膜分离技术的应用及发展趋势

综述世界和中国膜分离技术的发展，并对膜分离技术的基本特性、技术特点、膜材料、分类及膜分离装置进行了简单介绍；并介绍了膜分离法在化工及石油工业、食品工业、医药工业和医疗设备、生物技术和环境工程中的应用，并分析了膜分离技术将会在膜材料、新的膜过程和集成膜过程3个方面的发展趋势。同时指出如果能解决膜产品的价格、膜污染和膜分离性能的提高这3个膜的制约因素，膜分离技术将在人类社会的发展史上起到不可替代的作用。     

The vulnerability of karst springs—a case study of the Hubelj spring (SW Slovenia)

The hydraulic behaviour of the karst aquifer in the Hubelj spring catchment area (SW Slovenia) was studied by using an indirect research method based on natural tracers. The variations of natural tracers (in precipitation and in groundwater) during the storm event made possible the separation of the Hubelj spring storm hydrograph by the three-component separation technique. The results produced information on the aquifer recharge, storage and discharge processes, as well as on the mechanisms that affected them. They verified the so-called epikarst hypothesis presuming that an important part of a karst aquifer recharge reaches rapidly and intensively from the epikarst zone. It was demonstrated that epikarst water could occupy up to 50% of the spring discharge during precipitation events. This phenomenon could have important consequences on protection and management of the problems of karst aquifers, including engineering problems in karst areas. With this respect the results could give way to new engineering ideas.     

野外简易脱气装置简介

根据水力学原理结合水氡在实验室分析中水样鼓泡脱气的方法 ,进行了大量的野外试验 ,研制开发了野外简易脱气装置。通过几个月的试观测 ,脱气装置气流稳定 ,脱气效率高 ,完全可以满足自动化观测仪器对气量的需求。该装置解决了地下水化学在野外冷水泉无法进行气体观测的难题 ,而且制作简单、费用低廉 ,非常便于推广。     

钾-氩和氩-氩定年样品的送样要求及预处理

介绍了K-Ar和Ar-Ar法定年样品的送样要求及实验室预处理程序，样品粒度以250～180μm为宜；用量则视样品的K含量和年龄情况而定，K含量越高、年龄越老，所需样品量越少，多数样品的用量在几十至几百毫克；对于年龄情况不清楚的样品，10～20g手标本或者1～2g合适粒度的样品可以保证用量。全岩样品常受蚀变和捕虏晶的影响，有效的预处理可以在很大程度上消除这些干扰因素。文章还介绍了用稀HNO3消除碳酸盐、1．7mol／L HF消除轻微蚀变的影响以及电磁选剔除捕虏晶的实验过程。     

A mathematical model of concentrate solids content for the wet drum magnetic separator

Low concentrate density from wet drum magnetic separators in dense medium circuits can cause operating difficulties due to inability to obtain the required circulating medium density and, indirectly, high medium solids losses. The literature is almost silent on the processes controlling concentrate density. However, the common name for the region through which concentrate is discharged—the squeeze pan gap—implies that some extrusion process is thought to be at work. There is no model of magnetics recovery in a wet drum magnetic separator, which includes as inputs all significant machine and operating variables.A series of trials, in both factorial experiments and in single variable experiments, was done using a purpose built rig which featured a small industrial scale (700 mm lip length, 900 mm diameter) wet drum magnetic separator. A substantial data set of 191 trials was generated in this work. The results of the factorial experiments were used to identify the variables having a significant effect on magnetics recovery.It is proposed, based both on the experimental observations of the present work and on observations reported in the literature, that the process controlling magnetic separator concentrate density is one of drainage. Such a process should be able to be defined by an initial moisture, a drainage rate and a drainage time, the latter being defined by the volumetric flowrate and the volume within the drainage zone. The magnetics can be characterised by an experimentally derived ultimate drainage moisture. A model based on these concepts and containing adjustable parameters was developed. This model was then fitted to a randomly chosen 80% of the data, and validated by application to the remaining 20%. The model is shown to be a good fit to data over concentrate solids content values from 40% solids to 80% solids and for both magnetite and ferrosilicon feeds.     

氢化物分离一化学发光法测定痕量锑

采用Luminol－H。O。Air（巨）化学发光反应体系作为分析检测方法，建立了一个测定地质样品中痕量锑的化学发光分析法。方法的原理是用AgNO。吸收由样品发生的氢化锑气体，使吸收液中生成Sb（巨）与过量的K。Cr。O，反应生成Cr（1），方法的检出限为0．6us／mlSb，工作曲线的线性范围是2～1000ng／mlSb，测定的相对标准偏差小于5％。本方法已用于地质样品中痕量佛的测定。     

井间地震串联滤波波场分离方法

本文根据井间地震波场响应以及多种波场分离方法的性能，采用基于Ｋ－Ｌ变换的特征向量滤波与中值滤波相结合的串联滤波方法分离井间地震观测到的上、下行反射波。数值计算结果表明：在波场分离过程中，由于同时综合考虑了地震波能量主分量分布以及反射波同相轴时差两个参数，使得分离效果明显、处理更为简便，具有滤波特征矢量的选取条件更为宽松、无需精确确定拉平轴的时间等特点。     

地质样品中微量金银的在线分离富集方法

提出用ＶＳ－Ⅱ型强碱性阴离子交换纤维定量富集、硫脲解脱，流动注射在线分离富集—火焰原子吸收光谱法测定地质样品中痕量金银的分析方法。该方法检出限低，金为１．４μｇ／ｍＬ，银为０．３５μｇ／ｍＬ，相对标准偏差均小于２％，采样频率为１２０次／ｈ，用于地质样品中痕量金银的直接测定，结果令人满意。     

岩层移动动态过程的离散单元法分析

采动覆岩动态发展过程受地质、采矿条件诸多因素的影响,是一个十分复杂的时空过程。通过离散单元法数值模拟,揭示了综放开采条件下采场上覆岩层动态发展规律,特别是覆岩离层缝隙的分布规律、发展形态、空间位置以及与地质采矿条件的关系,揭示了工作面推进过程中,采场上覆岩层中重新分布的应力大小、方向及其发展变化规律,该应力的存在和变化规律是确定井下开采方法、支护方式的依据。