴石（Ｎｄ：ＹＡＧ）激光器与高精密ＭＭ１２００质谱计、电子倍增器联网，应用连续激光质谱对单颗粒矿物、光片样品进行微区４０Ａｒ／３９Ａｒ测年、坪年龄和等时线年龄研究。在光片上测定南极乔治王岛北海岸玄武岩等时线年龄（５２．３８±１．０５）Ｍａ和贵州绿豆岩年龄（２３９．１６±１４．１３）Ｍａ，两者与实际地质背景吻合。对两个中生代和太古代单颗粒黑云母进行连续激光质谱阶段升温４０Ａｒ／３９Ａｒ坪年龄谱测定，获得与常规法相一致的坪年龄谱     

哈达门沟金矿床成岩成矿时代的定点定年研究

哈达门沟大型钾长石 -石英脉型金矿床位于华北地台北缘西段的乌拉山地区。矿区西部的大桦背花岗岩和矿区内的伟晶岩脉与金矿化均具有较为密切的空间关系 ,这导致不少研究者认为哈达门沟金矿床与大桦背岩体或伟晶岩之间也具有时间和成因联系。通过采用先进的高灵敏的高分辨率的离子探针 (SHRIMP)对大桦背岩体、伟晶岩脉和钾长石化蚀变岩进行的锆石 U- Pb定点定年研究表明 :伟晶岩脉形成于 (1836± 5)× 10 6a,属吕梁旋回 ;大桦背岩体形成于 (353± 7)× 10 6a,应为海西旋回早期产物 ;金矿化年龄小于或等于 (132± 2 )× 10 6a,应为燕山晚期。这些年龄结果说明 ,本区金矿化比大桦背岩体晚至少 2 2 0× 10 6a,这排除了金矿化与大桦背岩体和伟晶岩脉之间有任何成因联系的可能性。蚀变岩的年龄还证明 ,虽然乌拉山和胶东地区金矿床的围岩和年龄不同 ,但两地区的金矿化却几乎同时发生。此外 ,大桦背岩体的形成年龄与华北地块和蒙古古陆块碰撞作用发生的时间基本一致 ,因此大桦背岩体的 SHRIMP年龄为这一碰撞作用提供了可靠的年代学证据。     

江西安远路迳金伯利质煌斑岩筒的Rb-Sr同位素年龄及其地质意义

报道了赣南安远县路迳金伯利质煌斑岩筒的 Rb-Sr等时线地质年龄 :t=( 3 7.6± 2 .2 ) Ma,初始值 [n( 87Sr) / n( 86Sr) ] i=0 .70 5 17± 0 .0 0 0 12。     

河北张家口水泉沟岩体SHRIMP年代学研究及其意义

采用先进的 SHRIMP测年技术对河北水泉沟碱性杂岩体进行了年龄测定，获得东坪金矿区水泉沟岩体二长岩锆石 U- Pb年龄为 (390± 6)Ma，后沟金矿区水泉沟岩体正长岩年龄 (386± 6)Ma，比较可信地确定了水泉沟岩体的成岩时代为晚加里东期—早海西期。这表明北部温都尔庙-西拉木伦河加里东俯冲造山运动强烈地影响本区，水泉沟岩体是这次运动的产物。根据前人测得的东坪和后沟金矿床蚀变围岩钾长石的 Ar- Ar和 K- Ar年龄，金矿化的时代是中生代燕山期，与岩体的成岩年龄有 200 Ma的时差，成因上可能与碱性杂岩体关系不大，因此，东坪和后沟等金矿床可能不属于碱性岩型金矿床。     

英峰岭红土-火山岩序列古地磁年代初步结果

夏商周断代工程的总目标是制订有科学依据的年表。研究途径主要有两条：1）根据古代天象记录，通过现代天文计算推定其年代；2）根据考古提供的系列样品作^14c年龄测定，转换成误差较小的、有考古内涵的历法年。天文推算可以得出年龄定点，^14C测年可以覆盖全面，建立起夏商周的年龄框架。两者结果互证，再同历史文献、考古研究等多学科综合研究，制订出夏商周三代年表。同过去相比，这应当是最有科学依据的。