星载GPS低轨卫星运动学定轨及研究进展

重点论述了星载GPS低轨卫星运动学定轨的基本原理和方法,指出了各种运动学定轨法的优点和不足,分析了各种运动学定轨法解算的特点,并给出了相应的处理策略,同时着重介绍了星载GPS低轨卫星运动学定轨及相关研究的进展。     

Estimation of Distribution Algorithm for Initial Orbit Determination of Too-short-arc Based on Kernel Density Estimation

A new approach of the initial orbit determination for too-short-arc with angular measurements is implemented by building the probabilistic model in the solution space with the estimation of distribution algorithm. Without any assumption about distribution, the non-parametric kernel density estimation is employed in the model building. The method, unlike other evolutionary algorithms, such as the genetic algorithm and particle swarm optimization, considers the fitness as well as the characteristics of the solution space. Numerical experiments with real observations indicate that without any constraints, the proposed technique has a good performance for the observations of usual accuracy.     

双偏振天气雷达同时收发模式的一种改进方法

目前,双偏振多普勒天气雷达的同时发射方式受到了普遍关注,作者针对该方式中偏振参量差分反射率存在较大误差的问题,研究了双发射通道相位差与差分反射率精度的关系,以及双通道发射功率差、接收机增益等对差分反射率的影响.在此基础上,给出了双偏振同时发射方式的一种改进方案,并讨论了该方案的优势和特点,设计了双偏振多普勒天气雷达同时发射方式下回波信号的处理框图.     

星载加速度计增强北斗自主定轨性能

卫星自主定轨是提高全球卫星导航系统(GNSS)可靠性、稳健性、完整性和生存能力的重要保证。新一代的北斗卫星已可以进行星间链路测距,从而达到提高卫星全球跟踪能力以及实现整个卫星导航系统的自主定轨。然而由于卫星运行会受到多种摄动力的影响,如果不能对这些摄动力进行精密的改正,在没有地面或其他天体提供绝对约束的条件下,导航系统会随着自主定轨时间的延长出现星座整体旋转。卫星所受摄动力分为保守力和非保守力两部分:对于保守力,如地球非球形摄动、潮汐摄动、太阳月球和其他三体引力,现在已有的力学模型可以很精确地进行改正;而非保守力(如太阳光压摄动),则难以用精确的模型进行改正,因此成为影响卫星定轨精度的主要因素。星载加速度计可以高精度地测量非保守力,并已成功应用于重力卫星(CHAMP、GRACE、GOCE)的重力场反演与大气研究中。本文研究主要探讨采用星上加速度计提高北斗卫星自主定轨精度和延长自主定轨时长的可行性。利用模拟的卫星轨道和星间链路数据,以及现有的星载加速度计误差模型,对北斗卫星系统分别使用星间链路数据和星间链路与加速度计组合数据,进行自主定轨与精度评定。计算结果表明,使用星间链路与星载加速度计数据进行自主定轨,较单纯使用星间链路数据精度具有明显改进。在模拟的星间测距观测数据具有0.33m随机噪声以及分米级系统误差,自主定轨两个月的情况下,联合使用加速度计数据的自主定轨IGSO和MEO卫星精度为分米级,而仅使用星间链路数据的定轨精度约为3~6m,比使用加速度计精度低一个量级。     

偏心跟管钻进技术在公路高边坡加固工程中的应用

介绍了偏心跟管钻进技术在西安一安康高速公路某高边坡破碎地层中的成孔工艺、施工配套设施和相应的技术措施。     

An Evaluation of Methods for the Chemical Decomposition of Geological Materials for Trace Element Determination using ICP-MS

Complete dissolution is essential to obtain accurate analytical results using ICP-MS. In this study, decomposition techniques (i.e. acid digestions using Savillex Teflon vials, a high pressure digestion system and microwave oven, a combined lithium tetraborate fusion - HF/HNO3 acid decomposition and sodium peroxide sinter) for the total dissolution of different types of geological reference materials have been investigated. Savillex Teflon vial HF/HNO3 digestion is effective for basaltic samples. The high pressure HF/HClO4 digestion (PicoTrace TC-805 digestion system, Bovenden, Germany) allows dissolution of basalts and ironstones. Granites and magnetite-rich samples can be dissolved using a high pressure HF/H₂SO₄ method. Geological samples cannot be effectively attacked by microwave acid digestion. A combined lithium tetraborate fusion - HF/HNO3 acid digestion method allows complete dissolution of many different types of geological materials; however, this method precludes the determination of volatile elements due to the high fusion temperature (1000 °C). A sodium peroxide sinter method at 480 °C has the potential for the rapid determination of Y, Sc and REE in different types of geological materials. However, the lack of ultra-pure reagents precludes the use of lithium tetraborate fusion and sodium peroxide sinter methods for the measurement of geological samples with low trace element abundances.     

An Ion Chromatography Method for the Determination of Major Anions In Geothermal Water Samples

A single-column suppressed ion chromatography technique was employed for the simultaneous determination of major and trace anions in sulfaterich groundwater samples. An analytical column, a self regenerating suppressor and sodium carbonate as the eluent were used to separate the anions. Method detection limits for the anions of interest were 10.4, 15.9, 36.8, 62, 60, 61 and 67 μg l⁻¹ for F⁻, Cl⁻, NO₂⁻, Br⁻, NO₃⁻, PO₄³⁻ and SO₄²⁻ respectively. The precision of the method was tested at five different concentration levels for each anion reference sample to evaluate the effectiveness of the method for groundwater analysis. Recovery studies were performed between two successive months by adding reference samples to the geothermal groundwater and drinking water samples. Precision was also assessed as the relative standard deviation of both repeatability (within-day) and reproducibility (between-day and different concentrations) for groundwater samples. Standard deviation and RSD values of 220 groundwater samples acquired over 8 months were evaluated. The suppressed ion chromatography technique was found to be a suitable method for determining major anions in sulfate-rich geothermal water samples.     

翡翠的鉴定特征

根据翡翠的不同加工处理方式,市场上将翡翠分为A货、B货、C货3类,通过对翡翠A、B、C货的各种物理性质及内外部特征的比较,阐述了它们之间的鉴别方法和鉴定特点,以及红外光谱仪、拉曼光谱仪等在翡翠处理方法上的运用.     

塔里木盆地麦盖提斜坡皮山北新1井白云质角砾岩地层时代厘定

本文结合岩石薄片、古生物孢粉、同位素、铂族元素、野外露头剖面等资料,对塔里木盆地麦盖提斜坡皮山北新1井钻遇的一套白云质角砾岩地层时代进行了厘定。结果认为：6 884~7 068 m段归属古近系吐依洛克组,化石含量较少;7 068~7 150 m段归属白垩系依格孜牙组,孢粉化石丰富。该井古近纪与白垩纪地层界线深度7 068 m,该位置碳同位素的突变指示海洋环境的剧烈变化,这可以与全球K/E界线处对比。同时,铂族元素在该深度见到明显的异常,其含量明显增大,尤其以Rh、Ru、Ir、Os等最为明显。通过此次厘定,丰富了对麦盖提斜坡晚白垩世—古近纪早期沉积格局的认识。     

微波消解-化学蒸气发生-原子荧光光谱法同时测定铁矿石中的痕量砷和汞

采用HCl-HNO3混合酸(体积比1∶1)微波消解铁矿样品,在消解后的样品母液中直接加入硫脲-抗坏血酸,预还原五价砷为三价砷,消除铁和其他共存离子对砷、汞测定的干扰,采用化学蒸气发生-双道原子荧光光谱法同时测定铁矿石中的痕量砷和汞。结果表明5%的HCl-HNO3混合酸(体积比1∶1)、20 g/L硼氢化钾溶液能有效保证砷、汞双元素的同时测定,制备的砷、汞标准使用溶液在2～5℃下密闭保存,在245 d内具有稳定性。砷的检出限为0.085μg/L,汞的检出限为0.008μg/L。通过分析5个铁矿石有证标准物质,测定As的相对标准偏差为0.9%～5.5%,回收率为77.7%～105.4%,检测值与标准值吻合;测定Hg的相对标准偏差为1.1%～3.7%,回收率为86.2%～113.2%。本方法是以牺牲汞元素的检出限来实现砷、汞两元素的同时测定,是建立在砷、汞单独测定基础上的一种快速检测方法,经全国不同地区9家实验室采用5个标准样品进行协同实验验证,能够满足日常分析要求。