化探样品中部分元素测定溶矿方法的改进

文章研究了用 1∶1王水分解化探样品中Cu、Pb、Zn、Co、Ni、Fe、Mn等元素新的样品溶解测定方法 ,即王水分解测定法 ,该法的检出限、准确度、精密度均达到 1∶5万化探样品分析要求。此法已用于化探及区域地质普查样品分析 ,并取得了较好效果     

1:25万多目标区域地球化学调查样品的分析测试质量监控方法

在1：25万多目标区域地球化学调查样品分析的质量监控方法中，提出以准确度与精密度并重，标准物质监控与重复样监控相结合。利用“多目标化探样品计算机管理软件”，实现对调查样品分析质量监控的自动化管理。应用该系统软件，只要建立好相应的分析数据库，就可自动获得分析报告、报出率、内检样检查、标样检查、标样监控图等监控数据。     

双星轨道拟合的研究进展

双星轨道拟合是天文学的一项基础性研究工作。其主要目的是给出双星系统的二体轨道参数,这些参数不仅是高精度、高网格密度星表参考架的必要组成部分,而且也为理解各种有关观测现象提供了必要的动力学基础;更重要的是,双星轨道拟合可以直接估计恒星物理和星系天文学等领域极有应用价值的恒星质量参数。因此,长期以来双星轨道拟合工作一直受到研究者的广泛关注。近年来,随着高精度的恒星运动学观测资料的大量积累,双星轨道拟合更成为天体测量和天体力学的一个共同的热点课题,有关研究也有了长足的进展。综述了双星轨道拟合的历史及现状,其中着重介绍了目前所用的主要观测资料和各种具体的拟合模型、拟合方法;简要描述了几种主要的双星星表;展望了今后双星轨道拟合工作的发展趋势。     

A digital elevation analysis: a spatially distributed flow apportioning algorithm

An integrated flow determination algorithm is proposed to calculate the spatial distribution of the topographic index to the channel network. The advantages of a single flow direction algorithm and other multiple flow direction schemes are selectively considered in order to address the drawbacks of existing algorithms. A spatially varying flow apportioning factor is introduced to distribute the contributing area from upslope cells to downslope cells. The channel initiation threshold concept is expanded and integrated into a spatially distributed flow apportioning algorithm to delineate a realistic channel network. The functional relationships between the flow apportioning factors and the expanded channel initiation threshold (ECIT) are developed to address the spatially varied flow distribution patterns considering the permanent channel locations. A genetic algorithm (GA) is integrated into the spatially distributed flow apportioning algorithm (SDFAA) with the objective function of river cell evaluation. An application of a field example suggests that the spatially distributed flow apportioning scheme provides several advantages over the existing approaches; the advantages include the relaxation of overdissipation problems near channel cells, the connectivity feature of river cells and the robustness of the parameter determination procedure over existing algorithms. Copyright © 2004 John Wiley & Sons, Ltd.     

精密定轨用地球大气模型误差的补偿方法

本文提出了一种用于精密轨道确定的地球大气模型误差的补偿方法，这种方法采用改进 大气周日峰角的技术，有效地补偿了大气密度模型的误差，并具有较好的物理意义．与传统 的每圈改进一次加速度的方法比较，轨道确定达到了相当的径向精度，且避免了轨道改进参 数间的相关性，同时解算参数的数量也少了一半．     

荧光分光光度法测定海洋生物中的谷胱甘肽

对应用荧光分光光度法测定海洋生物中还原型谷胱甘肽(GSH)含量的方法进行了研究,并测定了分属于鱼、虾、贝、藻的10种海洋生物中谷胱甘肽的含量。利用邻苯二甲醛与GSH反应构成的荧光体系,在激发波长为365nm,发射波长为425nm的条件下,方法的回收率为99.22%~99.69%,变异系数为2.16%。应用此方法测得10种海洋生物中谷胱甘肽的含量为:红笛鲷(Lutjanussanguineus)0.399mg/g,银鲳(Pampusargenteus)0.352mg/g,大海鲢(Megalopscyrinoides)0.561mg/g,尖紫蛤(Sanguinolariaacuta)0.289mg/g,菲律宾蛤仔(Ruditapesphilippinarun)0.287mg/g,墨吉对虾(Penaeusmerguiensis)0.892mg/g,凡纳滨对虾(Litopenaeusvannamei)1.434mg/g,囊藻(Colpomeniasinu-ose)0.221mg/g,石莼(Ulvalactucal)0.727mg/g,马尾藻(Sargassummuticum)0.137mg/g。     

Orbital linkages of Comet 6P/d'Arrest based on its asymmetric light curve

We present an investigation of different models of the nongravitational acceleration on Comet 6P/d'Arrest, as used in orbital linkages spanning 150 years from the discovery of the comet in 1851 until the recent observations made in 2001. Some of our models use the time-shifted g-like function to represent the variation of outgassing rate, but the main thrust is on models using instead a production curve that is fitted to recent light curve observations—mainly those in 1976. We pay special attention to the proper scaling of such a production curve, when applied to other apparitions with a different perihelion distance q, and we find a best fit with a q^−1.6 power-law. Generally, the best fit is found with models, in which the acceleration components are expressed in terms of the angular parameters of the rotating nucleus. We thus find the orientation of the spin axis, and using the orbital evolution we are able to predict a variable time shift of the outgassing curve. The very best results are found when applying this time shift to the light-curve based, angular models. The totality of the 1851-2001 observations can then be linked with a mean residual of less than 4″. This may be brought down to ∼^2″ by solving for individual ‘activity parameters’ of all apparitions, which are multiplicative factors applied to the acceleration amplitudes. These turn out to be within 10% of unity for the best fit. We have also performed a linkage to the observations of Comet 1678 (La Hire) using our models. We find an indication of a secular increase of the amount of asymmetry of the outgassing with respect to perihelion, part of which is due to the variable time shift caused by the orbital evolution.     

SHORT COMMUNICATION APPLICATION OF THE POWELL METHOD TO THE OPTIMIZATION OF FLOW INJECTION SYSTEMS

This paper describes the application of the Powell algorithm to the optimization of a flow injectionsystem configuration.The performance of this algorithm has been compared with the modified simplexmethod.The system studied is the determination of ammonia,based on the indophenol blue reaction.Alinear combination of sensitivity and sample throughput is used as the objective function because of itssimultaneous optimization capability.Results obtained show that the proposed method may reach theoptimal conditions with a lower number of experimental evaluations.     

Synthetically adaptive robust filtering for satellite orbit determination

The precise orbit information is the premise of the application of satellite, and the precise orbit deter- mination includes dynamic and geometric methods. The dynamic method estimates the position and veloc-ity of a satellite at one epoch by extending the obser-vational arc in order to include more observations of different epochs in it. It is realized by integrating the dynamic equation of the satellite so that the observa-tions at different epochs are related to the particular state. The dy…