石墨炉原子吸收法测定钛铁矿中的微量镉

研究了石墨炉原子吸收测定钛铁矿中微量元素 Cd 的方法,探索了在高含量的 Fe,Ti 基体干扰下以NH4H2PO4-H2NCSNH2-EDTA为混合基体改进剂的最佳仪器工作条件。在取样0．2000g,定容25 mL的条件下,方法检出限为0．006μg/g,用国家标准物质验证,其准确度（犚犈％）＜10％,12次测定精密度（犚犛犇％）＜10％,加标回收率90％～110％之间,符合国家相关要求。     

CAMS: Cameras for Allsky Meteor Surveillance to establish minor meteor showers

First results are presented from a newly developed meteoroid orbit survey, called CAMS – Cameras for Allsky Meteor Surveillance, which combines meteor detection algorithms for low-light video observations with traditional video surveillance tools. Sixty video cameras at three stations monitor the sky above 31° elevation. Goal of CAMS is to verify meteor showers in search of their parent comets among newly discovered near-Earth objects.This paper outlines the concept of operations, the hardware, and software methods used during operation and in the data reduction pipeline, and accompanies the data release of the first batch of meteoroid orbits. During the month of November 2010, 2169 precisely reduced meteoroid trajectories from 17 nights have an error in the apparent radiant of the trajectory <2° and error in speed <10%. Median values of the error are 0.31° and 0.53 km/s, respectively, sufficient to resolve the intrinsic dispersion of annual meteor showers and resolve minor showers from the sporadic background. The limiting visual magnitude of the cameras is +5.4, recording meteors of +4 magnitude and brighter, bright enough to stand out from the mostly fainter sporadic meteors detected as under dense radar echoes.CAMS readily detected all established showers (6) active during the clear nights in November. Of the showers that needed confirmation, we confirm the theta Aurigids (THA, IAU#390), the chi Taurids (CTA, IAU#388), and the omicron Eridanids (OER, IAU#338). We conclude that the iota November Aurigids (IAR, IAU#248) are in fact the combined activity of the theta Aurigids and chi Taurids, and this shower should be dismissed from the list. Finally, there is also a clustering consistent with the zeta Cancrids (ZCN, IAU#243), but we cannot exclude that this is lower perihelion dust belonging to the Orionid shower.Data are submitted to the IAU Meteor Data Center on a semi-regular basis, and can be accessed also at http://cams.seti.org.     

e-VLBI技术及其在卫星定轨中的应用概况

e-VLBI技术继承了VLBI本身具有的极高角分辨率,且其利用高速通讯网络传送观测数据,能够快速得到观测结果,这些优点对于卫星的快速测定轨和提高卫星现有的定轨精度是十分有利的。通过对e-VLBI技术特点的分析及其发展历程的回顾,并结合卫星的差分VLBI观测原理,重点阐述和讨论了e-VLBI技术在我国的应用现状、发展及要求,展望了我国未来e-VLBI的发展前景。     

区域性椭球元素确定方法的比较

介绍目前常用的3种椭球变换方法并分析其特点,归纳E1-E6区域椭球元素及大地坐标变动量的公式.利用实测数据对多点法确定的E5椭球和定向定位调整法确定的E6椭球进行比较,结果表明:E6椭球面与投影面更加密切吻合,优于E5椭球.     

陆态网GPS精密定轨方法与精度分析

介绍中国大陆构造环境监测网络精密定轨的方法和过程。基于2011-04-10到2011-04-19连续10d的IGS核心站观测数据,分别用全球120个IGS核心站和77个IGS核心站进行比较计算,并给出了精密定轨精度的统计分析结果。     

Optimization of streamflow measurements by the dilution of the food colorant E110 / Optimisation de la mesure de débit par dilution du colorant alimentaire E110

Abstract

This study presents the measurement of streamflows by constant dilution of a yellow-orange food colorant (E110). Field measurements are carried out in the Doria River, a mountain torrent in the Savoie pre-Alps, France. A limnimetric station installed 12 years ago is periodically calibrated by mechanical and chemical measurements. Moreover, simultaneous mechanical and chemical methods allow the statistical validation of the proposed technique. The main advantages of this method are the lack of toxicity, the absence of visible river colouring, comparable to that of aquatic organic matter, and the low detection limit. This method allows high flow measurement under suitable conditions.     

新疆测震台网与中国地震台网测定的地震震级对比分析

选用2010～2012年间新疆境内和边邻地区MS≥4.0地震41个,以中国地震台网给出的震级为标准震级,对新疆台网记录的数字记录波形使用不同仪器分析、仿真处理。用速度量记录直接计算,将速度量记录仿真为短周期WA位移记录、中长周期SK仪记录的勒夫波和长周期763仪记录的瑞利波位移记录计算震级,分别进行了震级偏差统计分析,初步得出震级偏差值的震级校正值,有利于提高新疆地震台网速报地震震级的准确性。     

An application of problem and product ontologies for the revision of beach nourishments

An ontological approach in GIS serves as a framework for the conceptualization of processes in the real world. In this paper, we examine an application in coastal change in the Netherlands, whereby beaches are subject to artificial nourishment to offset the effect of severe erosion. The use of ontologies helps to define two scenarios: S_I determined by the regulations from the Ministry for Public Works; S_II grounded on the abilities from an existing spatial dataset. A comparison between S_I and S_II shows that 72.8% of the objects suitable and unsuitable for nourishment are correctly classified. A higher overlap is found in areas where actual beach nourishments were carried out. Inaccuracies in attributes influence the determination of the objects. A sensitivity analysis applied to altitude illustrates a significant increase of objects suitable for nourishment for both scenarios, when altitude is decreased within the lower limit of the root mean square error for the 95% confidence interval. Moreover, the sensitivity of altitude shows that artificial boundaries for beach nourishment objects are not reasonable and consequently should be treated as vague objects.     

Determination of Fluoride Ions in Iron Ores by UV–VIS Spectrophotometry after Matrix Removal Using Diphonix® Resin

A modification of the spectrophotometric method for the determination of fluoride ions in iron‐rich materials is proposed. In this method the iron matrix was successfully removed using Diphonix^® resin. The studied sample was a ferruginous mineral which contained about 38% of iron. The Euronorm certified reference material (ECRM) 676‐1 (Iron Ore Sinter), as a commercially available material having a similar matrix (39.76% w/w Fe) and fluoride level (0.1% w/w), was used to validate the method. After partial digestion in concentrated hydrochloric acid the samples were diluted and passed through Diphonix^® resin. The concentration of fluoride ions was determined by a spectrophotometric method using a Zr:ER complex (λ = 540 nm). The result obtained for the ECRM was in good agreement with the certificate specification and thus proved the method to be applicable for the determination of fluoride ions in iron‐rich materials. Due to the easy digestion step and simple requirements for equipment, this method can be used in most laboratories.     

格栅坝（桩林）混凝土施工质量及温度控制

结合舟曲县罗家峪沟泥石流灾害治理工程格栅坝钢筋混凝土施工实例,介绍在受限条件下大体积混凝土在施工中采用质量控制技术措施及控制温度裂缝,为类似格栅坝混凝土施工提供借鉴。