Dating alluvial deposits with optically stimulated luminescence, AMS C and cosmogenic techniques, western Transverse Ranges, California, USA

In an effort to better understand chronology of alluvial episodes in Cuyama Valley in the western Transverse Ranges of California, USA, we employed optically stimulated luminescence, radiocarbon and cosmogenic radionuclide surface exposure dating methods. Twenty-one optical dates ranging from 0.01 to 27 ka were obtained from exposures of late-Holocene axial-fluvial deposits, Pleistocene–Holocene alluvial-fan deposits, and axial-fluvial sands interbedded within a late Pleistocene alluvial fan. These were cross-checked with 37 AMS radiocarbon dates from charcoal and wood from within a and five ¹⁰Be surface exposure dates from boulders on alluvial-fan surfaces. The OSL results show generally good stratigraphic consistency, logical comparison with the radiocarbon and cosmogenic data, and appear to be the best method for accurate dating within deposits of this nature because suitable material is fairly easy to find in these environments. The radiocarbon data contained numerous “detrital ages”, but well-bedded lenses of apparently in situ or minimally transported charcoal provide reliable age estimates for the associated alluvium. Radiocarbon dating of detrital charcoal in the older alluvial fan deposits was problematic. Our cosmogenic surface-exposure dating was consistent stratigraphically and with our other data, but we were unable to determine its accuracy due to the limited number of samples and the possibility of inherited radionuclides and post-depositional erosion. In light of our results, we suggest that OSL dating using the latest analytical techniques combined with rigorous methods for estimation of paleodase is reliable and of increasing utility in otherwise difficult-to-date coarse alluvial environments in the southwestern United States and elsewhere.     

Dating of lower terrace sediments from the Middle Rhine area, Germany

Modern and known-age Pleistocene fluvial sediments were investigated by optical dating of quartz to test the suitability of the approach for dating deposits from the deeply incised Middle Rhine Valley. Samples from modern flood sediments revealed skewed distributions indicating different residual levels of equivalent dose (D_e) within the different aliquots. Nevertheless, a substantial number of aliquots from the modern deposits reflect D_e values close to zero. For the Pleistocene samples, optical ages are in general consistent with age control given by the presence of the Laacher See Tephra and radiocarbon dating. However, some samples overestimate the known age by a few thousand years when using the arithmetic mean. This is apparently explained by including aliquots in the determination of mean D_e where the optical signal was incompletely bleached at deposition. The most difficult issue in this context is identifying a suitable approach that can distinguish between the variability of D_e due to partial bleaching and microdosimetry. However, even when considering these limitations it appears that optical dating will by a quite suitable method to date Pleistocene sediments from such a complex fluvial environment, especially when focusing on a precision scale beyond a few thousand years.     

Comparison of TL multiple aliquot, single grain GLSL SAR and C-14 ages for the Puritjarra, Australia, rock shelter

We report single-grain quartz luminescence ages for the Puritjarra rock shelter, with the aim of resolving an apparent discrepancy between ages obtained by ¹⁴C and a variety of luminescence methods, previously reported. Ages now found at all depths to 75 cm (ages to 30 ka) can be interpreted as largely resolving the differences. This implied caveat arises because single-grain methods are statistically inefficient. As a consequence, a degree of interpretation is inevitable in analysing the data. The emphasis in the present paper is an analysis making use of weighted histograms. The measurements by single grain OSL and ¹⁴C, including ABOX–SC, taken together, can be regarded as compatible. They indicate human occupation of the Puritjarra rock shelter at least as early as 30 ka BP.     

TL age-estimates for the Middle Palaeolithic layers at Theopetra cave (Greece)

The lowest stratigraphic unit of Theopetra cave (Greece) contains a Middle Palaeolithic sequence radiocarbon dated to between 46 and 35 ka BP; at the limit of this dating method. The upper part of this sequence has yielded late Middle Palaeolithic lithic assemblages containing several early Upper Palaeolithic artifacts. To get more precise dates for the human occupation of the cave, burnt flint specimens from these Middle Palaeolithic layers were dated by thermoluminescence. The dates obtained are coherent and indicate that the first human occupation of the cave took place at the end of isotopic stage 6 or more probably at the beginning of stage 5, much earlier than previously proposed. In the light of this new evidence, it is reasonable to assume that: (a) Theopetra contains the oldest dated Middle Palaeolithic deposits of Greece and (b) that the assemblages first interpreted as “Transitional Middle/Upper Palaeolithic” industries may be the result of post-depositional mixing of cultural material.     

Establishing the time of initial human occupation of Liang Bua, western Flores, Indonesia

Liang Bua, a limestone cave in western Flores, has an archaeological and faunal sequence known to span the last 95 ka and is the type-site for a small-bodied hominid species, Homo floresiensis. This paper describes the geomorphic history of this significant site, and presents numerical ages for key events as determined by thermoluminescence dating of sediments (using a dual-aliquot regenerative-dose protocol) and uranium-series dating of flowstones. Our age estimates indicate that Liang Bua existed as a subterranean chamber by 400 ka ago. It was subsequently exposed by the incision of the Wae Racang River, which invaded the cave around 190 ka and deposited an upward-fining sequence of water-rolled boulders and cobbles. The latter conglomerate was partially reworked around 130 ka ago and was capped by flowstones at 100 ka. The conglomerate also contains stone artefacts, which implies that the occupation of the surrounding area is at least as old as the time of emplacement of the conglomerate. After 190 ka, a complex sequence of erosion and deposition led to the accumulation of at least 11 m of sediment in the front chamber of the cave, which proved suitable for hominid occupation. Such geochronological and geomorphological information is extremely valuable for interpreting the archaeological record at Liang Bua and its wider significance.     

Chronology of an oyster reef on the coast of Bohai Bay, China: Constraints from optical dating using different luminescence signals from fine quartz and polymineral fine grains of coastal sediments

Fossil oyster reefs are indicators of past sea levels, and their formation is usually dated by means of radiocarbon. However, radiocarbon dating of the shells from coastal areas may be complicated by the varying sources of carbon. Here we applied optical dating methods to date the samples from above and below a fossil oyster bed in a section on the coast of Bohai Bay, China. The optical ages of the sediments were used to constrain the oyster bed. Single-aliquot regenerative-dose procedures using the OSL signal from fine grain quartz, the IRSL and post-IR OSL signals from polymineral fine grains were employed to determine equivalent dose (D_e). The behaviors of the different luminescence signals from quartz and polymineral grains during D_e measurements were examined. The results showed that the quartz OSL signal is more reliable than the polymineral IRSL and post-IR OSL signals with respect to dating for these coastal samples. The optical ages indicated that the oyster reef formed between ca. 6.2 and 5.0 ka.     

ESR dating of fluvial quartz: Estimate of the minimal distance transport required for getting a maximum optical bleaching

An ESR experimental study of artificial optical bleaching of sedimentary quartz has shown that the aluminum center was maximally bleached after a 6-month illumination equivalent to natural light. This duration seems too long to apply in natural conditions. Nevertheless, the measurement of the ESR intensity of aluminum centers in quartz extracted from modern sediments and deposited in sandy bars shows that the maximum bleaching has effectively been reached.

In order to determine the relationship between the bleaching and the distance covered by a quartz grain in a river, samples were collected along the Creuse River (France) from its spring to about 170 km downstream, where maximum bleaching levels were observed in previous studies. The ESR intensities of the aluminum and titanium centers in quartz were measured, using X-band spectroscopy, before and after artificial bleaching. The difference measured between these sub-samples shows that the maximum bleaching level is obtained in the course of the first kilometer. Hence, the assumption that ESR dating of fluvial sediment is based on the optical bleaching was validated.     

Multiple phases of North African humidity recorded in lacustrine sediments from the Fazzan Basin, Libyan Sahara

The Fazzan Basin of south-west Libya is at present arid with less than 20 mm of rainfall per annum. However, regionally extensive limestones, lacustrine sands and coquina (fossiliferous carbonate rock) deposits show that the Fazzan Basin previously contained a large palaeolake, indicating that the climate in the past was more humid. Optically stimulated luminescence (OSL) dating techniques have been applied to key lacustrine deposits within the basin in an attempt to provide an internally consistent chronology for this humidity record. Results indicate that palaeolake sediments within the Fazzan Basin record a very long history of palaeohydrological change, ranging from present day arid conditions to humidity capable of sustaining a lake with an approximate area of 76,250 km². The existence of humid periods in mid oxygen isotope stage 5 and the early Holocene is confirmed. An older lacustrine event, tentatively correlated to oxygen isotope stage 11, is also recognized. In addition, evidence is presented for at least two humid phases beyond the age range over which the conventional OSL dating technique is applicable. This study demonstrates that OSL dating of palaeolake sediments within the Fazzan Basin offers the potential to provide a detailed record of North African humidity spanning several glacial–interglacial cycles.     

Implications of broad dose distributions obtained with the single-aliquot regenerative-dose method on quartz fine-grains from loess

Six samples were collected from a section of Peoria Loess in Eustis, North America, for optically stimulated luminescence (OSL) dating of quartz, and all except one (LV90) produced narrow dose distributions. A comparative study was conducted on this sample and on a ‘well-behaved’ sample (LV91), involving other dating methods and examination of the quartz OSL. These investigations revealed differences in the quartz OSL growth with dose, OSL response to thermal treatments and the range of components within the OSL signals. An ultra-fast component was found in LV90 that displayed a higher rate of sensitivity change than the fast component and this had a malign influence on the determination of the equivalent dose. The distinctive luminescence characteristics of LV90 imply either a change in wind dynamics and/or the source area for the silt.     

Wavefield continuation datuming using a near surface model

When topography and low velocity zone differences vary greatly, conventional vertical static time shifts will cause wavefield distortion and influence wave equation seismic imaging for seismic data acquired on a complex near surface. In this paper, we propose an approach to datum correction that combines a joint tomography inversion with wavefield continuation to solve the static problem for seismic data on rugged acquisition topography. First, the near surface model is obtained by refracted wave tomography inversion. Second, the wavefield of sources and receivers are continued downward and upward to accomplish datum correction starting from a flat surface and locating the datum above topography. Based on the reciprocal theorem, Huygens＇ and Fresnel principles, the location of sources and receivers, and regarding the recorded data on the surface as a secondary emission, the sources and receivers are upward-continued to the datum above topography respectively. Thus, the datum correction using joint tomography inversion and wavefield continuation with the condition of a complex near surface is accomplished.