U-Pb Age Determination for Seven Standard Zircons using Inductively Coupled Plasma–Mass Spectrometry Coupled with Frequency Quintupled Nd-YAG (λ = 213 nm) Laser Ablation System: Comparison with LA-ICP-MS Zircon Analyses with a NIST Glass Reference Material

This paper evaluates the analytical precision, accuracy and long‐term reliability of the U‐Pb age data obtained using inductively coupled plasma–mass spectrometry (ICP‐MS) with a frequency quintupled Nd‐YAG (λ = 213nm) laser ablation system. The U‐Pb age data for seven standard zircons of various ages, from 28 Ma to 2400 Ma (FCT, SL13, 91500, AS3, FC1, QGNG and PMA7) were obtained with an ablation pit size of 30 μm diameter. For ²⁰⁷Pb/²⁰⁶Pb ratio measurement, the mean isotopic ratio obtained on National Institute of Standards and Technology (NIST) SRM610 over 4 months was 0.9105 ± 0.0014 (n = 280, 95% confidence), which agrees well with the published value of 0.9096. The time‐profile of Pb/U ratios during single spot ablation showed no significant difference in shape from NIST SRM610 and 91500 zircon standards. These results encouraged the use of the glass standard as a calibration standard for the Pb/U ratio determination for zircons with shorter wavelength (λ = 213 nm) laser ablation. But ²⁰⁶Pb/²³⁸U and ²⁰⁷Pb/²³⁵U ages obtained by this method for seven zircon standards are systematically younger than the published U‐Pb ages obtained by both isotope dilution–thermal ionization mass spectrometry (ID‐TIMS) and sensitive high‐resolution ion‐microprobe (SHRIMP). Greater discrepancies (3–4% younger ages) were found for the ²⁰⁶Pb/²³⁸U ages for SL13, AS3 and 91500 zircons. The origin of the differences could be heterogeneity in Pb/U ratio on SRM610 between the different disks, but a matrix effect accuracy either in the ICP ion source or in the ablation‐transport processes of the sample aerosols cannot be neglected. When the ²⁰⁶Pb/²³⁸U (= 0.2302) newly defined in the present study is used, the measured ²⁰⁶Pb/²³⁸U and ²⁰⁷Pb/²³⁵U ages for the seven zircon standards are in good agreement with those from ID‐TIMS and SHRIMP within ±2%. This suggests that SRM610 glass standard is suitable for ICP‐MS with laser ablation sampling (LA‐ICP‐MS) zircon analysis, but it is necessary to determine the correction factor for ²⁰⁶Pb/²³⁸U by measuring several zircon standards in individual laboratories.     

倒Y形竖井联系测量

介绍在小直径竖井联系测量中取消联系三角形,改用单根钢丝定点,全站仪引测高程的施测方法。     

等截面单桩抗拔承载性状试验研究

在基坑中对等截面单桩进行了抗拔静载试验，在桩身设置应变式钢筋计，成功测得桩身各截面的应变数据。分析试验所得数据，对试验抗拔桩抗拔系数的取值、侧摩阻力的发挥、混凝土桩身的开裂等进行了探讨，相应给出了抗拔桩的设计建议。     

Centrifuge modelling-based verification of response spectra design methods for some vulnerable structures

Residential RC framed structures suffered heavily during the 2001 Bhuj earthquake in Gujarat, India. These types of structures also saw severe damage in other earthquakes such as the 1999 Kocaeli earthquake in Turkey and 921 Ji-Ji earthquake in Taiwan. In this paper the seismic response of residential structures was investigated using physical modelling. Idealised soft storey and top heavy, two degrees of freedom (2DOF) portal frame structures were developed and tested on saturated and dry sand models at 25 g using the Schofield Centre 10-m Beam Centrifuge. It was possible to recreate observed field behaviour using these models. As observed in many of the recent earthquakes, soft storey structures were found to be particularly vulnerable to seismic loads. Elastic response spectra methods are often used in the design of simple portal frame structures. The seismic risk of these structures can be significantly increased due to modifications such as removal of a column or addition of heavy water tanks on the roof. The experimental data from the dynamic centrifuge tests on such soft storey or top-heavy models was used to evaluate the predictions obtained from the response spectra. Response spectra were able to predict seismic response during small to moderate intensity earthquakes, but became inaccurate during strong earthquakes and when soil structure interaction effects became important. Re-evaluation of seismic risk of such modified structures is required and time domain analyses suggested by building codes such as IBC, UBC or NEHRP may be more appropriate.     

单一滑面边坡的非稳定蠕变模型分析

对单一滑面边坡的非稳定蠕变分析是边坡稳定性研究的基础。文中对岩质边坡单一滑面的流变变形机制进行了分析，提出了一种能较好反映这一变形机制的非稳定蠕变模型。特别是描述单一滑面边坡的非稳定蠕变破坏阶段，并对其稳定性进行了讨论。结合一些工程实例进行了对比验证，为滑坡灾害的预测和防治提供依据。     

内蒙古宝音图岩群变质基性火山岩锆石U-Pb年龄及意义

内蒙古达茂旗宝音图岩群是在达茂旗、查干呼绍地区 1:5万区调和白云鄂博幅 1:2 5万区调过程中从过去的巴特敖包群和白云鄂博群未分岩组解体出来的中级变质岩系。通过对宝音图岩群中阳起钠长片岩、二云片岩 (原岩均为基性火山岩 )进行单颗粒锆石U -Pb法年龄测定 ,获得了两条不一致线上交点年龄 (2 486± 42 )Ma、(2 496± 2 6 )Ma ,代表了宝音图岩群基性火山岩及宝音图岩群的形成时代 ;在不一致线之外不同成因的锆石的2 0 7Pb/ 2 0 6Pb表面年龄 (2 2 2 7± 15 )Ma ,寓示着 2 2 0 0Ma左右发生了一次区域性变质热事件 ;下交点年龄 (319±486 )Ma和 (40 6± 46 )Ma ,代表了 2 5 0～ 480Ma时期该区大面积岩浆侵位及宝音图岩群后期变形变质改造的时期 ,两个年龄样的获得为研究古元古代古陆的裂解及白云鄂博海槽的形成提供了直接依据。     

圆弧状沉积盆地与软土单覆盖层出平面地表运动对比

采用解析方法，通过圆弧状沉积盆地与同样参数的软土均匀单覆盖层的对比，研究沉积盆地对平面SH波二维散射效应和其出平面地表运动。数值对比结果表明：（1）波垂直入射时盆地中央地表位移幅值反应，其随频率变化形式与软土单覆盖层的地表运动有较强的对应性，且此时单覆盖层地表位移幅值为其下降；（2）盆地的二维散射效应特点显著波的汇聚作用使盆地中的地表运动显著放大，总体上较软土单覆盖层的地表位移幅值要大，其频域内的最大反应则明显大于单覆盖层情况，但最大反应在盆地表面出现的位置依赖于入射波角度、盆地深宽比和盆地的软硬程度；（3）沉积盆地中地表位移运动有强烈扭转效应，且随盆地变软和入射波频率增高而增强。     

TEM法在寻找煤矿突水巷道中的应用

在地质勘探中,TEM法体积效应影响小,探测深度大,对低阻反映灵敏,因此,其作为一种物探手段,已被广泛应用于地球物理勘探的各个领域。TEM法在煤矿突水巷道勘探中,曲线形态为高电位单峰异常,这个特征用于煤矿充水巷道探测准确度高,效果明显。     

桩承载力时效对桩土相互作用及沉降的影响分析

对软土中两根47 m长灌注桩分别在成桩28 d和1 750 d后进行了承载力试验，其极限承载力提高幅度达到30％左右。分析了单桩承载力随时间提高(称为时效)的机理，提出了单桩承载力时效对桩筏基础桩土相互作用影响的分析方法，并结合工程实例进行了分析。     

武汉长江底钻孔同位素单井法地下水流速、流向测试

本文论述了在武汉市长江底部第四纪孔隙含水层中用单井稀释法测定地下水流速、流向实验的过程和结果。并对在这种试验条件下所得的测定结果进行分析讨论,得出了相应的结论。测试结果表明:武汉长江底部JC II 6号钻孔处地下水流向从上到下都受到地表长江水流的影响。上部受到影响大,而深部较弱,地下水流向从上到下逐渐向东偏转35°左右。上部中细砂层中的地下水流速,大于下部粗中砂层中地下水流速。本次测试由于测定点靠近江心地下水排泄带,其地下水和地表水的水头差0 5m左右,试验虽然采取了特殊的施工工艺,也还可能受到垂向流的微小影响,使测试结果中的水流速度比实际地下水水流速度可能要稍偏大些。但因本点水文地质条件决定了三段之间或地下水流和江水之间无明显的水头差,所以引起的误差不大,可以忽略不计。